316L stainless steel samples, as a widespread used material, were irradiated with HIPIB at the beam parameters of ion energy 300 keV, current density 100, 200 and 300 A/cm2, shot number 10 and pulse duration 75 ns. Th...316L stainless steel samples, as a widespread used material, were irradiated with HIPIB at the beam parameters of ion energy 300 keV, current density 100, 200 and 300 A/cm2, shot number 10 and pulse duration 75 ns. The surface morphology and the phase structure in the near surface region of original and treated samples were analyzed with scanning electron microscopy (SEM) and X-ray diffractometry (XRD). It is shown that the HIPIB irradiation can smooth the surface of the samples, and the preferred orientation is present in the surface layer of irradiated coupons. The influence of HIPIB irradiation on the oxidation behavior of 316L stainless steel at 700℃for up to 100 h was investigated. Electron probe microanalysis (EPMA) was used to study the distribution of elements in the oxidation products. It is found that the oxidation behavior of the irradiated coupons depends greatly on the ion current density of HIPIB. HIPIB irradiation with ion current density of 100 A/cm2 slightly reduces the oxidation rate with respect to the unirradiated coupon. The improvement of the oxidation resistance can be attributed to more oxide of Cr that forms on the surface of the irradiated coupons. In contrast, HIPIB irradiation with ion current density of 200 or 300 A/cm2 is proved to be detrimental, causing a higher oxidation rate.展开更多
The structural and phase transformations occurring in the near-surface layers of pre-quenched W6Mo5Cr4V2 high-speed steel (HSS) subjected to intensity pulsed ion beam (IPIB) melting have been investigated. The effect ...The structural and phase transformations occurring in the near-surface layers of pre-quenched W6Mo5Cr4V2 high-speed steel (HSS) subjected to intensity pulsed ion beam (IPIB) melting have been investigated. The effect of IPIB irradiation on wear resistance of the HSS has also been studied. The IPIB consists mainly of Cn+(30%)^0 H+(70%), with a high beam current density of 80A/cm2, acceleration voltage of 250kV, pulse duration of 70 ns. Samples were bombarded with 1, 3, 5 pulses respectively. It has been revealed that after IPIB irradiation the initial martensite in the near-surface layer of HSS changed into austenite and produced residual stresses by using electron microscopy and X-ray diffraction. Redistribution and interlace of dislocations in the irradiated samples were generated under the impact of shock wave. With increasing pulse times gradual liquid-phase dissolution of M6C carbide particles occurs in the near-surface layer and produces nanocrystalline MC. This process results in the decrease of martensite crystal (a-phase) and increase of austenite (y-phase) content and the dispersed carbide. Wear resistance of the HSS is improved by a factor of 2, which is explained by the formation of metastable phases such nanocrystal and residual stresses and the redistribution and interlace of dislocations.展开更多
基金Project (2003AA305610) supported by the Hi-tech Research and Development Program of China
文摘316L stainless steel samples, as a widespread used material, were irradiated with HIPIB at the beam parameters of ion energy 300 keV, current density 100, 200 and 300 A/cm2, shot number 10 and pulse duration 75 ns. The surface morphology and the phase structure in the near surface region of original and treated samples were analyzed with scanning electron microscopy (SEM) and X-ray diffractometry (XRD). It is shown that the HIPIB irradiation can smooth the surface of the samples, and the preferred orientation is present in the surface layer of irradiated coupons. The influence of HIPIB irradiation on the oxidation behavior of 316L stainless steel at 700℃for up to 100 h was investigated. Electron probe microanalysis (EPMA) was used to study the distribution of elements in the oxidation products. It is found that the oxidation behavior of the irradiated coupons depends greatly on the ion current density of HIPIB. HIPIB irradiation with ion current density of 100 A/cm2 slightly reduces the oxidation rate with respect to the unirradiated coupon. The improvement of the oxidation resistance can be attributed to more oxide of Cr that forms on the surface of the irradiated coupons. In contrast, HIPIB irradiation with ion current density of 200 or 300 A/cm2 is proved to be detrimental, causing a higher oxidation rate.
文摘The structural and phase transformations occurring in the near-surface layers of pre-quenched W6Mo5Cr4V2 high-speed steel (HSS) subjected to intensity pulsed ion beam (IPIB) melting have been investigated. The effect of IPIB irradiation on wear resistance of the HSS has also been studied. The IPIB consists mainly of Cn+(30%)^0 H+(70%), with a high beam current density of 80A/cm2, acceleration voltage of 250kV, pulse duration of 70 ns. Samples were bombarded with 1, 3, 5 pulses respectively. It has been revealed that after IPIB irradiation the initial martensite in the near-surface layer of HSS changed into austenite and produced residual stresses by using electron microscopy and X-ray diffraction. Redistribution and interlace of dislocations in the irradiated samples were generated under the impact of shock wave. With increasing pulse times gradual liquid-phase dissolution of M6C carbide particles occurs in the near-surface layer and produces nanocrystalline MC. This process results in the decrease of martensite crystal (a-phase) and increase of austenite (y-phase) content and the dispersed carbide. Wear resistance of the HSS is improved by a factor of 2, which is explained by the formation of metastable phases such nanocrystal and residual stresses and the redistribution and interlace of dislocations.
