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福建姜黄挥发油化学成分的HS-SPME-GC-MS分析 被引量:17
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作者 强悦越 韦航 +4 位作者 方灵 吴妙鸿 谭索 曾绍校 傅建炜 《中国食品添加剂》 CAS 2020年第1期147-153,共7页
采用水蒸气蒸馏法提取福建姜黄挥发油,应用顶空固相微萃取进样结合气相色谱-串联质谱联用技术(HS-SPME-GC-MS)分析姜黄挥发油的化学成分。结果表明:姜黄挥发油含有量为7.2%(mL/g),从姜黄挥发油中共分出62个色谱峰,初步鉴定出了其中的51... 采用水蒸气蒸馏法提取福建姜黄挥发油,应用顶空固相微萃取进样结合气相色谱-串联质谱联用技术(HS-SPME-GC-MS)分析姜黄挥发油的化学成分。结果表明:姜黄挥发油含有量为7.2%(mL/g),从姜黄挥发油中共分出62个色谱峰,初步鉴定出了其中的51种化学成分,占总挥发油总量的98.41%。在鉴定的化合物中,主要为单萜类化合物和倍半萜类化合物,其中新发现一种主要成分为β-柏木烯,相对含量占比高达26.58%,这可作为福建姜黄挥发油的特征成分和主要品质指标。本研究结果将为福建姜黄植物药材的品质评价提供科学依据。 展开更多
关键词 姜黄挥发油 顶空固相微萃取技术(Head space solid phase micro-extraction hs-spme) 气相色谱-质谱联用技术(Gas chromatography-mass spectrometry gc-ms) 化学成分
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Determination of Aromatic Components of Rosa davurica Pall. by Headspace Solid Phase Microextraction Combined with GC-MS 被引量:5
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作者 Yuan NIU Qiong XU +4 位作者 Jian ZHUANG Yude WANG Lilan DAI Dengfei LI Yalan ZHAO 《Medicinal Plant》 CAS 2018年第5期20-22,26,共4页
[Objectives] To determine the aromatic components of Rosa davurica Pall. [Methods] 42 kinds of aromatic components were identified from the flowers of R. davurica by headspace solid phase microextraction( HS-SPME) com... [Objectives] To determine the aromatic components of Rosa davurica Pall. [Methods] 42 kinds of aromatic components were identified from the flowers of R. davurica by headspace solid phase microextraction( HS-SPME) combined with gas chromatography-mass spectrometry( GC-MS). The main compounds were alcohols( 54. 88%) and aldehydes( 19. 55%). [Results] The top five components with the highest relative content were phenylethyl alcohol( 12. 69%),geraniol( 9. 85%),citronellol( 8. 80%),nerol( 7. 84%) and 2-n-pentylfuran( 7. 45%). [Conclusions] Headspace solid phase microextraction( HS-SPME) combined with gas chromatography-mass spectrometry( GC-MS) can provide basis for further development and utilization of R. davurica. 展开更多
关键词 Rosa davurica Pall. HEADSPACE solid phase MICROEXTRACTION (hs-spme) Gas chromatography-mass spectrometry (gc-ms) AROMATIC COMPONENTS
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Determination of Volatile Constituents,Total Flavonoids and Total Polysaccharides in the Roots of Artemisia argyi Levl. et Van. var.argyi cv. Qiai 被引量:1
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作者 Min GONG Jinqing LU +5 位作者 Yushuo XIAO Jiamin MENG Jingling HUANG Mengfei LIU Jiaxuan XIA Yi ZHOU 《Medicinal Plant》 2017年第6期1-4,9,共5页
[Objectives] To analyze the volatile components,the contents of total flavonoids and total polysaccharides of the roots of Artemisia argyi Levl. et Van. var. argyi cv. Qiai,and to provide a scientific basis for the co... [Objectives] To analyze the volatile components,the contents of total flavonoids and total polysaccharides of the roots of Artemisia argyi Levl. et Van. var. argyi cv. Qiai,and to provide a scientific basis for the comprehensive development and utilization of the resources.[Methods]The volatile components of the roots were extracted by solid phase micro-extraction( SPME),and its volatile components were analyzed by gas chromatography-mass spectrometry( GC-MS); the contents of total flavonoids and total polysaccharides in the samples were measured by UV-spectrophotometry. [Results] 44 peaks were isolated from the roots and 30 components were identified,accounting for 80. 9% of the total volatile components; the content of total flavonoids in the roots was 9. 42%; the content of total polysaccharides in the roots was 11. 05%.[Conclusions] After a comprehensive investigation,the olefins in the roots generally have antibacterial activity,the contents of the total flavonoids and total polysaccharides contained in the roots were relatively high,the roots of Artemisia argyi do have broad prospects for the development. 展开更多
关键词 The ROOTS of ARTEMISIA argyi Solid phase micro-extraction(SPME) Gas chromatography-mass spectrometry(gc-ms) TOTAL flavonoids TOTAL POLYSACCHARIDES
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Effects of Grafting on Volatile Compounds in Bitter Gourd Fruit
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作者 Ziji LIU Yu NIU +1 位作者 Renbo YU Yan YANG 《Agricultural Biotechnology》 CAS 2022年第4期113-115,123,共4页
[Objectives]This study was conducted to explore the effects of grafting on volatile compounds in bitter gourd fruit.[Methods]The volatile compounds and relative contents of grafted and non-grafted fruit were analyzed ... [Objectives]This study was conducted to explore the effects of grafting on volatile compounds in bitter gourd fruit.[Methods]The volatile compounds and relative contents of grafted and non-grafted fruit were analyzed by headspace solid phase micro-extraction with gas chromatography-mass spectrometry.[Results]There were 59 volatile compounds in Haiyan No.2S,including six unique compounds.There were 58 volatile compounds in Haiyan No.2J,including five unique compounds.[Conclusions]This study provides a scientific basis for further analysis of bitter gourd flavor regulation mediated by grafting. 展开更多
关键词 Bitter gourd GRAFTING Volatile compounds Headspace solid phase micro-extraction(hs-spme) Gas chromatography-mass spectrometry(gc-ms)
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