Titanium-aluminium-nitride(Ti_(1-x)Al_(x)N)coatings were deposited by close-field un balanced magnetron sputtering on M42 steel substrates and WC-6wt%Co inserts at 450℃.The tribological behavior was analyzed by slidi...Titanium-aluminium-nitride(Ti_(1-x)Al_(x)N)coatings were deposited by close-field un balanced magnetron sputtering on M42 steel substrates and WC-6wt%Co inserts at 450℃.The tribological behavior was analyzed by sliding against steel and WC-6wt%Co balls,while the turning performance was evaluated by a conventional tu rning machine at high cutting speeds without using coolants.In the tribological tests,the formation of transfer layer and the variations of hardness of the co atings played an important role for sliding against steel balls.For the coating s sliding against WC-6wt%Co balls,the Ti-Al-N coatings showed a similar frictio n coefficient,but the TiN coating exhibited a lower value.The difference could be explained by the tri-oxidation wear mechanism.In the turning tests,a super ior cutting performance of the coating was found at x=0.45,which endured 38 min utes before the tool flank wear reached the maximum value of 0.3mm,whereas only 20 minutes were endured for the TiN coating.The excellent performance of the c oatings in the turning tests could be explained by the enhanced mechanical prope rties and oxidation/diffusion resistance of the coatings.展开更多
To simulate the wear and corrosion behavior of high-strength EH47 hull steel in a complicated marine environment in which seawater,sea ice,and sea sand coexist,accelerated wear and corrosion tests were performed in a ...To simulate the wear and corrosion behavior of high-strength EH47 hull steel in a complicated marine environment in which seawater,sea ice,and sea sand coexist,accelerated wear and corrosion tests were performed in a laboratory setting using a tribometer.The effect of large loads on the behavior of abrasion and corrosion in a 3.5wt%NaCl solution with ice and sand to simulate a marine environment were investigated.The experimental results showed that the coefficient of friction(COF)decreases with increasing working load;meanwhile,the loading force and sand on the disk strongly influence the COF.The mechanisms of friction and the coupling effect of abrasion and corrosion in the 3.5wt%NaCl solution with sand were the wear and corrosion mechanisms;furthermore,the wear mechanism exerted the predominant effect.展开更多
Titanium has been increasingly applied to biomedical application because of its improved mechanical characteristics, corrosion resistance and biocompatibility. However their application remains limited, due to the low...Titanium has been increasingly applied to biomedical application because of its improved mechanical characteristics, corrosion resistance and biocompatibility. However their application remains limited, due to the low strength and poor wear resistance of unalloyed titanium. The purpose of this study is to evaluate the friction and wear behavior of high-strength titanium alloys: Ti-6Al-7Nb used in femoral stem (total hip prosthesis). The oscillating friction and wear tests have been carried out in ambient air with oscillating tribotester in accord with standards ISO 7148, ASTM G99-95a, ASTM G 133-95 under different conditions of normal applied load (3, 6 and 10 N) and sliding speed (1, 15 and 25 mm.s-1), and as a counter pair we used the ball of 100C 6, 10 mm of diameter. The surface morphology of the titanium alloys has been characterized by SEM, EDAX, micro hardness, roughness analysis measurements. The behavior observed for both samples suggests that the wear and friction mechanism during the test is the same for Ti alloys, and to increase resistance to wear and friction of biomedical titanium alloys used in total hip prosthesis (femoral stems) the surface coating and treatment are required.展开更多
弹带挤进膛线是一个复杂非线性的力学过程。膛线起始部磨损量是身管寿命评判的重要技术指标之一。为了真实地反映弹带挤进膛线过程中膛线起始部的磨损失效过程,以身管材料PCr Ni Mo钢制作销试样,以弹带材料96黄铜制作盘试样,基于MMS-1G...弹带挤进膛线是一个复杂非线性的力学过程。膛线起始部磨损量是身管寿命评判的重要技术指标之一。为了真实地反映弹带挤进膛线过程中膛线起始部的磨损失效过程,以身管材料PCr Ni Mo钢制作销试样,以弹带材料96黄铜制作盘试样,基于MMS-1G型销-盘式摩擦磨损试验机进行高温高速条件下的摩擦磨损试验,测定PCr Ni Mo钢/96黄铜摩擦副在高温、高速、干滑动条件下滑动速度和接触压力对摩擦系数和磨损率的影响。并应用扫描电子显微镜对摩擦表面进行观察,研究滑动速度和接触压力在销试样磨损失效过程中的影响过程。结果表明:滑动速度与接触压力对PCr Ni Mo钢的摩擦磨损性能有类似的影响规律,但影响程度不同,都存在敏感变化范围。展开更多
This study aims to examine the effect of replacing vanadium by niobium and iron on the tribological behavior of hot-isostatic-pressed titanium alloy （Ti-6Al-4V） biomaterial, using a ball-on-disk-type oscillating tri...This study aims to examine the effect of replacing vanadium by niobium and iron on the tribological behavior of hot-isostatic-pressed titanium alloy （Ti-6Al-4V） biomaterial, using a ball-on-disk-type oscillating tribometer, under wet conditions using physiological solution in accordance with the ISO7148 standards. The tests were carried out under a normal load of 6 N, with an AISI 52100 grade steel ball as a counter face. The morphological changes and structural evolution of the nanoparticle powders using different milling times （2, 6, 12 and 18 h） were studied. The morphological characterization indicated that the particle and crystallite size continuously decrease with increasing milling time to reach the lowest value of 4 nm at 18-h milling. The friction coefficient and wear rate were lower in the samples milled at 18 h （0.226, 0.297 and 0.423; and 0.66 × 10-2, 0.87 × 10-2 and 1.51 × 10-2 μm3 N-1 i, tm-1） for Ti-6Al-4Fe, Ti-6A1-7Nb and Ti-6Al-4V, respectively. This improvement in friction and wear resistance is attributed to the grain refinement at 18-h milling. The Ti-6Al-4Fe samples showed good tribological performance for all milling times.展开更多
基金The authors wish 10 thank the use of the facilities in ACARL which is suppored by the Innovation Technology Fund of Hong KongPWS acknowledges the support of the research scholarship from the City University of Hong Kong and ME thanks the financial support by a grant awarded by the Research Grant Council of the Hong Kong Special Administrative Region,China(No.CityU 1180/01E)
文摘Titanium-aluminium-nitride(Ti_(1-x)Al_(x)N)coatings were deposited by close-field un balanced magnetron sputtering on M42 steel substrates and WC-6wt%Co inserts at 450℃.The tribological behavior was analyzed by sliding against steel and WC-6wt%Co balls,while the turning performance was evaluated by a conventional tu rning machine at high cutting speeds without using coolants.In the tribological tests,the formation of transfer layer and the variations of hardness of the co atings played an important role for sliding against steel balls.For the coating s sliding against WC-6wt%Co balls,the Ti-Al-N coatings showed a similar frictio n coefficient,but the TiN coating exhibited a lower value.The difference could be explained by the tri-oxidation wear mechanism.In the turning tests,a super ior cutting performance of the coating was found at x=0.45,which endured 38 min utes before the tool flank wear reached the maximum value of 0.3mm,whereas only 20 minutes were endured for the TiN coating.The excellent performance of the c oatings in the turning tests could be explained by the enhanced mechanical prope rties and oxidation/diffusion resistance of the coatings.
基金This work was financially supported by the National Natural Science Foundation of China(Nos.51474127 and 51671100)the State Key Laboratory of Metal Material for Marine Equipment and Application-University of Science and Technology Liaoning co-project,China(Nos.SKLMEA-USTL 2017010 and 201905).
文摘To simulate the wear and corrosion behavior of high-strength EH47 hull steel in a complicated marine environment in which seawater,sea ice,and sea sand coexist,accelerated wear and corrosion tests were performed in a laboratory setting using a tribometer.The effect of large loads on the behavior of abrasion and corrosion in a 3.5wt%NaCl solution with ice and sand to simulate a marine environment were investigated.The experimental results showed that the coefficient of friction(COF)decreases with increasing working load;meanwhile,the loading force and sand on the disk strongly influence the COF.The mechanisms of friction and the coupling effect of abrasion and corrosion in the 3.5wt%NaCl solution with sand were the wear and corrosion mechanisms;furthermore,the wear mechanism exerted the predominant effect.
文摘Titanium has been increasingly applied to biomedical application because of its improved mechanical characteristics, corrosion resistance and biocompatibility. However their application remains limited, due to the low strength and poor wear resistance of unalloyed titanium. The purpose of this study is to evaluate the friction and wear behavior of high-strength titanium alloys: Ti-6Al-7Nb used in femoral stem (total hip prosthesis). The oscillating friction and wear tests have been carried out in ambient air with oscillating tribotester in accord with standards ISO 7148, ASTM G99-95a, ASTM G 133-95 under different conditions of normal applied load (3, 6 and 10 N) and sliding speed (1, 15 and 25 mm.s-1), and as a counter pair we used the ball of 100C 6, 10 mm of diameter. The surface morphology of the titanium alloys has been characterized by SEM, EDAX, micro hardness, roughness analysis measurements. The behavior observed for both samples suggests that the wear and friction mechanism during the test is the same for Ti alloys, and to increase resistance to wear and friction of biomedical titanium alloys used in total hip prosthesis (femoral stems) the surface coating and treatment are required.
文摘弹带挤进膛线是一个复杂非线性的力学过程。膛线起始部磨损量是身管寿命评判的重要技术指标之一。为了真实地反映弹带挤进膛线过程中膛线起始部的磨损失效过程,以身管材料PCr Ni Mo钢制作销试样,以弹带材料96黄铜制作盘试样,基于MMS-1G型销-盘式摩擦磨损试验机进行高温高速条件下的摩擦磨损试验,测定PCr Ni Mo钢/96黄铜摩擦副在高温、高速、干滑动条件下滑动速度和接触压力对摩擦系数和磨损率的影响。并应用扫描电子显微镜对摩擦表面进行观察,研究滑动速度和接触压力在销试样磨损失效过程中的影响过程。结果表明:滑动速度与接触压力对PCr Ni Mo钢的摩擦磨损性能有类似的影响规律,但影响程度不同,都存在敏感变化范围。
文摘This study aims to examine the effect of replacing vanadium by niobium and iron on the tribological behavior of hot-isostatic-pressed titanium alloy （Ti-6Al-4V） biomaterial, using a ball-on-disk-type oscillating tribometer, under wet conditions using physiological solution in accordance with the ISO7148 standards. The tests were carried out under a normal load of 6 N, with an AISI 52100 grade steel ball as a counter face. The morphological changes and structural evolution of the nanoparticle powders using different milling times （2, 6, 12 and 18 h） were studied. The morphological characterization indicated that the particle and crystallite size continuously decrease with increasing milling time to reach the lowest value of 4 nm at 18-h milling. The friction coefficient and wear rate were lower in the samples milled at 18 h （0.226, 0.297 and 0.423; and 0.66 × 10-2, 0.87 × 10-2 and 1.51 × 10-2 μm3 N-1 i, tm-1） for Ti-6Al-4Fe, Ti-6A1-7Nb and Ti-6Al-4V, respectively. This improvement in friction and wear resistance is attributed to the grain refinement at 18-h milling. The Ti-6Al-4Fe samples showed good tribological performance for all milling times.
