Experimental Study of Heat Transfer in an Insulated Local Heated fromBelow and Comparison with Simulation by Lattice Boltzmann Method

In this paper,experimental and numerical studies of heat transfer in a test local of side H=0.8 m heated from below are presented and compared.All the walls,the rest of the floor and the ceiling are made from plywood and polystyrene in sandwich form(3 mmplywood-3 cm polystyrene-3 mmplywood)just on one of the vertical walls contained a glazed door(2 H/3×0.15 m).This local is heated during two heating cycles by a square plate of iron the width L=0.6 H,which represents the heat source,its temperature Th is controlled.The plate is heated for two cycles by an adjustable set-point heat source placed just down the center of it.For each cycle,the heat source is switched“on”for 6 h and switched“off”for 6 h.The outdoor air temperature is kept constant at a low temperature Tc<Th.All measurements are carried out with k-type thermocouples and with flux meters.Results will be qualitatively presented for two cycles of heating in terms of temperatures and heat flux densitiesϕfor various positions of the test local.The temperature evolution of the center and the profile of the temperature along the vertical centerline are compared by two dimensions simulation using the lattice Boltzmann method.The comparison shows a good agreement with a difference that does not exceed±1℃.

A Mixed-Variable Experimental Design Method

Mixed-variable problems are inevitable in engineering. However, few researches pay attention to discrete variables. This paper proposed a mixed-variable experimental design method (ODCD): first, the design variables were divided into discrete variables and continuous variables;then, the DVD method was employed for handling discrete variables, the LHD method was applied for continuous variables, and finally, a Columnwise-Pairwise Algorithm was used for the overall optimization of the design matrix. Experimental results demonstrated that the ODCD method outperforms in terms of the sample space coverage performance.

Potato farmers’ preference for agricultural insurance in China: An investigation using the choice experimental method

Potato insurance plays an important role in transferring agricultural risks to promote the potato staple strategy. Understanding farmers’ real preferences for potato insurance attributes is important to improve the potato insurance. In this study, a choice experiment was designed with attributes such as peril, minimum compensation ratio for production loss, types of crops covered by insurance, annual premium per mu after subsidy, and complexity of claims procedures. We constructed a mixed logit model based on a questionnaire survey of 362 potato farmers’ choices of insurance attributes from 24 villages in Dingxi City of Gansu Province using random sampling. The results show that:(1) farmers prefer agricultural insurance with widely perils including output price drop and input cost risk;(2) farmers who have suffered plant disease and insect and pest damage are willing to pay a high premium for the insurance with a high compensation ratio and several types of crops covered;full-time farmers and large-scale farmers preferred insurance products with low complexity of claims procedures. Therefore, new potato insurance design could be considered specifically for different farmer groups such as those who had previous disaster experiences, and large-or small-scale farm operations.

Partition method and experimental validation for impact dynamics of flexible multibody system

The impact problem of a flexible multibody system is a non-smooth, high-transient, and strong-nonlinear dynamic process with variable boundary. How to model the contact/impact process accurately and efficiently is one of the main difficulties in many engineering applications. The numerical approaches being used widely in impact analysis are mainly from two fields： multibody system dynamics （MBS） and computational solid mechanics （CSM）. Approaches based on MBS provide a more efficient yet less accurate analysis of the contact/impact problems, while approaches based on CSM are well suited for particularly high accuracy needs, yet require very high computational effort. To bridge the gap between accuracy and efficiency in the dynamic simulation of a flexible multibody system with contacts/impacts, a partition method is presented considering that the contact body is divided into two parts, an impact region and a non-impact region. The impact region is modeled using the finite element method to guarantee the local accuracy, while the non-impact region is modeled using the modal reduction approach to raise the global efficiency. A three-dimensional rod-plate impact experiment is designed and performed to validate the numerical results. The principle for how to partition the contact bodies is proposed： the maximum radius of the impact region can be estimated by an analytical method, and the modal truncation orders of the non-impact region can be estimated by the highest frequency of the signal measured. The simulation results using the presented method are in good agreement with the experimental results. It shows that this method is an effec-rive formulation considering both accuracy and efficiency. Moreover, a more complicated multibody impact problem of a crank slider mechanism is investigated to strengthen this conclusion.

Application of orthogonal experimental design and Tikhonov regularization method for the identification of parameters in the casting solidification process

The inverse heat conduction method is one of methods to identify the casting simulation parameters. A new inverse method was presented according to the Tikhonov regularization theory. One appropriate regularized functional was established, and the functional was solved by the sensitivity coefficient and Newtonaphson iteration method. Moreover, the orthogonal experimental design was used to estimate the appropriate initial value and variation domain of each variable to decrease the number of iteration and improve the identification accuracy and efficiency. It illustrated a detailed case of AlSiTMg sand mold casting and the temperature measurement experiment was done. The physical properties of sand mold and the interracial heat transfer coefficient were identified at the meantime. The results indicated that the new regularization method was efficient in overcoming the ill-posedness of the inverse heat conduction problem and improving the stability and accuracy of the solutions.

Dynamic Modeling and Experimental Verification of an RPR Type Compliant Paralle Mechanism with Low Orders

Efficiency of calculating a dynamic response is an important point of the compliant mechanism for posture adjustment.Dynamic modeling with low orders of a 2R1T compliant parallel mechanism is studied in the paper.The mechanism with two out-of-plane rotational and one lifting degrees of freedom(DoFs)plays an important role in posture adjustment.Based on elastic beam theory,the stiffness matrix and mass matrix of the beam element are established where the moment of inertia is considered.To improve solving efficiency,a dynamic model with low orders of the mechanism is established based on a modified modal synthesis method.Firstly,each branch of the RPR type mechanism is divided into a substructure.Subsequently,a set of hypothetical modes of each substructure is obtained based on the C-B method.Finally,dynamic equation of the whole mechanism is established by the substructure assembly.A dynamic experiment is conducted to verify the dynamic characteristics of the compliant mechanism.

Potential-dependent insights into the origin of high ammonia yield rate on copper surface via nitrate reduction:A computational and experimental study

Focusing on revealing the origin of high ammonia yield rate on Cu via nitrate reduction(NO3RR),we herein applied constant potential method via grand-canonical density functional theory(GC-DFT)with implicit continuum solvation model to predict the reaction energetics of NO3RR on pure copper surface in alkaline media.The potential-dependent mechanism on the most prevailing Cu(111)and the minor(100)and(110)facets were established,in consideration of NO_(2)_(−),NO,NH_(3),NH_(2)OH,N_(2),and N_(2)O as the main products.The computational results show that the major Cu(111)is the ideal surface to produce ammonia with the highest onset potential at 0.06 V(until−0.37 V)and the highest optimal potential at−0.31 V for ammonia production without kinetic obstacles in activation energies at critical steps.For other minor facets,the secondary Cu(100)shows activity to ammonia from−0.03 to−0.54 V with the ideal potential at−0.50 V,which requires larger overpotential to overcome kinetic activation energy barriers.The least Cu(110)possesses the longest potential range for ammonia yield from−0.27 to−1.12 V due to the higher adsorption coverage of nitrate,but also with higher tendency to generate di-nitrogen species.Experimental evaluations on commercial Cu/C electrocatalyst validated the accuracy of our proposed mechanism.The most influential(111)surface with highest percentage in electrocatalyst determined the trend of ammonia production.In specific,the onset potential of ammonia production at 0.1 V and emergence of yield rate peak at−0.3 V in experiments precisely located in the predicted potentials on Cu(111).Four critical factors for the high ammonia yield and selectivity on Cu surface via NO3RR are summarized,including high NO3RR activity towards ammonia on the dominant Cu(111)facet,more possibilities to produce ammonia along different pathways on each facet,excellent ability for HER inhibition and suitable surface size to suppress di-nitrogen species formation at high nitrate coverage.Overall,our work provides comprehensive potential-dependent insights into the reaction details of NO3RR to ammonia,which can serve as references for the future development of NO3RR electrocatalysts,achieving higher activity and selectivity by maximizing these characteristics of copper-based materials.

Experimental Characterization of Rutting Performance of HMA Designed with Aggregate Gradations According to Superpave and Marshall Methods

The permanent deformation (rutting) of pavement is a major distress in flexible pavement. It is related to vehicles properties and/or pavement materials and conditions. This article presents an extensive experimental investigation in order to compare between the aggregate gradation according to Superpave and Marshall methods of asphalt concrete mix design on pavement rutting and to examine the sensitivity of rutting resistance to aggregate gradation. A wheel truck machine has been used for measurement of pavement rutting (permanent deformation). The tests were carried out at two controlled different air temperature 55℃ and 25℃. The results obtained showed that the adopting of aggregate gradation procedure of Superpave method of pavement mix design for Marshall method of asphalt concrete mix design can reduce the pavement rutting by about 50%. This achievement may be related to missing of three sieves in aggregate gradation procedure of Marshall method which controls rounded and finer aggregate particles. These sieves provide more continuity for aggregate gradation to ensure filling unnecessary gaps and produce more contact points between the aggregates in Hot Mix Asphalt (HMA). The outputs of the research support modifying Marshall method of asphalt concrete mix design by adopting aggregate gradation proposed in Superpave method. The results of study also showed that the coarser aggregate provided more resistance to pavement rutting.

An Experimental Method to Read Novels Without Literary Criticism

Though novel reading is a common experience to everybody,little has been researched to help average readers to understand a novel.In practice,there are two ways for them to understand a novel:one is to use literary criticism theories and the other is to refer to professional critics'criticism directly.However,the trouble is that the two methods are either time-consuming or far from convincing.In this paper,an experimental reading method is discussed to help average readers enhance reading experience.It aims at reaching the goal of reading without criticism,which,through making clear the aim of reading,putting main focus on the story only,will help readers to have a better understanding of reading.

Systematical approach in evaluation of LC method for determination of raloxifene hydrochloride and its impurities employing experimental design

Method validation presents a detailed investigation of analytical method and provision of the evidence that the method, when correctly applied, produces results that fit to the purpose. In order to achieve the method validation scope efficiently, experimental design presents a very useful tool. The greatest benefits of such approach could be seen in robustness testing through the provision of very useful data about the control of the chromatograp6hic system during the routine application. In this paper, robustness testing of the LC method proposed for the determination of raloxifene hydrochloride and its four impurities was done employing Plackett-Burman design. Applying this design, the effect of five real factors （acetonitrile content, sodium dodecyl sulfate content, column temperature, pH of the mobile phase and flow rate） on the corresponding resolution factors was investigated through twelve experiments. Furthermore, the insignificance intervals for significant factors were calculated and the parameters for system suitability tests were defined. Eventually, the other validation parameters were tested and the effectiveness of the proposed analytical method with a high degree of accuracy was confirmed.

Experimental validation method of elastic thin rod model for simulating the motional cable harness

To analyze the spring disturbance torque caused by motionai cable harness in a stabilized platform, the Kirchhoff theory based cable harness model has been previously developed to dynamically simulate the motional cable harness. In this paper, this model was validated by comparing the simulation results with the experiment results （ both the spring force and the deformed profile of the motional cable harness）. In the experiment, a special optical measuring instrument based on binocular vision was developed and the motion and deformation of cable harness were measured. A simpli- fied stabilized platform system was constructed, and the absolute value of spring disturbance force during the motion of this simplified frame was obtained by using a force gauge （0. 02 N precision）. The physical parameters of experimental specimen were also measured. The experimental and simulated results showed good agreement. These results should be useful for better motional cable harness layout design and reliable evaluation of the spring disturbance torque.

Numerical-experimental method for elastic parameters identification of a composite panel

A hybrid numerical-experimental approach to identify elastic modulus of a textile composite panel using vibration test data is proposed and investi- gated. Homogenization method is adopted to predict the initial values of elastic parameters of the composite, and parameter identification is transformed to an optimization problem in which the objective function is the minimization of the discrepancies between the experimental and numerical modal data. Case study is conducted employing a woven fabric reinforced composite panel. Three parameters （Ell, E22, G12） with higher sensitivities are selected to be identified. It is shown that the elastic parameters can be accurately identified from experimental modal data.

EFFECTS OF REACTION AND PROCESSING PARAMETERS ON ETHYLENE POLYMERIZATION USING DIFFERENT ZIEGLER-NATTA CATALYSTS:EMPLOYMENT OF TAGUCHI EXPERIMENTAL DESIGN AND RESPONSE SURFACE METHOD

Different Ziegler-Natta catalysts were employed to polymerize ethylene. To investigate the influences of reaction parameters, namely Al/Ti molar ratio, hydrogen and processing parameters, i.e. ethylene pressure and temperature, a Taguchi experimental design was worked out. An L27 orthogonal array was chosen to take the above-mentioned parameters and relevant interactions into account. Response surface method was the tool used to analyze the experimental design results. Al/Ti, ethylene pressure and temperature were selected as experimental design factors, and catalyst activity and polymerization yield were the response parameters. Increasing pressure, due to an increment in monomer accessibility, and rising Al/Ti, because of higher reduction in the catalysts, cause an increase in both polymerization yield and catalyst activity. Nonetheless, a higher temperature, thanks to reducing ethylene solubility in the slurry medium and partially catalyst destruction, lead to a reduction in both response parameters. A synergistic effect was also observed between temperature and pressure. All catalyst activities will reduce in the presence of hydrogen. Molecular weight also shows a decline in the presence of hydrogen as a transfer agent. However, the polydispersity index remains approximately intact. Using SEM, various morphologies, owing to different catalyst morphologies, were seen for the polyethylene.

New HPLC Method with Experimental Design and Fluorescence Detection for Analytical Study of Antihypertensive Mixture,Amlodipine and Valsartan

New HPLC method was developed for determination of amlodipine and valsartan in their binary mixture as a part of routine control of combined formulations. The method was validated to meet official requirements including selectivity, stability, linearity, precision and accuracy. Chromatography was carried out using a LiChrospher RP-18 column, a mixture containing acetonitrile, phosphate buffer of pH 3.5 and methanol (45:45:10, v/v/v) and new fluorescence detection at 255 nm for excitation and 448 nm for emission. The effect of methanol content, pH of the buffer, flow rate, detection wavelengths and column temperature was estimated in robustness study, according to a plan defined by the Plackett-Burman design. For identification of significant effects, both graphical and statistical methods were used. Ro-bustness for dissolution test was checked estimating the effects of paddle speed, temperature and pH of dissolution medium. The method was proved to complying with all official guidelines. Therefore, it is suitable for determination of amlodipine and valsartan in their binary mixtures for different analytical and pharmaceutical purposes.

Experimental analysis of interface contact behavior using a novel image processing method

The spatial and temporal evolution of real contact area of contact interface with loads is a challenge.It is generally believed that there is a positive linear correlation between real contact area and normal load.However,with the development of measuring instruments and methods,some scholars have found that the growth rate of real contact area will slow down with the increase of normal load under certain conditions,such as large-scale interface contact with small roughness surface,which is called the nonlinear phenomenon of real contact area.At present,there is no unified conclusion on the explanation of this phenomenon.We set up an experimental apparatus based on the total reflection principle to verify this phenomenon and analyze its mechanism.An image processing method is proposed,which can be used to quantitative analysis micro contact behaviors on macro contact phenomenon.The weighted superposition method is used to identify micro contact spots,to calculate the real contact area,and the color superimposed image is used to identify micro contact behaviors.Based on this method,the spatiotemporal evolution mechanism of real contact area nonlinear phenomena is quantitatively analyzed.Furthermore,the influence of nonlinear phenomenon of real contact area on the whole loading and unloading process is analyzed experimentally.It is found that the effects of fluid between contact interface,normal load amplitude and initial contact state on contact behavior cannot be ignored in large-scale interface contact with small roughness surface.

Experimental Plans Method to Formulate a Resin Concrete

This work is an experimental approach based on the method of experimental plans to determine a specific formulation of a resin concrete. In this study, an unsaturated polyester resin （thermosetting resin） was used with two types of mineral fillers （dune sand and crushed sand）, and with the addition of a marble powder to ensure the continuity of the particle size mixing granular. The lack of the methods for developing this kind of composite materials, had led us to perform an initial experimental approach to define the experimental field, that is to say determine the mass proportions of the various compounds of mixture of our study. In the second approach, we have established and implemented fully experimental plans with three factors namely： factor （1）： sand, factor （2）： resin, factor （3）： marble powder. Test results being the density of polymer concrete and the mechanical resistances. Finally, multi-parameters regression allowed us to determine predictive mathematical models for the different responses of the study. Tests results showed that at three days we got a tensile strength of about 16 MPa with a resin concrete density of 1.9 g/cm3. This shows the advantages of this material.

Evaluation of Full Experimental Design Method against Fractional Design Method and Taguchi Design Method in Machining Operation

DOE （design of experiments） is a systematic, rigorous approach to engineering problem-solving that applies principles and techniques at the data collection stage so as to ensure the generation of valid, defensible, and supportable engineering conclusions. This paper presents a comparison of three different experimental designs （full experimental design, fractional design and Taguchi design） aimed at studying the effects of cutting parameters variations on surface finish. The results revealed that the effects obtained by analyzing both fractional and Taguchi designs were comparable to the main effects and two-level interactions obtained by the full factorial design. Thus, we conclude that full factorial design appear to be reliable and more economical since they permit to reduce by a factor the amount of time and effort required to conduct the experimental design without losing valuable information. Thus, we conclude that full factorial design appear to be reliable and more economical and without losing valuable information.

RECONSTRUCTION OF PART OF AN ACTUAL BLAST-WAVE FLOW FIELD TO AGREE WITH EXPERIMENTAL DATA BY USING NUMERICAL METHOD WITH HIGH IDENTIFICATION

In this paper, on the basis of experimental data of two kinds of chemical explosions, the piston-pushing model of spherical blast-waves and the second-order Godunov-type scheme of finite difference methods with high identification to discontinuity are used to the numerical reconstruction of part of an actual hemispherical blast-wave flow field by properly adjusting the moving bounary conditions of a piston. This method is simple and reliable. It is suitable to the evaluation of effects of the blast-wave flow field away from the explosion center.

Visual Passive Ranging Method Based on Re-entrant Coaxial Optical Path and Experimental Verification

To overcome the shortcomings of the traditional passive ranging technology based on image, such as poor ranging accuracy, low reliability and complex system, a new visual passive ranging method based on re-entrant coaxial optical path is presented. The target image is obtained using double cameras with coaxial optical path. Since there is imaging optical path difference between the cameras, the images are different. In comparison of the image differences, the target range could be reversed. The principle of the ranging method and the ranging model are described. The relationship among parameters in the ranging process is analyzed quantitatively. Meanwhile,the system composition and technical realization scheme are also presented. Also, the principle of the method is verified by the equivalent experiment. The experimental results show that the design scheme is correct and feasible with good robustness. Generally, the ranging error is less than 10% with good convergence. The optical path is designed in a re-entrant mode to reduce the volume and weight of the system. Through the coaxial design,the visual passive range of the targets with any posture can be obtained in real time. The system can be widely used in electro-optical countermeasure and concealed photoelectric detection.

A METHOD OF ESTIMATING THE INFLUENCE OF EXPERIMENTAL ERRORS ON THE EXPERIMENTAL RESULTS OF MATERIAL PARAMETERS AND THE CRITERIA TO VALUE THIS INFLUENCE

In this paper the main sources causing the scatter of the experimental results of the material parameters are discussed. They can be divided into two parts: one is the experimental errors which are introduced because of the inaccuracy of experimental equipment, the experimental techniques, etc., and the form of the scatter caused by this source is called external distribution. The other is due to the irregularity and inhomogeneity of the material structure and the randomness of deformation process. The scatter caused by this source is inherent and then this form of the scatter is called internal distribution. Obviously the experimental distribution of material parameters combines these two distributions in some way; therefore, it is a sum distribution of the external distribution and the internal distribution. In view of this , a general method used to analyse the influence of the experimental errors on the experimental results is presented, and three criteria used to value this influence are defined. An example in which the fracture toughness KIC is analysed shows that this method is reasonable, convenient and effective.