Sm-Fe alloy films were electrodeposited in a high static magnetic field with the magnetic flux is perpendicular to the electric current.The samples were prepared on Cu substance in an aqueous solution by constant volt...Sm-Fe alloy films were electrodeposited in a high static magnetic field with the magnetic flux is perpendicular to the electric current.The samples were prepared on Cu substance in an aqueous solution by constant voltage method.The magnetic flux density used in the experiments were 0 T,2 T and 4 T,respectively.The microstructures,preferential orientation,composition of samples were characterized by SEM(equipped with EDS),AFM and XRD,respectively.The results showed that the thickness of films increased,whereas the concentration of Sm in films ascended first and then descended with the increasing of the flux density.The crystal grains were coarsened under the magnetic fields.The morphology of grains changed from granular at 0 T,to rough at 2 T and to cauliflower like at 4 T.The AFM results confirmed the different roughness of samples.However,the external field has not influenced the orientation of samples significantly.展开更多
文摘Sm-Fe alloy films were electrodeposited in a high static magnetic field with the magnetic flux is perpendicular to the electric current.The samples were prepared on Cu substance in an aqueous solution by constant voltage method.The magnetic flux density used in the experiments were 0 T,2 T and 4 T,respectively.The microstructures,preferential orientation,composition of samples were characterized by SEM(equipped with EDS),AFM and XRD,respectively.The results showed that the thickness of films increased,whereas the concentration of Sm in films ascended first and then descended with the increasing of the flux density.The crystal grains were coarsened under the magnetic fields.The morphology of grains changed from granular at 0 T,to rough at 2 T and to cauliflower like at 4 T.The AFM results confirmed the different roughness of samples.However,the external field has not influenced the orientation of samples significantly.
