In order to improve vibration mills grinding effect and increase productive efficiency, prime factors of vibration mills were gained much attention. The purpose of this study is to reveal product size distribution and...In order to improve vibration mills grinding effect and increase productive efficiency, prime factors of vibration mills were gained much attention. The purpose of this study is to reveal product size distribution and grinding dynamics of vibration mills by orthogonal experi-ments. The metallurgical refractory materials were used as research object. In order to explore the relationships between grinding effect and primary factors, lots of milling experiments were carried out. Based on the results, the conclusions can be summarized: as time runs, the size distri-bution shows exponential trend, and range becomes more and more narrow. Also the quantitative analysis result between grinding effect and primary factors was obtained by non-linear regres-sion: high frequency, high amplitude and low fill ratio can increase grinding speed.展开更多
An attempt was made to investigate the machinability of Si Cp/Al composites based on the experimental study using mill-grinding processing method. The experiments were carried out on a high-speed CNC machining center ...An attempt was made to investigate the machinability of Si Cp/Al composites based on the experimental study using mill-grinding processing method. The experiments were carried out on a high-speed CNC machining center using integrated abrasive cutting tool. The effects of combined machining parameters, e g, cutting speed(vs), feed rate(vf), and depth of cut(ap), with the same change of material removal rate(MRR) on the mill-grinding force and surface roughness(Ra) were investigated. The formation mechanism of typical machined surface defects was analyzed by SEM. The experimental results reveal that with the same change of material removal rate, lower mill-grinding force values can be gained by increasing depth of cut and feed rate simultaneously at higher cutting speed. With the same change of MRR value, lower surface roughness values can be gained by increasing the feed rate at higher cutting speed, rather than just increasing the depth of cut, or increasing the feed rate and depth of cut simultaneously. The machined surface of Si Cp/Al composites reveals typical defects which can influence surface integrity.展开更多
In order to optimize the current grinding procedure of the backup roll of 2050 continuously variable crown (CVC) mills, the behavior of rolling contact fatigue (RCF) cracking was investigated. Two RCF short cracks, in...In order to optimize the current grinding procedure of the backup roll of 2050 continuously variable crown (CVC) mills, the behavior of rolling contact fatigue (RCF) cracking was investigated. Two RCF short cracks, including vertical short crack and ratcheting short crack initiated from ratcheting, were observed. The behavior of both RCF cracks was analyzed in detail. Then a modified grinding procedure was proposed according to the behavior of RCF cracks and the preventive grinding strategy.展开更多
A new self-made additive of amidocyanogen-acetic salt was used in wet ball-grind technique (WBGT) for preparing hydrogen storage alloys, and the effect on the electrochemical performance of the alloy electrode was i...A new self-made additive of amidocyanogen-acetic salt was used in wet ball-grind technique (WBGT) for preparing hydrogen storage alloys, and the effect on the electrochemical performance of the alloy electrode was investigated in detail. It was found that the prepared electrode had perfect electrochemical performances, such as rapid activation, high capability, high-rate discharge (HRD) ability, and good stability. The first discharge capacitance at 0.2 C (throughout this study, n C rate means that the rated capacity of a hydrogen storage alloy (full capacity) is charged or discharged completely in 1/n h) reached 278 mAh·g^-1 and the discharge capacitance reached the maximum of 322 mAh·g^-1 only after two charge-discharge cycles. For the dry method, wet method, and WBGT, the high rate discharge (HRD) values (C5 c/C0.2c ratio) were approximately 0.59, 0.76, and 0.83, respectively. The stable discharge capacity at 3 C increased from 275 mAh·g^-1 (dry method)to 295 mAh·g^-1 (WBGT).展开更多
The fluidity and classification of bulk material (loose body) were introduced, the self-grinding mechanism and the affecting factors of bulk materials in various forms of phase, state and motion were investigated. A r...The fluidity and classification of bulk material (loose body) were introduced, the self-grinding mechanism and the affecting factors of bulk materials in various forms of phase, state and motion were investigated. A rotational-flow-state centrifugal autogenous grinder was developed on the basis of applying self-grinding mechanism of bulk material,the result tested by the autogenous grinder was compared with that tested by 4R Raymond mills, and fine particles with extremely high specific area were obtained. The feasibility of the developed new-type autogenous grinder in the view of fluid motion of bulk material was proved.展开更多
High-speed stirred mills are utilized to grind particles below 10mm. Grinding sulphide minerals to as low as 10mm achieve adequate mineral liberation for successful downstream mineral processing operations, such as fl...High-speed stirred mills are utilized to grind particles below 10mm. Grinding sulphide minerals to as low as 10mm achieve adequate mineral liberation for successful downstream mineral processing operations, such as flotation and leaching. Particle breakage mechanism such as fracture or abrasion, determines the morphological surface features of the product particles. It is anticipated that particles, which break along grain boundaries (intergranular) produce rough surfaces, whereas particles that break across the grain boundaries (transgranular) possess smoother surfaces. In this study, particles are ground in a stirred mill and their morphological features were analyzed using automated and manual detection methods. Literature and conventional belief are that high-speed stirred mills break particles by attrition. This paper showed that fracture is also an important breakage mechanism along with attrition. Breakage mechanism is a factor of input stress intensity, in the form of the mill agitator speed, and type of mineral. It is observed that at higher agitator speed galena fractures along the grain boundaries, whereas quartz, abrade across the grain boundaries.展开更多
This study aimed to prepare and characterize itraconazole (ITCZ)- or miconazole (MCZ)-loaded poly (lactide-co-glycolide) (PLGA) microparticles (MP) using a co-grinding method with ball milling, which is a solvent-free...This study aimed to prepare and characterize itraconazole (ITCZ)- or miconazole (MCZ)-loaded poly (lactide-co-glycolide) (PLGA) microparticles (MP) using a co-grinding method with ball milling, which is a solvent-free and convenient procedure. PLGA MP was prepared by grinding for 60 min, and the fixed theoretical drug loading was set at 9.1% and 16.7% for both drugs. The obtained loading efficiency for both drugs was estimated to be approximately 100%. The average diameters of the drug-loaded PLGA MP were approximately 20 - 35 μm. Powder X-ray diffraction (PXRD) or differential scanning calorimetry (DSC) confirmed amorphization of ITCZ and MCZ in ITCZ- or MCZ-loaded PLGA MP in all formulations. The drug release percentage from 9.1%-loaded ITCZ-PLGA7505 MP at 24 h was almost 50%, which was higher than that of ITCZ powder. The drug release percentage from MCZ-loaded PLGA7505 MP at 4 h was over 80%, which was higher than that of MCZ powder. This enhancement of release rate is caused by the amorphization of ITCZ or MCZ in the PLGA matrix. MCZ-loaded PLGA7510 MP showed a sustained release profile up to 24 h, suggesting that MCZ exists in an amorphous form in the PLGA matrix;however, the release rate declined owing to the large molecular weight of PLGA. Therefore, the release enhancement of antifungal drugs loaded on PLGA MP could be achieved by their amorphization using a co-grinding method with ball milling.展开更多
Surface topography of superalloy GH4169 workpieces machined by milling and grinding is different significantly. Meanwhile, surface roughness, as one of the main indicators of machined surface integrity, has a great in...Surface topography of superalloy GH4169 workpieces machined by milling and grinding is different significantly. Meanwhile, surface roughness, as one of the main indicators of machined surface integrity, has a great influence on the fatigue behavior of workpieces. Based on analyzing the formation mechanism and characteristics of surface roughness utilizing different machining processes and parameters, the machined surface roughness curve can be decoupled into two parts utilizing frequency spectrum analysis, which are kinematic surface roughness curve and stochastic surface roughness curve. The kinematic surface roughness curve is influenced by machining process,parameters, geometry of the cutting tool or wheel, the maximum height of which is expressed as Rz'.By subtracting the kinematic part from the measurement curve, the stochastic surface roughness curve and its maximum height Rz" can be obtained, which is influenced by the defects of cutting tool edge or abrasive grains, built-up edges(BUE), cracks, high frequency vibration and so on. On the other hand, the results of decoupling analysis of surface roughness curves indicate that Raand Rz values of milling GH4169 are 2–5 times and 1–3 times as high as those of grinding, while Rz" value of milling is 13.85%–37.7% as high as that of grinding. According to the results of fatigue life tests of specimens machined by milling and grinding, it can be concluded that fatigue behavior of GH4169 decreases with the increase of Rz"monotonically, even utilizing different machining processes.展开更多
Fiber-reinforced composites have become the preferred material in the fields of aviation and aerospace because of their high-strength performance in unit weight.The composite components are manufactured by near netsha...Fiber-reinforced composites have become the preferred material in the fields of aviation and aerospace because of their high-strength performance in unit weight.The composite components are manufactured by near netshape and only require finishing operations to achieve final dimensional and assembly tolerances.Milling and grinding arise as the preferred choices because of their precision processing.Nevertheless,given their laminated,anisotropic,and heterogeneous nature,these materials are considered difficult-to-machine.As undesirable results and challenging breakthroughs,the surface damage and integrity of these materials is a research hotspot with important engineering significance.This review summarizes an up-to-date progress of the damage formation mechanisms and suppression strategies in milling and grinding for the fiber-reinforced composites reported in the literature.First,the formation mechanisms of milling damage,including delamination,burr,and tear,are analyzed.Second,the grinding mechanisms,covering material removal mechanism,thermal mechanical behavior,surface integrity,and damage,are discussed.Third,suppression strategies are reviewed systematically from the aspects of advanced cutting tools and technologies,including ultrasonic vibration-assisted machining,cryogenic cooling,minimum quantity lubrication(MQL),and tool optimization design.Ultrasonic vibration shows the greatest advantage of restraining machining force,which can be reduced by approximately 60%compared with conventional machining.Cryogenic cooling is the most effective method to reduce temperature with a maximum reduction of approximately 60%.MQL shows its advantages in terms of reducing friction coefficient,force,temperature,and tool wear.Finally,research gaps and future exploration directions are prospected,giving researchers opportunity to deepen specific aspects and explore new area for achieving high precision surface machining of fiber-reinforced composites.展开更多
A compound process that integrates end electrical discharge (ED) milling and mechanical grinding to machine silicon carbide (SiC) ceramics is developed in this paper. The process employs a turntable with several unifo...A compound process that integrates end electrical discharge (ED) milling and mechanical grinding to machine silicon carbide (SiC) ceramics is developed in this paper. The process employs a turntable with several uniformly-distributed cylindrical copper electrodes and abrasive sticks as the tool, and uses a water-based emulsion as the machining fluid. End electrical discharge milling and mechanical grinding happen alternately and are mutually beneficial, so the process is able to effectively machine a large surface area on SiC ceramic with a good surface quality. The machining principle and characteristics of the technique are introduced. The effects of polarity, pulse duration, pulse interval, open-circuit voltage, discharge current, diamond grit size, emulsion concentration, emulsion flux, milling depth and tool stick number on performance parameters such as the material removal rate, tool wear ratio, and surface roughness have been investigated. In addition, the microstructure of the machined surface under different machining conditions is examined with a scanning electron microscope and an energy dispersive spectrometer. The SiC ceramic was mainly removed by end ED milling during the initial rough machining mode, whereas it is mainly removed by mechanical grinding during the later finer machining mode; moreover, the tool material can transfer to the workpiece surface during the compound process.展开更多
文摘In order to improve vibration mills grinding effect and increase productive efficiency, prime factors of vibration mills were gained much attention. The purpose of this study is to reveal product size distribution and grinding dynamics of vibration mills by orthogonal experi-ments. The metallurgical refractory materials were used as research object. In order to explore the relationships between grinding effect and primary factors, lots of milling experiments were carried out. Based on the results, the conclusions can be summarized: as time runs, the size distri-bution shows exponential trend, and range becomes more and more narrow. Also the quantitative analysis result between grinding effect and primary factors was obtained by non-linear regres-sion: high frequency, high amplitude and low fill ratio can increase grinding speed.
基金Funded by the National Defense Basic Scientific ResearchAerospace Science and Technology Corporation Commonality Technology Research Project
文摘An attempt was made to investigate the machinability of Si Cp/Al composites based on the experimental study using mill-grinding processing method. The experiments were carried out on a high-speed CNC machining center using integrated abrasive cutting tool. The effects of combined machining parameters, e g, cutting speed(vs), feed rate(vf), and depth of cut(ap), with the same change of material removal rate(MRR) on the mill-grinding force and surface roughness(Ra) were investigated. The formation mechanism of typical machined surface defects was analyzed by SEM. The experimental results reveal that with the same change of material removal rate, lower mill-grinding force values can be gained by increasing depth of cut and feed rate simultaneously at higher cutting speed. With the same change of MRR value, lower surface roughness values can be gained by increasing the feed rate at higher cutting speed, rather than just increasing the depth of cut, or increasing the feed rate and depth of cut simultaneously. The machined surface of Si Cp/Al composites reveals typical defects which can influence surface integrity.
文摘In order to optimize the current grinding procedure of the backup roll of 2050 continuously variable crown (CVC) mills, the behavior of rolling contact fatigue (RCF) cracking was investigated. Two RCF short cracks, including vertical short crack and ratcheting short crack initiated from ratcheting, were observed. The behavior of both RCF cracks was analyzed in detail. Then a modified grinding procedure was proposed according to the behavior of RCF cracks and the preventive grinding strategy.
文摘A new self-made additive of amidocyanogen-acetic salt was used in wet ball-grind technique (WBGT) for preparing hydrogen storage alloys, and the effect on the electrochemical performance of the alloy electrode was investigated in detail. It was found that the prepared electrode had perfect electrochemical performances, such as rapid activation, high capability, high-rate discharge (HRD) ability, and good stability. The first discharge capacitance at 0.2 C (throughout this study, n C rate means that the rated capacity of a hydrogen storage alloy (full capacity) is charged or discharged completely in 1/n h) reached 278 mAh·g^-1 and the discharge capacitance reached the maximum of 322 mAh·g^-1 only after two charge-discharge cycles. For the dry method, wet method, and WBGT, the high rate discharge (HRD) values (C5 c/C0.2c ratio) were approximately 0.59, 0.76, and 0.83, respectively. The stable discharge capacity at 3 C increased from 275 mAh·g^-1 (dry method)to 295 mAh·g^-1 (WBGT).
文摘The fluidity and classification of bulk material (loose body) were introduced, the self-grinding mechanism and the affecting factors of bulk materials in various forms of phase, state and motion were investigated. A rotational-flow-state centrifugal autogenous grinder was developed on the basis of applying self-grinding mechanism of bulk material,the result tested by the autogenous grinder was compared with that tested by 4R Raymond mills, and fine particles with extremely high specific area were obtained. The feasibility of the developed new-type autogenous grinder in the view of fluid motion of bulk material was proved.
文摘High-speed stirred mills are utilized to grind particles below 10mm. Grinding sulphide minerals to as low as 10mm achieve adequate mineral liberation for successful downstream mineral processing operations, such as flotation and leaching. Particle breakage mechanism such as fracture or abrasion, determines the morphological surface features of the product particles. It is anticipated that particles, which break along grain boundaries (intergranular) produce rough surfaces, whereas particles that break across the grain boundaries (transgranular) possess smoother surfaces. In this study, particles are ground in a stirred mill and their morphological features were analyzed using automated and manual detection methods. Literature and conventional belief are that high-speed stirred mills break particles by attrition. This paper showed that fracture is also an important breakage mechanism along with attrition. Breakage mechanism is a factor of input stress intensity, in the form of the mill agitator speed, and type of mineral. It is observed that at higher agitator speed galena fractures along the grain boundaries, whereas quartz, abrade across the grain boundaries.
文摘This study aimed to prepare and characterize itraconazole (ITCZ)- or miconazole (MCZ)-loaded poly (lactide-co-glycolide) (PLGA) microparticles (MP) using a co-grinding method with ball milling, which is a solvent-free and convenient procedure. PLGA MP was prepared by grinding for 60 min, and the fixed theoretical drug loading was set at 9.1% and 16.7% for both drugs. The obtained loading efficiency for both drugs was estimated to be approximately 100%. The average diameters of the drug-loaded PLGA MP were approximately 20 - 35 μm. Powder X-ray diffraction (PXRD) or differential scanning calorimetry (DSC) confirmed amorphization of ITCZ and MCZ in ITCZ- or MCZ-loaded PLGA MP in all formulations. The drug release percentage from 9.1%-loaded ITCZ-PLGA7505 MP at 24 h was almost 50%, which was higher than that of ITCZ powder. The drug release percentage from MCZ-loaded PLGA7505 MP at 4 h was over 80%, which was higher than that of MCZ powder. This enhancement of release rate is caused by the amorphization of ITCZ or MCZ in the PLGA matrix. MCZ-loaded PLGA7510 MP showed a sustained release profile up to 24 h, suggesting that MCZ exists in an amorphous form in the PLGA matrix;however, the release rate declined owing to the large molecular weight of PLGA. Therefore, the release enhancement of antifungal drugs loaded on PLGA MP could be achieved by their amorphization using a co-grinding method with ball milling.
基金supported by the Aeronautical Science Foundation of China (No.2016ZE51039)
文摘Surface topography of superalloy GH4169 workpieces machined by milling and grinding is different significantly. Meanwhile, surface roughness, as one of the main indicators of machined surface integrity, has a great influence on the fatigue behavior of workpieces. Based on analyzing the formation mechanism and characteristics of surface roughness utilizing different machining processes and parameters, the machined surface roughness curve can be decoupled into two parts utilizing frequency spectrum analysis, which are kinematic surface roughness curve and stochastic surface roughness curve. The kinematic surface roughness curve is influenced by machining process,parameters, geometry of the cutting tool or wheel, the maximum height of which is expressed as Rz'.By subtracting the kinematic part from the measurement curve, the stochastic surface roughness curve and its maximum height Rz" can be obtained, which is influenced by the defects of cutting tool edge or abrasive grains, built-up edges(BUE), cracks, high frequency vibration and so on. On the other hand, the results of decoupling analysis of surface roughness curves indicate that Raand Rz values of milling GH4169 are 2–5 times and 1–3 times as high as those of grinding, while Rz" value of milling is 13.85%–37.7% as high as that of grinding. According to the results of fatigue life tests of specimens machined by milling and grinding, it can be concluded that fatigue behavior of GH4169 decreases with the increase of Rz"monotonically, even utilizing different machining processes.
基金the National Key R&D Program of China(Grant No.2020YFB2010500)the National Natural Science Foundation of China(Grant Nos.51975305 and 51905289)+2 种基金Shandong Natural Science Foundation,China(Grant Nos.ZR2020KE027 and ZR2020ME158)the Innovation Talent Supporting Program for Postdoctoral Fellows of Shandong Province,China(Grant No.SDBX2020012)the Major Science and Technology Innovation Engineering Projects of Shandong Province,China(Grant No.2019JZZY020111).
文摘Fiber-reinforced composites have become the preferred material in the fields of aviation and aerospace because of their high-strength performance in unit weight.The composite components are manufactured by near netshape and only require finishing operations to achieve final dimensional and assembly tolerances.Milling and grinding arise as the preferred choices because of their precision processing.Nevertheless,given their laminated,anisotropic,and heterogeneous nature,these materials are considered difficult-to-machine.As undesirable results and challenging breakthroughs,the surface damage and integrity of these materials is a research hotspot with important engineering significance.This review summarizes an up-to-date progress of the damage formation mechanisms and suppression strategies in milling and grinding for the fiber-reinforced composites reported in the literature.First,the formation mechanisms of milling damage,including delamination,burr,and tear,are analyzed.Second,the grinding mechanisms,covering material removal mechanism,thermal mechanical behavior,surface integrity,and damage,are discussed.Third,suppression strategies are reviewed systematically from the aspects of advanced cutting tools and technologies,including ultrasonic vibration-assisted machining,cryogenic cooling,minimum quantity lubrication(MQL),and tool optimization design.Ultrasonic vibration shows the greatest advantage of restraining machining force,which can be reduced by approximately 60%compared with conventional machining.Cryogenic cooling is the most effective method to reduce temperature with a maximum reduction of approximately 60%.MQL shows its advantages in terms of reducing friction coefficient,force,temperature,and tool wear.Finally,research gaps and future exploration directions are prospected,giving researchers opportunity to deepen specific aspects and explore new area for achieving high precision surface machining of fiber-reinforced composites.
基金supported by the National Natural Science Foundation of China(50675225)the Scientific Research Personnel Service Project from the Ministry of Science and Technology of China(2009GJC60047)the Independent Innovation Research Project from China University of Petroleum(11CX04031A)
文摘A compound process that integrates end electrical discharge (ED) milling and mechanical grinding to machine silicon carbide (SiC) ceramics is developed in this paper. The process employs a turntable with several uniformly-distributed cylindrical copper electrodes and abrasive sticks as the tool, and uses a water-based emulsion as the machining fluid. End electrical discharge milling and mechanical grinding happen alternately and are mutually beneficial, so the process is able to effectively machine a large surface area on SiC ceramic with a good surface quality. The machining principle and characteristics of the technique are introduced. The effects of polarity, pulse duration, pulse interval, open-circuit voltage, discharge current, diamond grit size, emulsion concentration, emulsion flux, milling depth and tool stick number on performance parameters such as the material removal rate, tool wear ratio, and surface roughness have been investigated. In addition, the microstructure of the machined surface under different machining conditions is examined with a scanning electron microscope and an energy dispersive spectrometer. The SiC ceramic was mainly removed by end ED milling during the initial rough machining mode, whereas it is mainly removed by mechanical grinding during the later finer machining mode; moreover, the tool material can transfer to the workpiece surface during the compound process.