Aggregation of CeAlO_(3) inclusions in heavy ingot of a steel containing 0.007% aluminum

The distribution of inclusions at the bottom of a Ce-treated heavy steel ingot was detected and calculated.The three-dimensional morphology and spatial distribution of CeAlOs clusters were characterized using the electrolytic extraction and Micro-CT detection.A model of inclusion collision to predict the aggregation of CeAlO_(3) inclusions in the ingot was established and validated by measured results.Inclusions were mainly CeAlO_(3) and a small amount of Ce_(2)O_(2)S in the tundish after cerium treatment.The collision and aggregation of inclusions led to the formation of large clusters in the ingot during the solidification process.Large slag entrainment inclusions,large CeAO_(3) clusters and small CeAlO_(3) particles were observed from the center to the edge of the ingot bottom.Large inclusions were mainly concentrated at the center.The number density of inclusions larger than 200μm was 0.21 mm^(-3).The maximum diameter of CeA1O_(3) clusters was 1340μm.From the edge to the radial center and from the bottom to the top,the average diameter of inclusions gradually increased due to the longer solidification time of the ingot.

Formation mechanism of shrinkage and large inclusions of a 70t 12Cr2Mo1 heavy steel ingot

Shrinkage cavities and large inclusions are serious internal defects of heavy steel ingot and influence the quality of subsequent forgings. In order to remove these two types of defects, a 70 t 12Cr2Mo1 heavy ingot fabricated by vacuum carbon de-oxidation process was sectioned and investigated by means of structure observation and EDS analysis. To further study the forming mechanism of shrinkage and inclusion defects and find possible solutions, simulation on pouring and solidification processes was also carried out using Fluent and ProCAST software, respectively. Results show that the shrinkage defects do not appear in the middle-upper part of the ingot. The critical value of shrinkage cavity criterion is ascertained as 0.013 on the basis of sectioning investigation and simulation results, which can be used in computer simulation to predict and avoid shrinkage defects in production of 12Cr2Mo1 ingots with different weights. However, large inclusions are found at the bottom of the ingot body. The bad thermal conditions of the ingot surface and large amount of entrained slag are the main origin of the large inclusions. The simulation result of the pouring process shows that large inclusions may be eliminated by combined measures of improving the top thermal condition and controlling the height of rudimental molten steel in the ladle to above 300 mm.

Phenomena at three-phase electroslag remelting

The electroslag remelting(ESR)process is widely used to produce high-quality ingots and billets for high-alloyed steels and alloys.Both the single-phase and three-phase alternating current diagram with bifilar and monofilar connection are in use for heavy ingot manufacturing.The numerical simulation of the three-phase bifilar circuit for the 120 t three-phase bifilar six-electrode ESR furnace at different variants of electric connection was presented and discussed.At the bifilar diagram of power supply,the geometrical location of electrodes in a mould holds critical importance for performances:the close location of bifilar pair electrodes provides the highest heat productivity,but the equidistant location of electrodes gives a much more uniform heat distribution.The monofilar mulit-electrode diagram of three-phase connection without phase shift shows the most uniform distribution of potential and heat generation as well as a favorable magnetic field that makes this kind the most promising for providing a high quality of heavy ingots.

Effects of Thermal Gradients and Rotational Flows on Grain Growth in 22 t Steel Ingots

Heavy ingots are widely used in many industrial fields. The coarse grains formed during the process of in- got solidification influence the properties and fracture behaviors of the final products. The coarse grain growth was simulated under different thermal gradients. A 30Cr2Ni4MoV steel ingot was melted in a cubic crucible with dimen-sions of 15 cm×10 cm×23 cm, and the cooling conditions on each side of the crucible were controlled by different thermal curves. The influences of thermal gradients and rotational flows on grain growth in heavy steel ingots were then investigated both numerically and experimentally. The results showed that when the amplitude of the rotation angle was 60°, the metal was solidified under a reciprocating horizontal rotational condition when the angular velocity was 10 （°）/s or 20 （°）/s. As the thermal gradient increased, the lengths of the primary columnar grains in- creased, and the diameters of equiaxed grains decreased. When the direction of flow rotation was perpendicular to the direction of grain growth, the columnar grain zone was nearly eliminated, and the average diameter of equiaxed grains was 0.5 mm.

Improving ingot homogeneity by modified hot-top pulsed magneto-oscillation

Heavy ingots,especially the ingot of more than 10 t,often contain detrimental heterogeneous defects,such as macrosegregation,shrinkage pipes,and cracks.Hot-top pulsed magneto-oscillation(HPMO)can refine the solidified structure of ingot and improve their homogeneity.However,it may exacerbate the positive segregation at the upper part of the ingot body.Thus,a round table HPMO riser with a feeding part was designed,and the microstructure and macrosegregation of Al–Si alloy ingots solidified with and without HPMO were investigated.The simulation and experimental results indicated that round table HPMO riser could enable fine and uniform solidified structures in the whole ingot body;in the meantime,feeding part allowed the melt with enriched solute to gather in the upper part of the riser until the last solidification stage of ingot.This provides an effective approach for obtaining highly homogenized ingots.