The hard X-ray nanoprobe beamline at the SSRF

The hard X-ray nanoprobe beamline BL13U is a phase-Ⅱ beamline project at the Shanghai Synchrotron Radiation Facility.The beamline aims to enable comprehensive experiments at high spatial resolutions ranging from 50 to 10 nm. The X-ray energy range of the beamline, 5–25 keV, can detect most elements in the periodic table. Two operating modes were designed to accommodate the experimental requirements of high-energy resolution or high photon flux, respectively. X-ray nanofluorescence, nanodiffraction, and coherent diffraction imaging are developed as the main experimental techniques for BL13U. This paper describes the beamline optics, end station configurations, experimental methods under development, and preliminary test results. This comprehensive overview aims to provide a clear understanding of the beamline capabilities and potential applications.

Energy spectrum computed tomography multi-parameter imaging in preoperative assessment of vascular and neuroinvasive status in gastric cancer

BACKGROUND Vascular and nerve infiltration are important indicators for the progression and prognosis of gastric cancer(GC),but traditional imaging methods have some limitations in preoperative evaluation.In recent years,energy spectrum computed tomography(CT)multiparameter imaging technology has been gradually applied in clinical practice because of its advantages in tissue contrast and lesion detail display.AIM To explore and analyze the value of multiparameter energy spectrum CT imaging in the preoperative assessment of vascular invasion(LVI)and nerve invasion(PNI)in GC patients.METHODS Data from 62 patients with GC confirmed by pathology and accompanied by energy spectrum CT scanning at our hospital between September 2022 and September 2023,including 46 males and 16 females aged 36-71(57.5±9.1)years,were retrospectively collected.The patients were divided into a positive group(42 patients)and a negative group(20 patients)according to the presence of LVI/PNI.The CT values(CT40 keV,CT70 keV),iodine concentration(IC),and normalized IC(NIC)of lesions in the upper energy spectrum CT images of the arterial phase,venous phase,and delayed phase 40 and 70 keV were measured,and the slopes of the energy spectrum curves[K(40-70)]from 40 to 70 keV were calculated.Arterial Core Tip:To investigate the application value of multiparameter energy spectrum computed tomography(CT)imaging in the preoperative assessment of vascular and nerve infiltration in patients with gastric cancer(GC).The imaging data of GC patients were retrospectively analyzed to evaluate the accuracy and sensitivity of CT for identifying and quantifying vascular and nerve infiltration and for comparison with postoperative pathological results.The purpose of this study was to verify the clinical feasibility and potential advantages of multiparameter energy spectrum CT imaging in guiding preoperative diagnosis and treatment decision-making and to provide a new imaging basis for improving the diagnostic accuracy and prognosis of GC patients.

Weighted Hard Combination for Cooperative Spectrum Sensing in Cognitive Radio Networks

Weighted one bit hard combination for cooperative spectrum sensing is proposed in this paper. Two thresholds are adopted to divide the possible energy value into three weighted regions. If the energy value falls into the corresponding region,it will be judged as "1",no information or "0". When the probability of false alarm is constrained to be constant,the objective is to maximize the probability of detection. The optimization problem is simplified by separating the weight of the middle region into several intervals. Simulation results show that the sensing performance of the proposed scheme is much better than that of the traditional one bit hard combination scheme and almost the same as that of the equal gain combination(EGC) scheme. Moreover,compared with the traditional one bit hard combination,fewer average sensing bits are required to transmit to the data fusion center with the proposed method.

Hard X-Ray Modulation Telescope(HXMT) Mission

The HXMT mission concept consists of a slat-collimated hard X-ray detector assembly sensitive in 20～250 keV with a collection area of about 5000 cm2. Based on the reconstruction technique by direct demodulation developed in recent years, HXMT is mainly devoted to performing a hard X-ray all-sky imaging survey with both high sensitivity and high spatial resolution. It can also be used to make pointed observations of X-ray sources to study their spectroscopic and temporal properties in details. The main detector of HXMT consists of 18 individual cylindrical NaI(T1)/CsI(Na) phoswich modules, each with anarea of 283.5 cm2 and a field of view of 5.7°× 1.1° (FWHM). Its spatial resolution and position accuracy are 5′ and 1′ by using the direct demodulation in 1994, and in 2000 its feasibility and technical demonstration study was selected as a project under the Major State Basic Research Program of China. In October 2005, this project entered the full design phase and was listed as a candidate for the first dedicated astronomy satellite around 2010. We are now also considering secondary low energy instruments for this satellite.

Status of the Hard X-ray Modulation Telescope Project

The Hard X-ray Modulation Telescope(HXMT) is China's first astronomical satellite.It will perform a broad band(1–250 keV) scan survey and do pointed observations of X-ray sources to study their spectra and multi-wavelength temporal properties. The pre-flight models of the satellites have been finished, and the flight models are in production. The expected launch date of HXMT is in late 2015.

Spectrometer of hard X-ray imager payload onboard the ASO-S mission

A spaceborne hard X-ray spectrometer, composed of an array of 99 scintillation detectors and associated readout electronics, has been developed for the hard X-ray imager(HXI). The HXI is one of the three payloads onboard the advanced space-based solar observatory(ASO-S), which is scheduled to be launched in early 2022 as the first Chinese solar satellite. LaBr3 scintillators and photomultiplier tubes with a super bialkali cathode are used to achieve an energy resolution better than 20% at 30 keV.Further, a new multi-channel charge-sensitive readout application-specific integrated circuit guarantees high-frequency data acquisition with low power consumption. This paper presents a detailed design of the spectrometer for the engineering model of the HXI and discusses its noise and linearity performance.

High-resolution pixelated CdZnTe detector prototype system for solar hard X-ray imager

A multichannel low-noise electronic prototype system was designed for a pixelated CdZnTe detector. This system is the result of preliminary work on a solar hard X-ray imager, which is one of the three payloads for future solar observations satellite-Advanced Space-based Solar Observatory(ASO-S). A new charge-sensitive amplifier application-specific integrated circuit, VATA450.3, with an on-chip analog-to-digital converter, is used to read out 8×8 anode pixel signals. Two CdZnTe detectors with a thickness of 2 mm and 5 mm were tested. The 2-mm-thick detector achieved energy resolution better than 5%(fullwidth at half-maximum, FWHM) at 59.5 keV, and the 5-mm-thick detector had better resolution than 1.2%(FWHM) at 662 keV. The design and test results of the prototype system are discussed in this paper.

Hard X-ray focusing resolution and efficiency test with a thickness correction multilayer Laue lens

The multilayer Laue lens(MLL) is a diffractive focusing optical element which can focus hard X-rays down to the nanometer scale. In this study, a WSi_(2)/Si multilayer structure consisting of 1736 layers, with a 7.2-nm-thick outermost layer and a total thickness of 17 μm, is prepared by DC magnetron sputtering. Regarding the thin film growth rate calibration, we correct the long-term growth rate drift from 2 to 0.6%, as measured by the grazing incidence X-ray reflectivity(GIXRR). A one-dimensional line focusing resolution of 64 nm was achieved,while the diffraction efficiency was 38% of the-1 order of the MLL Shanghai Synchrotron Radiation Facility(SSRF) with the BL15U beamline.

Hard X-Ray PHA System on the HT-7 Tokamak

A new hard X-ray pulse-height analysis （PHA） system has been established on HT-7 tokamak for long pulse steady-state operation. This PHA system consists of hard X-ray diagnostics and multi-channel analysers （MCA）. The hard X-ray diagnostics consists of a vertical X-ray detector array （CdTe） and a horizontal X-ray detector array （NaI）. The hard X-ray diagnostics can provide the profile of power deposition and the distribution function of fast electron during radio frequency （RF） current drive. The MCA system is the electronic part of the PHA system, which has been modularized and linked to PC through LAN. Each module of MCA can connect with 8 X-ray detectors. The embedded Ethernet adapter in the MCA module makes the data communication between PC and MCA very convenient. A computer can control several modules of MCA through certain software and a hub. The RAM in MCA can store 1024 or more spectra for each detector and therefore the PHA system can be applied in the long pulse discharge of several minutes.

Design of Time-Resolved Shifted Dual Transmission Grating Spectrometer for the X-Ray Spectrum Diagnostics

A new time-resolved shifted dual transmission grating spectrometer （SDTGS） is designed and fabricated in this work. This SDTGS uses a new shifted dual transmission grating （SDTG） as its dispersive component, which has two sub transmission gratings with different line densities, of 2000 lines/mm and 5000 lines/mm. The axes of the two sub transmission gratings in SDTG are horizontally and vertically shifted a certain distance to measure a broad range of 0.1-5 keV time-resolved X-ray spectra. The SDTG has been calibrated with a soft X-ray beam of the synchrotron radiation facility and its diffraction efficiency is also measured. The designed SDTGS can take full use of the space on a record panel and improve the precision for measuring spatial and temporal spectrum simultaneously. It will be a promising application for accurate diagnosis of the soft X-ray spectrum in inertial confinement fusion.

Energy spectrum of multi-radiation of X-rays in a low energy Mather-type plasma focus device

The multi-radiation of X-rays was investigated with special attention to their energy spectrum in a Mather-type plasma focus device （operated with argon gas）. The analysis is based on the effect of anomalous resistances. To study the energy spectrum, a four-channel diode X-ray spectrometer was used along with a special set of filters. The filters were suitable for detection of medium range X-rays as well as hard X-rays with energy exceeding 30 keV. The results indicate that the anomalous resistivity effect during the post pinch phase may cause multi-radiation of X-rays with a total duration of 300 ± 50 ns. The significant contribution of Cu-Kα was due to the medium range X-rays, nonetheless, hard X-rays with energies greater than 15 keV also participate in the process. The total emitted X-ray energy in the forms of Cu-K and Cu-K/3 was around 0.14 ± 0.02 （J/Sr） and 0.04 ±0.01 （J/Sr）, respectively. The total energy of the emitted hard X-ray （〉 15 keV） was around 0.12± 0.02 （J/Sr）.

Improving Plasma Confinement by Controlling Hard X-Ray

Since runaway electrons and magnetohydrodynamics activity can contribute to serious damage and energy losses in tokamaks, the effect of an external electric field on runaway electrons and hard x-ray spectra is investigated. Parameters such as the plasma current, the hard x-ray photons count and the mean energy of runaway electrons are measured. Positive and negative voltages of 300 V are applied at lOms after the plasma initiation （while the plasma is forming）, at 15ms （while the plasma is stable） and at 20ms （while the plasma is fading away） to attain the most effective time of applying the external electric field. The number of hard x-ray photons has the most changes in the range of O-200 keV when the external electric fields are applied. Also in the duration of 20-30ms of plasma the greatest number of hard x-ray spectra is detected. When the external electric fields are applied, the mean energy of runaway electrons reduces significantly, especially at 15 ms （while the plasma is stab/e）.

Photon Temperatures of Hard X-Ray Emission of LHCD Plasmas in HT-7 Tokamak

A detailed study of photon temperatures （Tph） of hard X-ray emission in lower hybrid current drive （LHCD） plasmas is presented. The photon temperature increases with the increase in plasma current and decreases with the increase in plasma density. In lower hybrid power and phase scanning experiments; there is no appreciable change in the photon temperature. The numerical results based on ray-tracing calculation and Fokker-Planck solver gives reasonable explanation for the experimental observation. Both experimental and numerical results reveal that the photon temperature depends mainly on global effects of the fast electron population, synergy between the fast electron and the loop voltage and the Coulomb slowing down.

Hard X-ray in-line outline imaging for blood vessels:first generation synchrotron radiation without contrast agents in vitro

Objective: Phase-contrast X-ray imaging which reduces radiation exposure, is a promising technique for observing the inner structures of biological soft tissues without the aid of contrast agents. The present study intends to depict blood vessels of rabbits and human livers with hard X-ray in-line outline imaging without contrast agents using synchrotron radiation. Methods: All samples were fixed with formalin and sliced into 6 mm sections. The imaging experiments were performed with Fuji-IX80 films on the 4W1A light beam of the first generation synchrotron radiation in Beijing, China. The device of the experiment, which supplies a maximum light spot size of 20×10 mm was similar to that of in-line holography. The photon energy was set at 8 KeV and high quality imagines were obtained by altering the distance between the sample and the film. Results: The trees of rabbit-liver blood vessels and the curved vessels of the cirrhotic human liver were revealed on the images, where vessels < 20 μm in diameter were differentiated. Conclusion: These results show that the blood vessels of liver samples can be revealed by using hard X-ray in-line outline imaging with the first generation synchrotron radiation without contrast agents.

Detailed calibration of the PI-LCX：1300 high performance single photon counting hard x-ray CCD camera

X-ray charge-coupled-device（CCD） camera working in single photon counting mode is a type of x-ray spectrometer with high-sensitivity and superior signal-to-noise performance. In this study, two single photon counting CCD cameras with the same mode（model： PI-LCX： 1300） are calibrated with quasi-monochromatic x-rays from radioactive sources and a conventional x-ray tube. The details of the CCD response to x-rays are analyzed by using a computer program of multi-pixel analyzing and event-distinguishing capability. The detection efficiency, energy resolution, fraction of multi-pixel events each as a function of x-ray energy, and consistence of two CCD cameras are obtained. The calibrated detection efficiency is consistent with the detection efficiency from Monte Carlo calculations with XOP program. When the multi-pixel event analysis is applied, the CCDs may be used to measure x-rays up to 60 ke V with good energy resolution（E /？E ≈ 100 at60 ke V）. The difference in detection efficiency between two CCD cameras is small（5.6% at 5.89 ke V）, but the difference in fraction of the single pixel event between them is much larger（25% at 8.04 ke V）. The obtained small relative error of detection efficiency（2.4% at 5.89 ke V） makes the high accurate measurement of x-ray yield possible in the laser plasma interaction studies. Based on the discrete calibration results, the calculated detection efficiency with XOP can be used for the whole range of 5 ke V–30 ke V.

High-rate electrochemical H_(2)O_(2) production over multimetallic atom catalysts under acidic–neutral conditions

Hydrogen peroxide(H_(2)O_(2))production by the electrochemical 2-electron oxygen reduction reaction(2e−ORR)is a promising alternative to the energy-intensive anthraquinone process,and single-atom electrocatalysts show the unique capability of high selectivity toward 2e−ORR against the 4e−one.The extremely low surface density of the single-atom sites and the inflexibility in manipulating their geometric/electronic configurations,however,compromise the H_(2)O_(2) yield and impede further performance enhancement.Herein,we construct a family of multiatom catalysts(MACs),on which two or three single atoms are closely coordinated to form high-density active sites that are versatile in their atomic configurations for optimal adsorption of essential*OOH species.Among them,the Cox–Ni MAC presents excellent electrocatalytic performance for 2e−ORR,in terms of its exceptionally high H_(2)O_(2) yield in acidic electrolytes(28.96 mol L^(−1) gcat.^(−1) h^(−1))and high selectivity under acidic to neutral conditions in a wide potential region(>80%,0–0.7 V).Operando X-ray absorption and density functional theory analyses jointly unveil its unique trimetallic Co2NiN8 configuration,which efficiently induces an appropriate Ni–d orbital filling and modulates the*OOH adsorption,together boosting the electrocatalytic 2e−ORR capability.This work thus provides a new MAC strategy for tuning the geometric/electronic structure of active sites for 2e−ORR and other potential electrochemical processes.

Geant4 simulation of fast-electron bremsstrahlung imaging at the HL-3 tokamak

To further research on high-parameter plasma,we plan to develop a two-dimensional hard X-ray(HXR)imaging system at the HL-3 tokamak to measure HXRs with energies ranging from 20 to 300 keV.The application of an array-structured detector ensures that this system can measure HXR-radiation spectra from the entire plasma cross section.Therefore,it is suitable for the study of fast-electron physics,such as radio-frequency wave current drives,fast electrons driving instabilities,and plasma disruptions in fusion research.In this study,we develop a simulation for calculating fast-electron bremsstrahlung in the HL-3 tokamak based on the Monte Carlo simulation code Geant4,in which the plasma geometry and forward scattering of fast-electron bremsstrahlung are considered.The preliminary calculation results indicate that the HXR energy deposi-tion on the detector is symmetrically distributed,even though the plasma distribution is asymmetric owing to the toroidal effect.These simulation results are helpful in constructing the relationship between the energy deposition on the detector and parameter distribution on the plasma cross section during HL-3 experiments.This is beneficial for the reconstruction of the fast-electron-distribution function and for optimizing the design of the HXR-imaging system.

渗氮层深度检验方法对比

本文采用金相法、硬度法、热染法、淬火法以及能谱仪测量5种方法对21CrMoVA、25Cr2MoVA、38CrMoAlA、X20Cr13材料渗层深度进行测定。结果表明:金相法、热染法、淬火法、能谱仪测量与硬度法测量的结果差别不大,其中能谱仪测量的结果总体来说与硬度法(仲裁方法)的差值最小。

Monte Carlo simulation for bremsstrahlung and photoneutron yields in high-energy x-ray radiography

This paper reports on the results of calculations using a Monte Carlo code （MCNP5） to study the properties of photons, electrons and photoneutrons obtained in the converted target and their transportations in x-ray radiography. A comparison between measurements and calculations for bremsstrahlung and photoneutrons is presented. The radiographic rule and the effect of the collimator on the image are studied with the experimental model. The results provide exact parameters for the optimal design of radiographic layout and shielding systems.

Broadband time-resolved elliptical crystal spectrometer for X-ray spectroscopic measurements in laser-produced plasmas

The X-ray spectrometer used in high-energy-density plasma experiments generally requires both broad X-ray energy coverage and high temporal, spatial, and spectral resolutions for overcoming the difficulties imposed by the X-ray back- ground, debris, and mechanical shocks. By using an elliptical crystal together with a streak camera, we resolve this issue at the SG-II laser facility. The carefully designed elliptical crystal has a broad spectral coverage with high resolution, strong rejection of the diffuse and/or fluorescent background radiation, and negligible source broadening for extended sources. The spectra that are Bragg reflected （23° 〈 θ 〈 38°） from the crystal are focused onto a streak camera slit 18 mm long and about 80 μm wide, to obtain a time-resolved spectrum. With experimental measurements, we demonstrate that the quartz（1011） elliptical analyzer at the SG-II laser facility has a single-shot spectral range of （4.64-6.45） keV, a typical spectral resolution of E/△E = 560, and an enhanced focusing power in the spectral dimension. For titanium （Ti） data, the lines of interest show a distribution as a function of time and the temporal variations of the He-α and Li-like Ti satellite lines and their spatial profiles show intensity peak red shifts. The spectrometer sensitivity is illustrated with a temporal resolution of better than 25 ps, which satisfies the near-term requirements of high-energy-density physics experiments.