In this study, well-dispersed gold nanoparticles were prepared by using intra-molecular reduction of sodium gold sulfite, without using additional reductants and chloride free. The technical parameters including trans...In this study, well-dispersed gold nanoparticles were prepared by using intra-molecular reduction of sodium gold sulfite, without using additional reductants and chloride free. The technical parameters including transformation temperature, pH, and concentration were optimized by the single-factor method as 90 C, pH 1, and 0.01 mmol/L [Na3Au（SO3）2], respectively. The resultant colloidal transmission electron microscopy images （TEM） and UV-vis absorption spectrophotometer spectra were acquired to check their properties, and the results show this kind of colloidal gold is controlled to 6 nm in sizes and has good stability in solution.展开更多
基金financially supported by the National Natural Science Foundation of China(No.20976201)the Graduate's Scientific Research Foundation of Central South University of Forestry and Technology(No.CX2012B04)
文摘In this study, well-dispersed gold nanoparticles were prepared by using intra-molecular reduction of sodium gold sulfite, without using additional reductants and chloride free. The technical parameters including transformation temperature, pH, and concentration were optimized by the single-factor method as 90 C, pH 1, and 0.01 mmol/L [Na3Au（SO3）2], respectively. The resultant colloidal transmission electron microscopy images （TEM） and UV-vis absorption spectrophotometer spectra were acquired to check their properties, and the results show this kind of colloidal gold is controlled to 6 nm in sizes and has good stability in solution.
