Residual stress modeling of mitigated fused silica damage sites with CO_(2)laser annealing

A numerical model based on measured fictive temperature distributions is explored to evaluate the residual stress fields of CO_(2)laser-annealed mitigated fused silica damage sites.The proposed model extracts the residual strain from the differences in thermoelastic contraction of fused silica with different fictive temperatures from the initial frozen-in temperatures to ambient temperature.The residual stress fields of mitigated damage sites for the CO_(2)laser-annealed case are obtained by a finite element analysis of equilibrium equations and constitutive equations.The simulated results indicate that the proposed model can accurately evaluate the residual stress fields of laser-annealed mitigated damage sites with a complex thermal history.The calculated maximum hoop stress is in good agreement with the reported experimental result.The estimated optical retardance profiles from the calculated radial and hoop stress fields are consistent with the photoelastic measurements.These results provide sufficient evidence to demonstrate the suitability of the proposed model for describing the residual stresses of mitigated fused silica damage sites after CO_(2)laser annealing.

Alkylene-functionality in bridged and fused nitrogen-rich poly-cyclic energetic materials:Synthesis,structural diversity and energetic properties

From the standpoint of chemical structures,the organic backbones of energetic materials can be classified into aromatic rings,nonaromatic rings,and open chains.Although the category of aromatic energetic compounds exhibits several advantages in the regulation of energetic properties,the nonaromatic heterocycles,assembling nitramino explosophores with simple alkyl bridges,still have prevailed in benchmark materials.The methylene bridge plays a pivotal role in the constructions of the classic nonaromatic heterocycle-based energetic compounds,e.g.,hexahydro-1,3,5-trinitro-1,3,5-triazine(RDX)and octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine(HMX),whereas ethylene bridge is the core moiety of state-of-the-art explosive 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane(CL-20).In this context,it is of great interest to employ simple and practical bridges to assemble aromatic and nonaromatic nitrogen-rich heterocycles,thereby expanding the structural diversity of energetic materials,e.g.,bridged and fused nitrogen-rich poly-heterocycles.Furthermore,alkyl-bridged poly-heterocycles highlight the potential for the open chain type of energetic materials.In this review,the development of alkyl bridges in linking nitrogen-rich heterocycles is presented,and the perspective of the newly constructed energetic backbones is summarized for the future design of advanced energetic materials.

Research on aiming methods for small sample size shooting tests of two-dimensional trajectory correction fuse

The longitudinal dispersion of the projectile in shooting tests of two-dimensional trajectory corrections fused with fixed canards is extremely large that it sometimes exceeds the correction ability of the correction fuse actuator.The impact point easily deviates from the target,and thus the correction result cannot be readily evaluated.However,the cost of shooting tests is considerably high to conduct many tests for data collection.To address this issue,this study proposes an aiming method for shooting tests based on small sample size.The proposed method uses the Bootstrap method to expand the test data;repeatedly iterates and corrects the position of the simulated theoretical impact points through an improved compatibility test method;and dynamically adjusts the weight of the prior distribution of simulation results based on Kullback-Leibler divergence,which to some extent avoids the real data being"submerged"by the simulation data and achieves the fusion Bayesian estimation of the dispersion center.The experimental results show that when the simulation accuracy is sufficiently high,the proposed method yields a smaller mean-square deviation in estimating the dispersion center and higher shooting accuracy than those of the three comparison methods,which is more conducive to reflecting the effect of the control algorithm and facilitating test personnel to iterate their proposed structures and algorithms.;in addition,this study provides a knowledge base for further comprehensive studies in the future.

eFuse器件的电迁移三维有限元仿真

应用有限元分析软件建立了电可编程熔丝(eFuse)器件的三维有限元模型,通过离子流通量散度法和最小原子浓度法对eFuse器件的电迁移熔断过程进行了多物理场耦合有限元仿真,仿真结果能够较好地拟合器件的实际熔断效果。通过仿真对比了不同阴极面积和不同编程电压条件下的电迁移过程及熔断效果。结果表明,更大的阴极面积能够提高熔丝局部的温度梯度,从而提高熔断效率;更高的编程电压能够提供更高的电流密度和温度,从而加速电迁移的发生并增大了eFuse熔断区的面积。提出了一种具有外部辅助加热功能的eFuse器件结构,并在不同条件下进行了电迁移熔断仿真,结果表明该结构能够显著提高eFuse器件局部的离子流通量散度,从而提高eFuse存储单元的熔断效率和编程良率。

Multi-Objective Optimization of Fused Deposition Modeling for Mechanical Properties of Biopolymer Parts Using the Grey-Taguchi Method

The urgent need to develop customized functional products only possible by 3D printing had realized when faced with the unavailability of medical devices like surgical instruments during the coronavirus-19 disease and the ondemand necessity to perform surgery during space missions.Biopolymers have recently been the most appropriate option for fabricating surgical instruments via 3D printing in terms of cheaper and faster processing.Among all 3D printing techniques,fused deposition modelling(FDM)is a low-cost and more rapid printing technique.This article proposes the fabrication of surgical instruments,namely,forceps and hemostat using the fused deposition modeling(FDM)process.Excellent mechanical properties are the only indicator to judge the quality of the functional parts.The mechanical properties of FDM-processed parts depend on various process parameters.These parameters are layer height,infill pattern,top/bottom pattern,number of top/bottom layers,infill density,flow,number of shells,printing temperature,build plate temperature,printing speed,and fan speed.Tensile strength and modulus of elasticity are chosen as evaluation indexes to ascertain the mechanical properties of polylactic acid(PLA)parts printed by FDM.The experiments have performed through Taguchi’s L27orthogonal array(OA).Variance analysis(ANOVA)ascertains the significance of the process parameters and their percent contributions to the evaluation indexes.Finally,as a multiobjective optimization technique,grey relational analysis(GRA)obtains an optimal set of FDM process parameters to fabricate the best parts with comprehensive mechanical properties.Scanning electron microscopy(SEM)examines the types of defects and strong bonding between rasters.The proposed research ensures the successful fabrication of functional surgical tools with substantial ultimate tensile strength(42.6 MPa)and modulus of elasticity(3274 MPa).

A novel energetic framework with the combination of 5,6-fused triazolo-triazine and nitropyrazole-tetrazole for energy-stability balanced explosive

In recent years,the introduction of fused rings own high density and low sensitivity has promoted the development of energetic materials.However,the development of energetic compounds containing fused and bridged rings by introducing multiple nitrogen heterocycles at different sites of fused rings is still difficult to progress,which seriously limits the emergence of advanced energetic compounds.In this study,a series of energetic materials choosing different nitrogen rich heterocycles at the vacancies of the fused ring,i.e.,neutral compound 5,6 and their ionic derivatives(compounds 7-12)were designed and synthesized.Compounds 5 and 6 were further confirmed by single crystal X-ray diffraction,while the crystal analysis and theoretical calculations were carried out to explore the relationship between crystal structure and physicochemical properties.All of the newly synthesized compounds(5-12)are insensitive to mechanical stimulation(IS>40 J;FS≥342 N)and they own the high detonation velocity(D:8322-9075 m/s).Notably,hydrazine salt 11 own the higher detonation velocity(9075 m/s)and powder density(1.83 g/cm^(3)),but exhibits lower sensitivity(IS>40 J)than the classical energetic compound RDX(8795 m/s,1.80 g/cm^(3),7.5 J).It is obvious that the combination of 5,6-fused triazolo-triazine and nitropyrazole-tetrazole may be a new energetic skeleton for synthesising the heterocyclic compounds with balanced energy-stability.

Numerical simulation and printability analysis of fused deposition modeling with dual-temperature control

Ideal tissue engineering scaffolds need interconnected pores and high porosity to enable cell survival,migration,proliferation,and differentiation.However,obtaining a high-resolution structure is difficult with traditional one-temperature control fused deposition modeling(FDM).In this study,we propose a dual-temperature control method to improve printability.A numerical model is developed in which the viscosity is a function of temperature and shear rate to study the influence of two different temperature control modes.Quantitative tests are used to assess filament formation and shape fidelity,including one-dimensional filament printing,deposition at corners,fusion,and collapse.By using dual-temperature control,the width of the deposited poly(ε-caprolactone)filament is reduced to 50μm.The comparative results of both the experimental method and numerical simulation suggest that the dual-temperature control FDM can manufacture spatially arranged constructs and presents a promising application in tissue engineering。

A Hybrid Deep Fused Learning Approach to Segregate Infectious Diseases

Humankind is facing another deadliest pandemic of all times in history,caused by COVID-19.Apart from this challenging pandemic,World Health Organization(WHO)considers tuberculosis(TB)as a preeminent infectious disease due to its high infection rate.Generally,both TB and COVID-19 severely affect the lungs,thus hardening the job of medical practitioners who can often misidentify these diseases in the current situation.Therefore,the time of need calls for an immediate and meticulous automatic diagnostic tool that can accurately discriminate both diseases.As one of the preliminary smart health systems that examine three clinical states(COVID-19,TB,and normal cases),this study proposes an amalgam of image filtering,data-augmentation technique,transfer learning-based approach,and advanced deep-learning classifiers to effectively segregate these diseases.It first employed a generative adversarial network(GAN)and Crimmins speckle removal filter on X-ray images to overcome the issue of limited data and noise.Each pre-processed image is then converted into red,green,and blue(RGB)and Commission Internationale de l’Elcairage(CIE)color spaces from which deep fused features are formed by extracting relevant features using DenseNet121 and ResNet50.Each feature extractor extracts 1000 most useful features which are then fused and finally fed to two variants of recurrent neural network(RNN)classifiers for precise discrimination of threeclinical states.Comparative analysis showed that the proposed Bi-directional long-short-term-memory(Bi-LSTM)model dominated the long-short-termmemory(LSTM)network by attaining an overall accuracy of 98.22%for the three-class classification task,whereas LSTM hardly achieved 94.22%accuracy on the test dataset.

Modelling a Fused Deep Network Model for Pneumonia Prediction

Deep Learning(DL)is known for its golden standard computing paradigm in the learning community.However,it turns out to be an extensively utilized computing approach in the ML field.Therefore,attaining superior outcomes over cognitive tasks based on human performance.The primary benefit of DL is its competency in learning massive data.The DL-based technologies have grown faster and are widely adopted to handle the conventional approaches resourcefully.Specifically,various DL approaches outperform the conventional ML approaches in real-time applications.Indeed,various research works are reviewed to understand the significance of the individual DL models and some computational complexity is observed.This may be due to the broader expertise and knowledge required for handling these models during the prediction process.This research proposes a holistic approach for pneumonia prediction and offers a more appropriate DL model for classification purposes.This work incorporates a novel fused Squeeze and Excitation(SE)block with the ResNet model for pneumonia prediction and better accuracy.The expected model reduces the human effort during the prediction process and makes it easier to diagnose it intelligently as the feature learning is adaptive.The experimentation is carried out in Keras,and the model’s superiority is compared with various advanced approaches.The proposed model gives 90%prediction accuracy,93%precision,90%recall and 89%F1-measure.The proposed model shows a better trade-off compared to other approaches.The evaluation is done with the existing standard ResNet model,GoogleNet+ResNet+DenseNet,and different variants of ResNet models.

A Fused Machine Learning Approach for Intrusion Detection System

The rapid growth in data generation and increased use of computer network devices has amplified the infrastructures of internet.The interconnectivity of networks has brought various complexities in maintaining network availability,consistency,and discretion.Machine learning based intrusion detection systems have become essential to monitor network traffic for malicious and illicit activities.An intrusion detection system controls the flow of network traffic with the help of computer systems.Various deep learning algorithms in intrusion detection systems have played a prominent role in identifying and analyzing intrusions in network traffic.For this purpose,when the network traffic encounters known or unknown intrusions in the network,a machine-learning framework is needed to identify and/or verify network intrusion.The Intrusion detection scheme empowered with a fused machine learning technique(IDS-FMLT)is proposed to detect intrusion in a heterogeneous network that consists of different source networks and to protect the network from malicious attacks.The proposed IDS-FMLT system model obtained 95.18%validation accuracy and a 4.82%miss rate in intrusion detection.

Effect of Fibre Size on Mechanical Properties and Surface Roughness of PLA Composites by Using Fused Deposition Modelling (FDM)

Naturalfibre as a reinforcing agent has been widely used in many industrial applications.Nevertheless,several factors need to be considered,such as the size and weight percentage of thefibre used in binding.Using fused deposition modelling(FDM),this factor was investigated by varying the size of naturalfibre as the responding variable with afixed weight percentage of kenaffibre.The process of modifying the naturalfibre in terms of size might increase the dispersion of kenaffibre in the polymer matrix and increase the adhesion bonding between thefibre and matrix of composites,subsequently improving the interfacial bonding between these two phases.In this paper,the effect offibre size was evaluated by performing the mechanical test,Scanning Electron Micrograph(SEM)to observe the morphology of the composites,and also by surface analysis.The surface roughness was visualised using a 3D profilometer and thefigure was illustrated as colour shading in the image.The composite withfibre size≤100μm displayed better tensile andflexural strength,compared to other sizes.In conclusion,by reducing the size of thefibre,the composites could develop high strength performance for industrial applications.

Development and Evaluation of Recycled Polypropylene and Bean Pod Powder Composite Biomaterial for Fused Filament Fabrication

Approximately 450 million tons of plastic and agricultural waste are produced each year in the world. Only a small portion of this plastic waste is recycled, and a small portion of this agricultural waste is used as fuel or fertilizer, and the rest of this waste is left in the environment or is burned, resulting in environmental and air pollution. For proper disposal, plastic and agricultural waste can be used in the manufacture of composites as raw materials. In this study, we had evaluated the use of bean pod powder (BPp) was used as natural reinforcing filler in recycled polypropylene (rPP) based composites. BPp/rPP composite filaments were developed using the extrusion method and the samples were printed by Fused Filament Fabrication (FFF). Composites with rPP matrix containing different weight fractions of BPp (5%, 10% and 15%) were fabricated to observe and compare the mechanical properties (tensile, flexural, and compressive strength) of the filament composites. In addition, the filament surface was analyzed for roughness and particle size of bean pod powder. The results established that BPp/rPP composites exhibited better tensile, flexural, and compressive strength than rPP and pure PP. By adding 5 wt% BPp, the tensile strength of rPP increased from 20.4 MPa to 22.8 MPa. The highest flexural strength (15.05 MPa) was obtained at 5 wt% BPp among all composites and the highest compressive strength (24.5 MPa), was obtained at 10 wt% BPp. Therefore, it can be concluded that by carefully selecting the ratio of BPp to bean pod powder, it is therefore possible to positively influence the mechanical properties of the resulting composite.

Characterization of 3D Printed Poly(3-Hydroxybutyric-Co-3-Hydroxyvalerate) by Fused Granular Fabrication through Thermal and Mechanical Analyses

Poly[R-3-hydroxybutyrate-co-(R-3-hydroxyvalerate)] (PHBVs) copolymers are promising biopolymers, which could substitute petroleum-based plastics for various applications. PHB and PHBV pellets were processed on a customized 3D printer via Fused Granular Manufacturing (FGM) approach modified with a Mahor screw extruder. To anticipate the behaviour of PHBVs when transformed using conventional thermo-mechanical shaping processes, thermal and mechanical analyses were carried out in order to better understand the effect of annealing temperature on their crystallization behaviour and mechanical properties of PHB polymer and PHBV copolymer. The objectives of the present work were to propose an experimental strategy to study the melting and crystallization events, crystalline structure changes, and mechanical performances of both PHB homopolymer and PHBV copolymer according to identical thermal annealing treatments. A monitoring of 3D printed PHB and PHBV structures was achieved by coupling Differential Scanning Calorimetry (DSC) and tensile tests. .

Optimization of Extrusion Process Parameters of Recycled High-Density Polyethylene-Thermoplastic Starch Composite for Fused Filament Fabrication

High-density poly-ethylene (HDPE) is a nonbiodegradable recyclable plastic which is widely utilized in single use packaging applications. Consequently, it constitutes a significant amount of plastic waste found in landfills. From literature, it has been shown that parts produced using composites of HDPE with carbohydrate-based polymers, such as thermoplastic starch (TPS), experience mechanical degradation through hydrolytic degradation process. The possible utilization of recycled-HDPE (rHDPE) and TPS composite in nonconventional manufacturing processes such as Fused filament fabrication (FFF) has however not been explored. This study explores the potential application of rHDPE and TPS composites in FFF and optimizes the extrusion process parameters used in rHDPE-TPS filament production process. Taguchi method was utilized to analyze the extrusion process. The extrusion process parameters studied were the spooling speed, extrusion speed and the extrusion temperatures. The response variable studied was the filament diameter. In this research, the maximum TPS content achieved during filament production was 40 wt%. This filament was however challenging to use in FFF printers due to frequent nozzle clogging. Printing was therefore done with filaments that contained 0 - 30 wt% TPS. The experimental results showed that the most significant parameter in extrusion process was the spooling speed, followed by extrusion speed. Extrusion temperature had the least significant influence on the filament diameter. It was observed that increase in TPS content resulted in reduced warping and increased rate of hydrolytic degradation. Mechanical properties of printed parts were investigated and the results showed that increasing TPS content resulted in reduction in tensile strength, reduction in compression strength and increase in stiffness. The findings of this research provide valuable insights to plastic recycling industries and researchers regarding the utilization of recycled HDPE and TPS composites as substitute materials in FFF.

BacFuse棘突间植入术和后路椎间融合固定术治疗腰椎间盘突出症的对比研究

目的通过与后路椎间融合固定术(PLIF)对比,评价Bac Fuse棘突间植入术治疗腰椎间盘突出症的中短期临床疗效。方法回顾性分析2014年1月至2015年1月符合入组标准的单节段腰椎间盘突出症60例,其中BacFuse组30例,PLIF组30例。统计分析两组的住院时间、手术时间、术中失血量。术前、术后6月的视觉模拟评分(VAS)、日本骨科学会腰痛评分(JOA)、椎间盘后缘高度(PDH)。结果 BacFuse组性别、年龄、手术节段与PLIF组相比较无统计学差异。BacFuse组和PLIF组相比,住院时间较短(t=-10.17,P<0.001),手术时间也较短(t=-28.94,P<0.001),出血量较少(t=-31.03,P<0.001),差异均有统计学意义。术后6月随访两组VAS评分均小于术前(P<0.001),两组术前及术后6个月随访VAS评分差异无统计学意义。术后6月随访两组JOA评分均显著大于术前(P<0.001),两组术前及术后6个月随访JOA评分差异无统计学意义。BacFuse组术前PDH 6.26±1.7 mm,6个月随访8.27±1.9 mm,较术前明显改善(t=-12.347,P<0.001)。PLIF组术前PDH 6.33±1.4 mm,6个月随访8.41±1.4mm,较术前明显改善(t=-14.007,P<0.001)。两组术前及术后6月随访PDH差异无统计学意义(P>0.05)。结论 BacFuse棘突间植入术在与PLIF效果相似的情况下损伤更小,是治疗腰椎间盘突出症的有效微创方法。

基于fused惩罚的稀疏主成分分析

本文旨在研究基于fused惩罚的稀疏主成分分析方法,以适用于相邻变量之间高度相关甚至完全相等的数据情形。首先,从回归分析角度出发,提出一种求解稀疏主成分的简便思路,给出一种广义的稀疏主成分模型——GSPCA模型及其求解算法,并证明在惩罚函数取1-范数时,该模型与现有的稀疏主成分模型——SPC模型的求解结果一致。其次,提出将fused惩罚与主成分分析相结合,得到一种fused稀疏主成分分析方法,并从惩罚性矩阵分解和回归分析两个角度,给出两种模型形式。在理论上证明了两种模型的求解结果是一致的,故将其统称为FSPCA模型。模拟实验显示,FSPCA模型在处理相邻变量之间高度相关甚至完全相等的数据集上表现良好。最后,将FSPCA模型应用于手写数字识别,发现与SPC模型相比,FSPCA模型所提取的主成分具备更好的解释性。

基于Fuse的用户态文件系统的设计

现有的文件系统大都运行在内核态下,与内核紧密结合,导致难以对其进行功能上的扩展。针对内核文件系统的这个问题,本文提出了一个基于Fuse框架实现的用户级文件系统dbfuse。一方面将文件系统从内核态中解放出来;另一方面使用数据库技术有效地保证文件系统数据的完整性和安全性,给数据共享带来的方便。

针对发动机平面度的二维FusedLASSO多元统计控制图

针对具有二维平面自然顺序关系的多元数据,提出了一种基于二维Fused LASSO回归模型的多元统计过程控制图。由于二维Fused LASSO多元回归模型对相邻系数的差异进行惩罚,因此它对检测出变量间的自然顺序关系非常有效。通过数值仿真实验可以看到,二维Fused LASSO控制图能更加快速有效地检测出具有二维平面自然顺序的多元过程中均值发生的变化,且在偏移量越大的情况下优势更加明显。最后通过对发动机平面度数据的实例验证,给出了二维Fused LASSO控制图的步骤和适用性。

Micro/nano Indentation and Single Grit Diamond Grinding Mechanism on Ultra Pure Fused Silica

The existing research about ductile grinding of fused silica glass was mainly focused on how to carry out ductile regime material removal for generating very ＂smoothed＂ surface and investigate the machining-induced damage in the grinding in order to reduce or eliminate the subsurface damage.The brittle/ductile transition behavior of optical glass materials and the wear of diamond wheel are the most important factors for ductile grinding of optical glass.In this paper,the critical brittle/ductile depth,the influence factors on brittle/ductile transition behavior,the wear of diamond grits in diamond grinding of ultra pure fused silica（UPFS） are investigated by means of micro/nano indentation technique,as well as single grit diamond grinding on an ultra-stiff machine tool,Tetraform ＂C＂.The single grit grinding processes are in-process monitored using acoustic emission（AE） and force dynamometer simultaneously.The wear of diamond grits,morphology and subsurface integrity of the machined groves are examined with atomic force microscope（AFM） and scanning electron microscope（SEM）.The critical brittle/ductile depth of more than 0.5 μm is achieved.When compared to the using roof-like grits,by using pyramidal diamonds leads to higher critical depths of scratch with identical grinding parameters.However,the influence of grit shapes on the critical depth is not significant as supposed.The grinding force increased linearly with depth of cut in the ductile removal regime,but in brittle removal regime,there are large fluctuations instead of forces increase.The SEM photographs of the cross-section profile show that the median cracks dominate the crack patterns beneath the single grooves.Furthermore,The SEM photographs show multi worn patterns of diamond grits,indicating an inhomogeneous wear mechanism of diamond grits in grinding of fused silica with diamond grinding wheels.The proposed research provides the basal technical theory for improving the ultra-precision grinding of UPFS.

CO_2 Density-Raman Shift Relation Derived from Synthetic Inclusions in Fused Silica Capillaries and Its Application

The densities of CO2 inclusions in minerals are commonly used to determine the crystallizing conditions of the host minerals. However, conventional microthermometry is difficult to apply for inclusions of small size （〈 5-10 μm） or low density. Raman analysis is an alternative method for determining CO2 density, provided that the CO2 density-Raman shift relation is known. This study aims to establish this CO2 density-Raman shift relation by using CO2 inclusions synthesized in fused silica capillaries. By using this newly-developed synthetic technique, we formed pure CO2 inclusions, and their densities were determined by microthermometry. The Raman analysis showed that the relation between CO2 density （D in g/cm^3） and the separations （△ in cm^-1） between the two main bands （i.e. Fermi diad bands） in CO2 Raman spectra can be represented by a cubic equation： D （g/cm^3）=0.74203（-0.019^3＋5.90332△^2-610.79472△＋21050.30165）-3.54278 （r^2=0.99920）. Our calculated D value for a given A is between those obtained from two previously-reported equations, which were derived from different experimental methods. An example was given in this study to demonstrate that the densities of natural CO2 inclusions that could not be derived from microthermometry could be determined by using our method.