The forming limit diagrams ( FLD ) of AZ31B magnesium alloy sheet were tested by means of the electro etching grid method based on the forming experiment of magnesium alloy sheet carried out with a BCS- 30D sheet fo...The forming limit diagrams ( FLD ) of AZ31B magnesium alloy sheet were tested by means of the electro etching grid method based on the forming experiment of magnesium alloy sheet carried out with a BCS- 30D sheet forming testing machine and the strain testing analysis made with an advanced ASAME automatic strain measuring system. Experiments show that, at room temperature, the mechanical properties and deep drawing peorformance of AZ31B cold-rolled magnesium alloy sheet were so poor that it failed to test the forming limit diagrams without an ideal forming and processing capacity, while the hot-rolled magnesium alloy sheet was of a little better plasticity and forming peorformance after testing its forming limit diagrams. It can be concluded that the testing of the forming limit curves ( FLC ) offers the theoretical foundation for the drawing of the deep drawing and forming process of magnesium alloy sheet.展开更多
In this study,the effects of pre-strain-induced tensile twins(TTWs)and controlled heat treatment on the formability behavior of AZX311 Mg alloy sheets were investigated.A 4%compressive strain was applied to pre-strain...In this study,the effects of pre-strain-induced tensile twins(TTWs)and controlled heat treatment on the formability behavior of AZX311 Mg alloy sheets were investigated.A 4%compressive strain was applied to pre-strain the sheets using the in-plane compression(IPC)technique along the rolling direction(RD)to introduce TTWs.The pre-strained(PS)samples were subsequently heat-treated at 250℃,350℃,and 400℃ independently for 1 hr,and are termed as PSA1,PSA2,and PSA3,respectively.Erichsen cupping tests were conducted to assess the formability of the sheet samples under different initial conditions.The results showed that the PS sample heat-treated at 250℃ for 1hr exhibited a decrease in the Erichsen index(IE)compared to the as-rolled sample,whereas PSA2 and PSA3 samples showed an increase in IE values.Microtexture analysis revealed that most of the TTWs generated through pre-twinning were stable at 250℃;however,the twin volume fraction reduced to 41%at 350℃ compared to the PS samples due to enhanced thermal activity at that temperature.Furthermore,PSA2 samples showed severe grain coarsening in some areas of the sample,and the fraction of such grains increased in the PSA3 samples.The stretch formability(IE value)of PSA2 samples showed a 32.3%increase compared to the as-rolled specimens.Additionally,the analysis of the deformed specimen at failure under the Erichsen test indicated that considerable detwinning occurs in the PS and PSA1 samples,whereas dislocation slip activity dominates in the PSA2 and PSA3 samples during stretch forming.Apart from detwinning and dislocation slip,deformation twins were also observed in all samples after the Erichsen test.Thus,this work highlights the importance of texture control and its underlying mechanisms via pre-twinning followed by heat treatment and their impact on the room temperature(RT)stretch formability of AZX311 Mg alloy sheets.展开更多
Low-alloyed magnesium(Mg)alloys have emerged as one of the most promising candidates for lightweight materials.However,their further application potential has been hampered by limitations such as low strength,poor pla...Low-alloyed magnesium(Mg)alloys have emerged as one of the most promising candidates for lightweight materials.However,their further application potential has been hampered by limitations such as low strength,poor plasticity at room temperature,and unsatisfactory formability.To address these challenges,grain refinement and grain structure control have been identified as crucial factors to achieving high performance in low-alloyed Mg alloys.An effective way for regulating grain structure is through grain boundary(GB)segregation.This review presents a comprehensive summary of the distribution criteria of segregated atoms and the effects of solute segregation on grain size and growth in Mg alloys.The analysis encompasses both single element segregation and multi-element co-segregation behavior,considering coherent interfaces and incoherent interfaces.Furthermore,we introduce the high mechanical performance low-alloyed wrought Mg alloys that utilize GB segregation and analyze the potential impact mechanisms through which GB segregation influences materials properties.Drawing upon these studies,we propose strategies for the design of high mechanical performance Mg alloys with desirable properties,including high strength,excellent ductility,and good formability,achieved through the implementation of GB segregation.The findings of this review contribute to advancing the understanding of grain boundary engineering in Mg alloys and provide valuable insights for future alloy design and optimization.展开更多
This study investigated the influence of graded Zn content on the evolution of precipitated and iron-rich phases and grain struc-ture of the alloys,designed and developed the Al–8.0Zn–1.5Mg–1.5Cu–0.2Fe(wt%)alloy w...This study investigated the influence of graded Zn content on the evolution of precipitated and iron-rich phases and grain struc-ture of the alloys,designed and developed the Al–8.0Zn–1.5Mg–1.5Cu–0.2Fe(wt%)alloy with high strength and formability.With the increase of Zn content,forming the coupling distribution of multiscale precipitates and iron-rich phases with a reasonable matching ratio and dispersion distribution characteristics is easy.This phenomenon induces the formation of cell-like structures with alternate distribu-tion of coarse and fine grains,and the average plasticity–strain ratio(characterizing the formability)of the pre-aged alloy with a high strength is up to 0.708.Results reveal the evolution and influence mechanisms of multiscale second-phase particles and the corresponding high formability mechanism of the alloys.The developed coupling control process exhibits considerable potential,revealing remarkable improvements in the room temperature formability of high-strength Al–Zn–Mg–Cu alloys.展开更多
Repeated unidirectional bending (RUB) was carried out to improve the texture of commercial AZ31B magnesium alloy sheets. All specimens were prepared in the rolling direction. The forming limit diagrams (FLDs) of A...Repeated unidirectional bending (RUB) was carried out to improve the texture of commercial AZ31B magnesium alloy sheets. All specimens were prepared in the rolling direction. The forming limit diagrams (FLDs) of AZ31B magnesium alloy sheet were determined experimentally by conducting stretch-forming tests at room temperature, 100, 200 and 300 ℃ Compared with the as-received sheet, the lowest limited strain of AZ31B magnesium alloy sheet with tilted texture in the FLD increased by 79% at room temperature and 104% at 100 ℃. The texture also affected the extension of the forming limit curves (FLC) in the FLD. However, the FLCs of two kinds of sheets almost overlapped at temperature above 200 ℃. It can be concluded that the reduction of (0002) texture intensity is effective to the improvement of formability not only at room temperature but also at low-and-medium temperature. The effect of texture on FLDs becomes weak with increasing temperature.展开更多
The influences of strength coefficient K, work hardening exponent n and thickness t of the overlapping sheet on bulging process are analyzed based on hardening material model. Also, bulging experiments are carried out...The influences of strength coefficient K, work hardening exponent n and thickness t of the overlapping sheet on bulging process are analyzed based on hardening material model. Also, bulging experiments are carried out by taking the aluminum alloy LF21 as formed sheet metal, and selecting overlapping sheet with different thicknesses and material properties, by which accuracy of the above analysis result is verified in the aspects of geometric shape, thickness distribution and limit bulging height. The results show that higher strength coefficient K, larger work hardening exponent n and proper thickness of the overlapping sheet are helpful to improve the formability and forming uniformity of formed sheet metal.展开更多
The effect of the repeated unidirectional bending (RUB) process and annealing on the formability of magnesium alloy sheets was investigated. The RUB process and annealing treatments produce two effects on microstruc...The effect of the repeated unidirectional bending (RUB) process and annealing on the formability of magnesium alloy sheets was investigated. The RUB process and annealing treatments produce two effects on microstructure: grain coarsening and weakening of the texture. The sheet that underwent RUB and was annealed at 300 ℃exhibits the best formability owing to the reduction of the (0002) basal texture intensity, which results in low yield strength, large fracture elongation, small Lankford value (r-value) and large strain hardening exponent (n-value). Compared with the as-received sheet, the coarse-grain sheet produced by RUB and annealing at 400 ℃ exhibits lower tensile properties but higher formability. The phenomenon is because the deformation twin enhanced by grain coarsening can accommodate the strain of thickness.展开更多
The effects of strain rate on microstructure and formability of AZ31B magnesium alloy sheets were investigated through uniaxial tensile tests and hemispherical punch tests with strain rates of 10^-4, 10^-3, 10^-2, 10^...The effects of strain rate on microstructure and formability of AZ31B magnesium alloy sheets were investigated through uniaxial tensile tests and hemispherical punch tests with strain rates of 10^-4, 10^-3, 10^-2, 10^-1 s^-1 at 200℃. The results show that the volume fraction of dynamic recrystallization grains increases and the original grains are gradually replaced by recrystallization grains with the strain rate decreasing. A larger elongation and a smaller r-value are obtained at a lower strain rate, moreover the erichsen values become larger with the strain rate reducing, so the formability improves. This problem arises in part from the enhanced softening and the coordination of recrystallization grains during deformation.展开更多
Influence of thermomechanical processing on the microstructure, texture evolution and mechanical properties of A1-Mg-Si-Cu alloy sheets was studied systematically. The quite weak mechanical properties anisotropy was o...Influence of thermomechanical processing on the microstructure, texture evolution and mechanical properties of A1-Mg-Si-Cu alloy sheets was studied systematically. The quite weak mechanical properties anisotropy was obtained in the alloy sheet through thermomechanical processing optimizing. The highly elongated microstmcture is the main structure for the hot or cold-rolled alloy sheets. H {001 } (110) and E { 111 } (110) are the main texture components in the surface layer of hot-rolled sheet, while ]/-fibre is dominant in quarter and center layers. Compared with the hot-rolled sheet, the intensities offl-fibre components are higher after the first cold rolling, but H {001 }(110) component in the surface layer decreases greatly. Almost no deformation texatre can be observed after intermediate annealing. And fl-fibre becomes the main texture again after the final cold rolling. With the reduction of the thickness, the through-thickness texture gradients become much weaker. The through-thickness recrystallization texture in the solution treated sample only has cubeyD {001 }(310) component. The relationship among thermomechanical processing, microstructure, texture and mechanical orouerties was analyzed.展开更多
Flow behavior of the Al-Si coated boron steel was investigated with Gleeble-3500,in comparison with the uncoated one.Effect of deformation conditions on the coating integrity was characterized by optical microscopy.Fa...Flow behavior of the Al-Si coated boron steel was investigated with Gleeble-3500,in comparison with the uncoated one.Effect of deformation conditions on the coating integrity was characterized by optical microscopy.Facture surfaces of the coated steels were inspected under SEM.Experimental results indicate that the ultimate tensile strength and ductility of the Al-Si coated boron steel are lower than those of the uncoated steel under test conditions.Extensive cracks occur in the coating after tensile tests;the width and density of cracks are sensitive to the deformation temperatures and strain rates.The bare substrate exposed between the separate coating segments is oxidized.Appearance of the oxide degrades the Al-Si coating adhesion.Remarkable difference between formability of the coating layer and the substrate is confirmed.The formability of the Al-Si coating could be optimized by controlling the phase transformation of the ductile Fe-rich intermetallic compounds within it during the austenization.展开更多
Ring hoop tension test and tube bulging test were carried out at elevated temperatures up to 480 ℃to evaluate the formability of AZ31B extruded tube for internal high pressure forming (IHPF) process. The total elon...Ring hoop tension test and tube bulging test were carried out at elevated temperatures up to 480 ℃to evaluate the formability of AZ31B extruded tube for internal high pressure forming (IHPF) process. The total elongation along hoop direction and the maximum expansion ratio (MER) of the tube were obtained. The fracture surface after bursting was also analyzed. The results show that the total elongation along hoop direction and the MER value have a similar changing tendency as the testing temperature increases, which is quite different from the total elongation along axial direction. Both the total elongation along hoop direction and the MER value increase to a peak value at about 160 ℃. After that, they begin to decrease quickly until a certain rebounding temperature is reached. From the rebounding temperature, they begin to increase rapidly again. Burnt structure appears on the fracture surface when tested at temperatures higher than 420 ℃. Therefore, the forming temperature of the tested tube should be lower than 420 ℃, even though bigger formability can be achieved at higher temperature.展开更多
Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analys...Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analysis and experiments of viscous warm pressure bulging (VWPB) of AZ31B magnesium alloy were conducted to analyze the influence of different ellipticity dies on the formability of AZ31B magnesium alloy. At the same time, based on the grid strain rule, the forming limit diagram (FLD) of VWPB of AZ31B magnesium alloy was obtained through measuring the strain of bulging specimens. The results showed that at the temperature range of viscous medium thermal stability, the viscous medium can fit the geometry variation of sheet and generate non-uniform pressure field, and as the die ellipticity increases, the difference value of non-uniform pressure reduces. Meanwhile, according to the FLD, the relationship between part complexity and ultimate deformation was investigated.展开更多
The formability of AA5052/polyethylene/AA5052 sandwich sheets was experimentally studied. Three kinds of AA5052/polyethylene/AA5052 sandwich specimens with different thicknesses of core materials were prepared by the ...The formability of AA5052/polyethylene/AA5052 sandwich sheets was experimentally studied. Three kinds of AA5052/polyethylene/AA5052 sandwich specimens with different thicknesses of core materials were prepared by the hot pressing adhesive method. Then, the uniaxial tensile tests were conducted to investigate the mechanical properties of AA5052/polyethylene/ AA5052 sandwich sheets, and the stretching tests were carried out to investigate the influences of polymer core thickness on the limit dome height of the sandwich sheet. The forming limit curves for three kinds of sandwich sheets were obtained. The experimental results show that the forming limit of the AA5052/polyethylene/AA5052 sandwich sheet is higher than that of the monolithic AA5052 sheet, and it increases with increasing the thickness of polyethylene core.展开更多
Experimental study has been conducted for an interstitial free(IF) sheet steel on its surface roughness evolution and formability with respect to grain size and sheet thickness effect. The surface roughness of IF she...Experimental study has been conducted for an interstitial free(IF) sheet steel on its surface roughness evolution and formability with respect to grain size and sheet thickness effect. The surface roughness of IF sheet steel is proportional to effective strain, grain size and inversely proportional to sheet thickness; the larger grain reduces the formability by accelerating the surface roughening rate and enhance formability by raising the workhardening rate, while the latter effect plays the dominate role. The grain size effect on surface roughening and formability is more obvious when the sheets are thinner.展开更多
The effectsof melt overheating degree on the undercooling degree and resultant solidification structures of Nd9Fe85-xTi4C2Bx(x=10, 12) glass-forming alloyswerestudied by differential thermal analysis combining with ...The effectsof melt overheating degree on the undercooling degree and resultant solidification structures of Nd9Fe85-xTi4C2Bx(x=10, 12) glass-forming alloyswerestudied by differential thermal analysis combining with solidification structure analysis. The results indicate that the undercooling degree of Nd9Fe85-xTi4C2Bx(x=10, 12) alloys significantly increaseswith the rise of melt overheating degree, and two overheating degree thresholds corresponding to the drastic increase of the mean undercooling degree are found for each of the alloys. The existence of two turning points of the mean undercooling degreescan be linked to the structure transitions inside the overheated melts, which result in the evident increase of volume fraction of amorphous phasein the solidified structures.展开更多
The effect of friction coefficient on the deep drawing of aluminum alloy AA6111 at elevated temperatures was analyzed based on the three conditions using the finite element analysis and the experimental approach.Resul...The effect of friction coefficient on the deep drawing of aluminum alloy AA6111 at elevated temperatures was analyzed based on the three conditions using the finite element analysis and the experimental approach.Results indicate that the friction coefficient and lubrication position significantly influence the minimum thickness,the thickness deviation and the failure mode of the formed parts.During the hot forming process,the failure modes are draw mode,stretch mode and equi-biaxial stretch mode induced by different lubrication conditions.In terms of formability,the optimal value of friction coefficient determined in this work is 0.15.At the same time,the good agreement is performed between the experimental and simulated results.Fracture often occurs at the center of cup bottom or near the cup corner in a ductile mode or ductile-brittle mixed mode,respectively.展开更多
The deformation behavior and mechanism of Ti2AlNb-based alloy were experimentally investigated at elevated temperatures. Firstly, the stress?strain relationships at different temperatures and strain rates were investi...The deformation behavior and mechanism of Ti2AlNb-based alloy were experimentally investigated at elevated temperatures. Firstly, the stress?strain relationships at different temperatures and strain rates were investigated via uniaxial tensile testing. Then, formability data, as determined by examining the deep drawing and bending abilities, were obtained through limiting draw ratio (LDR) and bending tests. Finally, metallographic experiments and fracture morphology investigations were conducted to examine the thermal deformation mechanism of the alloy. The results showed that as the temperature increased, the total elongation increased from 13.58% to 97.82% and the yield strength decreased from 788 to 80 MPa over the temperature range from 750 to 950 °C at a strain rate 0.001 s?1. When the temperature reached 950 °C, the strain rate was found to have a great influence on the deformation properties. The plastic formability of the sheet metal was significantly improved and a microstructuraltransformation of O toB2 andα2 occurred in this temperature region, revealing the deformation mechanism of its plasticity.展开更多
Mg-Li alloy,as a superlight metallic engineering material,shows great potential in the fields of aerospace and militarydue to its high specific strength,better formability,and excellent electromagnetic shielding perfo...Mg-Li alloy,as a superlight metallic engineering material,shows great potential in the fields of aerospace and militarydue to its high specific strength,better formability,and excellent electromagnetic shielding performance.The research process ofMg-Li alloys is reviewed and three main problems are pointed out.Aimed at the poor corrosion resistance of Mg-Li alloys,thecorrosion behavior is mainly summarized.The surface treatment technologies,including electroplating,electroless plating,plasmaspraying,molten salt replacement,conversion coating,anodizing,micro-arc oxidation,organic coating,and organic-inorganic hybridcoating,are introduced in detail.Finally,the future development of corrosion and protection of Mg?Li alloys is discussed.展开更多
Mg and its alloys have continued to attract interest for several structural and super-sensitive applications because of their light weight and good combination of engineering properties.However for some of these appli...Mg and its alloys have continued to attract interest for several structural and super-sensitive applications because of their light weight and good combination of engineering properties.However for some of these applications,high plastic deformability is required to achieve desired component shapes and configurations;unfortunately,Mg and its alloys have low formability.Scientifically,the plastic behaviour of Mg and its alloys ranks among the most complex and difficult to reconcile in metallic material systems.But basically,the HCP crystal structure coupled with low stacking fault energies(SFE)are largely linked to the poor ductility exhibited by Mg alloys.These innate material characteristics have regrettably limited wide spread applicability of Mg and its alloys.Several research efforts aimed at exploring processing strategies to make these alloys more amenable for high formability–mediated engineering use have been reported and still ongoing.This paper reviews the structural metallurgy of Mg alloys and its influence on mechanical behaviour,specifically,plasticity characteristics.It also concisely presents various processing routes(Alloying,Traditional Forming and Severe Plastic Deformation(SPD))which have been explored to enhance plastic deformability in Mg and its alloys.Grain refinement and homogenising of phases,reducing CRSS between slip modes,twinning suppression to activate non-basal slip,and weakening and randomisation of the basal texture were observed as the formability enhancing strategies explored in the reviewed processes.While identifying the limitations of these strategies,further areas to be explored for enhancing plasticity of Mg alloys are highlighted.展开更多
The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were perf...The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were performed by pre-strain paths,i.e.,tension(6%)and compression(5%)perpendicular to the c-axis along extrusion direction(ED),to investigate the microstructural evolution and mechanical properties of AZ31 Mg alloy sheets.The distinction in the texture evolution and strain hardening behavior was illustrated in connection with the pre-strain paths for the activities of twinning and slip.The result shows that the activation of the deformation mode was closely bound up with the grain orientation and the additional applied load direction.The{10–12}twin-texture components with c-axis//ED were generated by precompression,which can provide an appropriate alternative to accommodate the thin sheet thickness strain and enhance the room temperature formability of Mg alloy sheet.展开更多
文摘The forming limit diagrams ( FLD ) of AZ31B magnesium alloy sheet were tested by means of the electro etching grid method based on the forming experiment of magnesium alloy sheet carried out with a BCS- 30D sheet forming testing machine and the strain testing analysis made with an advanced ASAME automatic strain measuring system. Experiments show that, at room temperature, the mechanical properties and deep drawing peorformance of AZ31B cold-rolled magnesium alloy sheet were so poor that it failed to test the forming limit diagrams without an ideal forming and processing capacity, while the hot-rolled magnesium alloy sheet was of a little better plasticity and forming peorformance after testing its forming limit diagrams. It can be concluded that the testing of the forming limit curves ( FLC ) offers the theoretical foundation for the drawing of the deep drawing and forming process of magnesium alloy sheet.
基金supported by the Science and Engineering Research Board(SERB),a statutory body of the Department of Science&Technology(DST),Government of India through the Start-up Research Grant(SRG)scheme(File No.SRG/2020/000341).
文摘In this study,the effects of pre-strain-induced tensile twins(TTWs)and controlled heat treatment on the formability behavior of AZX311 Mg alloy sheets were investigated.A 4%compressive strain was applied to pre-strain the sheets using the in-plane compression(IPC)technique along the rolling direction(RD)to introduce TTWs.The pre-strained(PS)samples were subsequently heat-treated at 250℃,350℃,and 400℃ independently for 1 hr,and are termed as PSA1,PSA2,and PSA3,respectively.Erichsen cupping tests were conducted to assess the formability of the sheet samples under different initial conditions.The results showed that the PS sample heat-treated at 250℃ for 1hr exhibited a decrease in the Erichsen index(IE)compared to the as-rolled sample,whereas PSA2 and PSA3 samples showed an increase in IE values.Microtexture analysis revealed that most of the TTWs generated through pre-twinning were stable at 250℃;however,the twin volume fraction reduced to 41%at 350℃ compared to the PS samples due to enhanced thermal activity at that temperature.Furthermore,PSA2 samples showed severe grain coarsening in some areas of the sample,and the fraction of such grains increased in the PSA3 samples.The stretch formability(IE value)of PSA2 samples showed a 32.3%increase compared to the as-rolled specimens.Additionally,the analysis of the deformed specimen at failure under the Erichsen test indicated that considerable detwinning occurs in the PS and PSA1 samples,whereas dislocation slip activity dominates in the PSA2 and PSA3 samples during stretch forming.Apart from detwinning and dislocation slip,deformation twins were also observed in all samples after the Erichsen test.Thus,this work highlights the importance of texture control and its underlying mechanisms via pre-twinning followed by heat treatment and their impact on the room temperature(RT)stretch formability of AZX311 Mg alloy sheets.
基金the support of the National Natural Science Foundation of China(52071093 and 51871069)the Natural Science Foundation of Heilongjiang Province of China(LH2023E059)+1 种基金the Fundamental Research Program of Shenzhen Science and Technology Innovation Commission(JCYJ20210324131405015)PolyU Grant(1-BBR1)。
文摘Low-alloyed magnesium(Mg)alloys have emerged as one of the most promising candidates for lightweight materials.However,their further application potential has been hampered by limitations such as low strength,poor plasticity at room temperature,and unsatisfactory formability.To address these challenges,grain refinement and grain structure control have been identified as crucial factors to achieving high performance in low-alloyed Mg alloys.An effective way for regulating grain structure is through grain boundary(GB)segregation.This review presents a comprehensive summary of the distribution criteria of segregated atoms and the effects of solute segregation on grain size and growth in Mg alloys.The analysis encompasses both single element segregation and multi-element co-segregation behavior,considering coherent interfaces and incoherent interfaces.Furthermore,we introduce the high mechanical performance low-alloyed wrought Mg alloys that utilize GB segregation and analyze the potential impact mechanisms through which GB segregation influences materials properties.Drawing upon these studies,we propose strategies for the design of high mechanical performance Mg alloys with desirable properties,including high strength,excellent ductility,and good formability,achieved through the implementation of GB segregation.The findings of this review contribute to advancing the understanding of grain boundary engineering in Mg alloys and provide valuable insights for future alloy design and optimization.
基金supported by the National Key Research and Development Program of China(No.2021YFE0115900)the National Natural Science Foundation of China(Nos.52371016,51871029,and 51571023)the Opening Project of State Key Laboratory for Advanced Metals and Materials(Nos.2020-ZD02 and No.2022-Z03).
文摘This study investigated the influence of graded Zn content on the evolution of precipitated and iron-rich phases and grain struc-ture of the alloys,designed and developed the Al–8.0Zn–1.5Mg–1.5Cu–0.2Fe(wt%)alloy with high strength and formability.With the increase of Zn content,forming the coupling distribution of multiscale precipitates and iron-rich phases with a reasonable matching ratio and dispersion distribution characteristics is easy.This phenomenon induces the formation of cell-like structures with alternate distribu-tion of coarse and fine grains,and the average plasticity–strain ratio(characterizing the formability)of the pre-aged alloy with a high strength is up to 0.708.Results reveal the evolution and influence mechanisms of multiscale second-phase particles and the corresponding high formability mechanism of the alloys.The developed coupling control process exhibits considerable potential,revealing remarkable improvements in the room temperature formability of high-strength Al–Zn–Mg–Cu alloys.
基金Project(CSTC2010AA4035)supported by Scientific and Technological Project of Chongqing Science and Technology Commission,ChinaProject(50504019)supported by the National Natural Science Foundation of China+1 种基金Project(CDJZR11130008)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(CDJXS10130001)supported by the Chongqing University Postgraduates'Science and Innovation Fund,China
文摘Repeated unidirectional bending (RUB) was carried out to improve the texture of commercial AZ31B magnesium alloy sheets. All specimens were prepared in the rolling direction. The forming limit diagrams (FLDs) of AZ31B magnesium alloy sheet were determined experimentally by conducting stretch-forming tests at room temperature, 100, 200 and 300 ℃ Compared with the as-received sheet, the lowest limited strain of AZ31B magnesium alloy sheet with tilted texture in the FLD increased by 79% at room temperature and 104% at 100 ℃. The texture also affected the extension of the forming limit curves (FLC) in the FLD. However, the FLCs of two kinds of sheets almost overlapped at temperature above 200 ℃. It can be concluded that the reduction of (0002) texture intensity is effective to the improvement of formability not only at room temperature but also at low-and-medium temperature. The effect of texture on FLDs becomes weak with increasing temperature.
基金Project(51205260)supported by the National Natural Science Foundation of ChinaProject(L2012046)supported by the Liaoning Provincial Committee of Education,China
文摘The influences of strength coefficient K, work hardening exponent n and thickness t of the overlapping sheet on bulging process are analyzed based on hardening material model. Also, bulging experiments are carried out by taking the aluminum alloy LF21 as formed sheet metal, and selecting overlapping sheet with different thicknesses and material properties, by which accuracy of the above analysis result is verified in the aspects of geometric shape, thickness distribution and limit bulging height. The results show that higher strength coefficient K, larger work hardening exponent n and proper thickness of the overlapping sheet are helpful to improve the formability and forming uniformity of formed sheet metal.
基金Project(CSTC2010AA4035)supported by Scientific and Technological Project of Chongqing Science and Technology Commission,ChinaProject(50504019)supported by the National Natural Science Foundation of China+1 种基金Project(CDJZR11130008)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(CDJXS10130001)supported by the Chongqing University Postgraduates'Science and Innovation Fund,China
文摘The effect of the repeated unidirectional bending (RUB) process and annealing on the formability of magnesium alloy sheets was investigated. The RUB process and annealing treatments produce two effects on microstructure: grain coarsening and weakening of the texture. The sheet that underwent RUB and was annealed at 300 ℃exhibits the best formability owing to the reduction of the (0002) basal texture intensity, which results in low yield strength, large fracture elongation, small Lankford value (r-value) and large strain hardening exponent (n-value). Compared with the as-received sheet, the coarse-grain sheet produced by RUB and annealing at 400 ℃ exhibits lower tensile properties but higher formability. The phenomenon is because the deformation twin enhanced by grain coarsening can accommodate the strain of thickness.
基金Project(CSTC2010AA4035) supported by Scientific and Technological Project of Chongqing Science and Technology Commission, ChinaProject(CDJZR11130008) supported by the Fundamental Research Funds for the Central Universities,ChinaProject (2008DFR50040) supported by the Ministry of Science and Technology of China
文摘The effects of strain rate on microstructure and formability of AZ31B magnesium alloy sheets were investigated through uniaxial tensile tests and hemispherical punch tests with strain rates of 10^-4, 10^-3, 10^-2, 10^-1 s^-1 at 200℃. The results show that the volume fraction of dynamic recrystallization grains increases and the original grains are gradually replaced by recrystallization grains with the strain rate decreasing. A larger elongation and a smaller r-value are obtained at a lower strain rate, moreover the erichsen values become larger with the strain rate reducing, so the formability improves. This problem arises in part from the enhanced softening and the coordination of recrystallization grains during deformation.
基金Project(2013AA032403) supported by the National High-Tech Research and Development Program of ChinaProject(YETP0409) supported by the Beijing Higher Education Young Elite Teacher Project in 2013,ChinaProject(51301016) supported by the National Natural Science Foundation of China
文摘Influence of thermomechanical processing on the microstructure, texture evolution and mechanical properties of A1-Mg-Si-Cu alloy sheets was studied systematically. The quite weak mechanical properties anisotropy was obtained in the alloy sheet through thermomechanical processing optimizing. The highly elongated microstmcture is the main structure for the hot or cold-rolled alloy sheets. H {001 } (110) and E { 111 } (110) are the main texture components in the surface layer of hot-rolled sheet, while ]/-fibre is dominant in quarter and center layers. Compared with the hot-rolled sheet, the intensities offl-fibre components are higher after the first cold rolling, but H {001 }(110) component in the surface layer decreases greatly. Almost no deformation texatre can be observed after intermediate annealing. And fl-fibre becomes the main texture again after the final cold rolling. With the reduction of the thickness, the through-thickness texture gradients become much weaker. The through-thickness recrystallization texture in the solution treated sample only has cubeyD {001 }(310) component. The relationship among thermomechanical processing, microstructure, texture and mechanical orouerties was analyzed.
基金Project (51275185) supported by the National Natural Science Foundation of China
文摘Flow behavior of the Al-Si coated boron steel was investigated with Gleeble-3500,in comparison with the uncoated one.Effect of deformation conditions on the coating integrity was characterized by optical microscopy.Facture surfaces of the coated steels were inspected under SEM.Experimental results indicate that the ultimate tensile strength and ductility of the Al-Si coated boron steel are lower than those of the uncoated steel under test conditions.Extensive cracks occur in the coating after tensile tests;the width and density of cracks are sensitive to the deformation temperatures and strain rates.The bare substrate exposed between the separate coating segments is oxidized.Appearance of the oxide degrades the Al-Si coating adhesion.Remarkable difference between formability of the coating layer and the substrate is confirmed.The formability of the Al-Si coating could be optimized by controlling the phase transformation of the ductile Fe-rich intermetallic compounds within it during the austenization.
基金Project(50805033)supported by the National Natural Science Foundation of ChinaProject(E200804)supported by the Natural Science Foundation of Heilongjiang Province of China
文摘Ring hoop tension test and tube bulging test were carried out at elevated temperatures up to 480 ℃to evaluate the formability of AZ31B extruded tube for internal high pressure forming (IHPF) process. The total elongation along hoop direction and the maximum expansion ratio (MER) of the tube were obtained. The fracture surface after bursting was also analyzed. The results show that the total elongation along hoop direction and the MER value have a similar changing tendency as the testing temperature increases, which is quite different from the total elongation along axial direction. Both the total elongation along hoop direction and the MER value increase to a peak value at about 160 ℃. After that, they begin to decrease quickly until a certain rebounding temperature is reached. From the rebounding temperature, they begin to increase rapidly again. Burnt structure appears on the fracture surface when tested at temperatures higher than 420 ℃. Therefore, the forming temperature of the tested tube should be lower than 420 ℃, even though bigger formability can be achieved at higher temperature.
基金Project(51575364)supported by the National Natural Science Foundation of ChinaProject(2013024014)supported by the Natural Foundation of Liaoning Province,China
文摘Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analysis and experiments of viscous warm pressure bulging (VWPB) of AZ31B magnesium alloy were conducted to analyze the influence of different ellipticity dies on the formability of AZ31B magnesium alloy. At the same time, based on the grid strain rule, the forming limit diagram (FLD) of VWPB of AZ31B magnesium alloy was obtained through measuring the strain of bulging specimens. The results showed that at the temperature range of viscous medium thermal stability, the viscous medium can fit the geometry variation of sheet and generate non-uniform pressure field, and as the die ellipticity increases, the difference value of non-uniform pressure reduces. Meanwhile, according to the FLD, the relationship between part complexity and ultimate deformation was investigated.
基金Project(HIT.NSRIF.2009033) supported by the Scientific Research Foundation of Harbin Institute of Technology,China
文摘The formability of AA5052/polyethylene/AA5052 sandwich sheets was experimentally studied. Three kinds of AA5052/polyethylene/AA5052 sandwich specimens with different thicknesses of core materials were prepared by the hot pressing adhesive method. Then, the uniaxial tensile tests were conducted to investigate the mechanical properties of AA5052/polyethylene/ AA5052 sandwich sheets, and the stretching tests were carried out to investigate the influences of polymer core thickness on the limit dome height of the sandwich sheet. The forming limit curves for three kinds of sandwich sheets were obtained. The experimental results show that the forming limit of the AA5052/polyethylene/AA5052 sandwich sheet is higher than that of the monolithic AA5052 sheet, and it increases with increasing the thickness of polyethylene core.
文摘Experimental study has been conducted for an interstitial free(IF) sheet steel on its surface roughness evolution and formability with respect to grain size and sheet thickness effect. The surface roughness of IF sheet steel is proportional to effective strain, grain size and inversely proportional to sheet thickness; the larger grain reduces the formability by accelerating the surface roughening rate and enhance formability by raising the workhardening rate, while the latter effect plays the dominate role. The grain size effect on surface roughening and formability is more obvious when the sheets are thinner.
基金Projects(51174121,51274125)supported by the National Natural Science Foundation of ChinaProject(2010R50016-30)supported by Zhejiang Province Science and Technology Innovation Team of Key Projects,ChinaProject supported by the K.C.Wong Magna Fund of Ningbo University,China
文摘The effectsof melt overheating degree on the undercooling degree and resultant solidification structures of Nd9Fe85-xTi4C2Bx(x=10, 12) glass-forming alloyswerestudied by differential thermal analysis combining with solidification structure analysis. The results indicate that the undercooling degree of Nd9Fe85-xTi4C2Bx(x=10, 12) alloys significantly increaseswith the rise of melt overheating degree, and two overheating degree thresholds corresponding to the drastic increase of the mean undercooling degree are found for each of the alloys. The existence of two turning points of the mean undercooling degreescan be linked to the structure transitions inside the overheated melts, which result in the evident increase of volume fraction of amorphous phasein the solidified structures.
基金Project(2009ZX04014-074)supported by the National Science and Technology Major Project of ChinaProject(P2014-15)supported by the State Key Laboratory of Materials Processing and Die&Mould Technology,Huazhong University of Science and Technology,ChinaProject(20120006110017)supported by the Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘The effect of friction coefficient on the deep drawing of aluminum alloy AA6111 at elevated temperatures was analyzed based on the three conditions using the finite element analysis and the experimental approach.Results indicate that the friction coefficient and lubrication position significantly influence the minimum thickness,the thickness deviation and the failure mode of the formed parts.During the hot forming process,the failure modes are draw mode,stretch mode and equi-biaxial stretch mode induced by different lubrication conditions.In terms of formability,the optimal value of friction coefficient determined in this work is 0.15.At the same time,the good agreement is performed between the experimental and simulated results.Fracture often occurs at the center of cup bottom or near the cup corner in a ductile mode or ductile-brittle mixed mode,respectively.
基金Project(XAEP-KIZ-KIB-1309-0063)supported by the Fundamental Research for General Armament Department,China
文摘The deformation behavior and mechanism of Ti2AlNb-based alloy were experimentally investigated at elevated temperatures. Firstly, the stress?strain relationships at different temperatures and strain rates were investigated via uniaxial tensile testing. Then, formability data, as determined by examining the deep drawing and bending abilities, were obtained through limiting draw ratio (LDR) and bending tests. Finally, metallographic experiments and fracture morphology investigations were conducted to examine the thermal deformation mechanism of the alloy. The results showed that as the temperature increased, the total elongation increased from 13.58% to 97.82% and the yield strength decreased from 788 to 80 MPa over the temperature range from 750 to 950 °C at a strain rate 0.001 s?1. When the temperature reached 950 °C, the strain rate was found to have a great influence on the deformation properties. The plastic formability of the sheet metal was significantly improved and a microstructuraltransformation of O toB2 andα2 occurred in this temperature region, revealing the deformation mechanism of its plasticity.
基金Project(2017zzts005) supported by the Fundamental Research Funds for the Central Universities of Central South University
文摘Mg-Li alloy,as a superlight metallic engineering material,shows great potential in the fields of aerospace and militarydue to its high specific strength,better formability,and excellent electromagnetic shielding performance.The research process ofMg-Li alloys is reviewed and three main problems are pointed out.Aimed at the poor corrosion resistance of Mg-Li alloys,thecorrosion behavior is mainly summarized.The surface treatment technologies,including electroplating,electroless plating,plasmaspraying,molten salt replacement,conversion coating,anodizing,micro-arc oxidation,organic coating,and organic-inorganic hybridcoating,are introduced in detail.Finally,the future development of corrosion and protection of Mg?Li alloys is discussed.
文摘Mg and its alloys have continued to attract interest for several structural and super-sensitive applications because of their light weight and good combination of engineering properties.However for some of these applications,high plastic deformability is required to achieve desired component shapes and configurations;unfortunately,Mg and its alloys have low formability.Scientifically,the plastic behaviour of Mg and its alloys ranks among the most complex and difficult to reconcile in metallic material systems.But basically,the HCP crystal structure coupled with low stacking fault energies(SFE)are largely linked to the poor ductility exhibited by Mg alloys.These innate material characteristics have regrettably limited wide spread applicability of Mg and its alloys.Several research efforts aimed at exploring processing strategies to make these alloys more amenable for high formability–mediated engineering use have been reported and still ongoing.This paper reviews the structural metallurgy of Mg alloys and its influence on mechanical behaviour,specifically,plasticity characteristics.It also concisely presents various processing routes(Alloying,Traditional Forming and Severe Plastic Deformation(SPD))which have been explored to enhance plastic deformability in Mg and its alloys.Grain refinement and homogenising of phases,reducing CRSS between slip modes,twinning suppression to activate non-basal slip,and weakening and randomisation of the basal texture were observed as the formability enhancing strategies explored in the reviewed processes.While identifying the limitations of these strategies,further areas to be explored for enhancing plasticity of Mg alloys are highlighted.
基金National Natural Science Foundation of China(51701033,51701035)Chongqing Municipal Education Commission(KJQN201901504,KJZD-K202001502)Chongqing Science and Technology Commission(cstc2018jcyjAX0022).
文摘The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were performed by pre-strain paths,i.e.,tension(6%)and compression(5%)perpendicular to the c-axis along extrusion direction(ED),to investigate the microstructural evolution and mechanical properties of AZ31 Mg alloy sheets.The distinction in the texture evolution and strain hardening behavior was illustrated in connection with the pre-strain paths for the activities of twinning and slip.The result shows that the activation of the deformation mode was closely bound up with the grain orientation and the additional applied load direction.The{10–12}twin-texture components with c-axis//ED were generated by precompression,which can provide an appropriate alternative to accommodate the thin sheet thickness strain and enhance the room temperature formability of Mg alloy sheet.