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Research on casing deformation prevention technology based on cementing slurry system optimization
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作者 Yan Yan Meng Cai +3 位作者 Wen-Hai Ma Xiao-Chuan Zhang Li-Hong Han Yong-Hong Liu 《Petroleum Science》 SCIE EI CAS CSCD 2024年第2期1231-1240,共10页
The casing deformation prevention technology based on the optimization of cement slurry is proposed to reduce the casing deformation of shale oil and gas wells during hydraulic fracturing. In this paper, the fracture ... The casing deformation prevention technology based on the optimization of cement slurry is proposed to reduce the casing deformation of shale oil and gas wells during hydraulic fracturing. In this paper, the fracture mechanism of hollow particles in cement sheath was firstly analyzed by discrete element method, and the effect of hollow particles in cement on casing deformation was investigated by laboratory experiment method. Finally, field test was carried out to verify the improvement effect of the casing deformation based on cement slurry modification. The results show that the formation displacement can be absorbed effectively by hollow particles inside the cement transferring the excessive deformation away from casing. The particles in the uncemented state provide deformation space during formation slipping. The casing with diameter of 139.7 mm could be passed through by bridge plug with the diameter of 99 mm when the mass ratio of particle/cement reaches 1:4. According to the field test feedback, the method based on optimization of cement slurry can effectively reduce the risk of casing deformation, and the recommended range of hollow microbeads content in the cement slurry is between 15% and 25%. 展开更多
关键词 cement slurry Hollow ceramsite Casing deformation Formation slip Field test
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Physical model investigation on effects of drainage condition and cement addition on consolidation behavior of tailings slurry within backfilled stopes 被引量:1
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作者 Qinghai Ma Guangsheng Liu +1 位作者 Xiaocong Yang Lijie Guo 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第8期1490-1501,共12页
Estimation of stressses within the tailings slurry during self-weight consolidation is a critical issue for cost-effective barricade design and efficient backfill planning in underground mine stopes.This process requi... Estimation of stressses within the tailings slurry during self-weight consolidation is a critical issue for cost-effective barricade design and efficient backfill planning in underground mine stopes.This process requires a good understanding of self-weight consolidation behaviors of the tailings slurry within practical stopes,where many factors can have significant effects on the consolidation,including drainage condition and cement addition.In this paper,the prepared tailings slurry with different cement contents(0,4.76wt%,and 6.25wt%)was poured into1.2 m-high columns,which allowed three drainage scenarios(undrained,partial lateral drainage near the bottom part,and full lateral drainage boundaries)to investigate the effects of drainage condition and cement addition on the consolidation behavior of the tailings slurry.The consolidation behavior was analyzed in terms of pore water pressure(PWP),settlement,volume of drainage water,and residual water content.The results indicate that increasing the length of the drainage boundary or cement content aids in PWP dissipation.In addition,constructing an efficient drainage boundary was more favorable to PWP dissipation than increasing cement addition.The final stable PWP on the column floor was not sensitive to cement addition.The final settlement of uncemented tailings slurry was independent of drainage conditions,and that of cemented tailings slurry decreased with the increase in cement addition.Notably,more pore water can drain out from the cemented tailings slurry than the uncemented tailings slurry during consolidation. 展开更多
关键词 tailings backfill CONSOLIDATION slurry drainage cement content physical model test
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Development of a High-Temperature Thixotropic Cement Slurry System
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作者 Ping Lv Jiufei Liu +5 位作者 Mengran Xu Hui Tian Huajie Liu Yuhuan Bu Zhuang Cai Junfeng Qu 《Fluid Dynamics & Materials Processing》 EI 2023年第11期2907-2921,共15页
Cementing carbonate reservoirs is generally a difficult task.The so-called thixotropic cement slurry has gained considerable attention in this regard as it can help tofix some notable problems.More precisely,it can ea... Cementing carbonate reservoirs is generally a difficult task.The so-called thixotropic cement slurry has gained considerable attention in this regard as it can help tofix some notable problems.More precisely,it can easilyfill the leakage layer;moreover,its gelling strength can grow rapidly when pumping stops,thereby increasing the resistance to gas channeling,effectively preventing this undesired phenomenon in many cases.High-temperature thixotropic cement slurry systems,however,are still in an early stage of development and additional research is needed to make them a viable option.In the present study,using a self-developed composite high-temperature thixotropic additive as a basis,it is shown that the compressive strength can be adjusted by tuning the proportion of silica sand,the high-temperature retarder,fluid loss additive and dispersant(compatible with the thixotropic additive).According to the tests,the developed high-temperature thixotropic cement slurry system has a 14 d compressive strength of 29.73 MPa at 150°C,and a thickening time of 330 min when the dosage of retarder is 2%.At the same time,the rheological property,water loss,permeability,water separation rate,and settlement stability of the cement slurry system meet the requirements of cementing construction. 展开更多
关键词 High temperature resistance THIXOTROPY cement slurry system
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A Comprehensive Method for the Optimization of Cement Slurry and to Avoid Air Channeling in High Temperature and High-Pressure Conditions
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作者 Yanjun Li Wandong Zhang +3 位作者 Jiang Wu Yuhao Yang Chao Zhang Huanqiang Yang 《Fluid Dynamics & Materials Processing》 EI 2023年第5期1237-1248,共12页
Air channeling in the annulus between the casing and the cement sheath and/or between the cement sheath and formation is the main factor affecting the safe operation of natural gas wells at high temperatures and press... Air channeling in the annulus between the casing and the cement sheath and/or between the cement sheath and formation is the main factor affecting the safe operation of natural gas wells at high temperatures and pressures.Prevention of this problem requires,in general,excellent anti-channeling performances of the cement sheath.Three methods to predict such anti-channeling performances are proposed here,which use the weightless pressure of cement slurry,the permeability of cement stone and the volume expansion rate of cement sheath as input parameters.Guided by this approach,the anti-channeling performances of the cement slurry are evaluated by means of indoor experiments,and the cement slurry is optimized accordingly.The results show that the dangerous transition time of the cement slurry with optimized dosage of admixture is only 76 min,the permeability of cement stone is 0.005 md,the volume shrinkage at final setting is only 0.72%,and the anti-channeling performances are therefore maximized.The effective utilization of the optimized cement slurry in some representative wells(LD10–1-A1 and LD10–1-A2 in LD10–1 gas field)is also discussed. 展开更多
关键词 High temperature and high pressure cement slurry anti-channeling weightlessness pressure PERMEABILITY volume shrinkage
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Performance of Fiber Cement Slurry in the Oil and Gas Well Cementation 被引量:1
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作者 BuYuhuan WangRuihe +1 位作者 ChengRongchao LiYuhai 《Petroleum Science》 SCIE CAS CSCD 2005年第2期88-91,共4页
Based on a carbon fiber cement slurry system developed in the previous work, the relationship between the carbon fiber and the performance of the cement slurry was experimentally investigated. Results show that the us... Based on a carbon fiber cement slurry system developed in the previous work, the relationship between the carbon fiber and the performance of the cement slurry was experimentally investigated. Results show that the use of fiber has no effect on the slurry rheological mode, but influences its rheological behavior. When the fiber proportion ranges from 0.12% to 0.19% and the fiber length from 400 to 1,400 μm, the slurry rheological behavior can be improved. Under the normal pressure, the use of fiber can shorten the thickening time of the cement slurry. When the proportion of the constant-length fiber increases, the water loss of the cement slurry decreases first and then increases, and when the fiber length increases (the fiber proportion being kept constant), the water loss shows the same trend. This indicates that there are optimal values for the fiber length and proportion, which vary under the experimental conditions in the following respective ranges: 0.12%-0.37% and 700-1,400 μm . 展开更多
关键词 cement slurry carbon fiber rheological behavior thickening time water loss
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Analysis of the Weight Loss of High Temperature Cement Slurry 被引量:1
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作者 Kunhong Lv Zhiqiang Huang +1 位作者 Xingjie Ling Xueqin Xia 《Fluid Dynamics & Materials Processing》 EI 2022年第5期1307-1318,共12页
The weight loss of cement slurry is the main cause of early annular air channeling and accurate experimental evaluation of the law of loss change is the key to achieve compression stability and prevent this undesired ... The weight loss of cement slurry is the main cause of early annular air channeling and accurate experimental evaluation of the law of loss change is the key to achieve compression stability and prevent this undesired phenomenon.Typically,tests on the pressure loss of cement slurry are carried out for temperature smaller than 120°C,and this condition cannot simulate effectively the situation occurring in high temperature wells.For this reason,in this study a series of experimental tests have been conducted considering a larger range of temperatures,different retarders and fluid loss additives.The results show that with an increase in the temperature,the weight loss curve of cement slurry changes from a“two-stage”to a“three-stage”behavior,and the risk of channeling increases accordingly.On increasing the amount of retarder and fluid loss additive,the transition time of cement slurry displays a non-monotonic behavior(it decreases first and then increases).It is found that the optimized retarder and fluid loss additive dosage are 0.2%and 2.5%,respectively. 展开更多
关键词 cementING weight loss test weight loss law cement slurry EVALUATION anti-gas channeling
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A Cementing Technology for Shale Oil Horizontal Wells 被引量:2
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作者 Yudong Tian Gonghui Liu +6 位作者 Yue Qi Jun Li Yan Xi Wei Lian Xiaojie Bai Penglin Liu Xiaoguang Geng 《Fluid Dynamics & Materials Processing》 EI 2023年第11期2837-2845,共9页
Organic rich dark shale of Q Formation can be found in many areas(e.g.,in the North of S Basin).The shale target stratum is easy to hydrate and often undergoes spallation.Therefore,centering the casing in the horizont... Organic rich dark shale of Q Formation can be found in many areas(e.g.,in the North of S Basin).The shale target stratum is easy to hydrate and often undergoes spallation.Therefore,centering the casing in the horizontal section of the irregular borehole is relatively difficult.Similarly,achieving a good cementflushing efficiency under complex borehole conditions is a complex task.Through technologies such as centralizer,efficient preflushing,multi-stageflushing and ductile cement slurry,better performances can be achieved.In this study,it is shown that the cementing rate in the DY2H horizontal section is 97.8%,which is more than 34%higher than that of adjacent wells.This cementing matching technology for sidetracking horizontal wells can be used to improve the cementing quality of continental shale and provides a reference for future applications in thisfield. 展开更多
关键词 Shale oil sidetracking horizontal well tough cement slurry cementing technology
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Preparation of Fine Cement Slurries by Wet-Ground Using a Pneumatic Colloid Mill
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作者 袁海滨 易伟欣 于弘奕 《Journal of Donghua University(English Edition)》 EI CAS 2015年第4期594-596,608,共4页
This study aims to investigate the preparation of fine cement slurries by wet-ground using a pneumatic colloid mill. A pneumatic colloid mill was designed and produced. Furthermore,ordinary Portland cement slurries we... This study aims to investigate the preparation of fine cement slurries by wet-ground using a pneumatic colloid mill. A pneumatic colloid mill was designed and produced. Furthermore,ordinary Portland cement slurries were ground using the pneumatic colloid mill. Moreover,the fineness of ground cement slurries was studied. The particle sizes of ground cement slurries with various cumulated percent were all better than those of cement slurries before grinding. When water was used as the dispersant,the best average diameter of cement slurries was obtained by grinding for 10,and 15 min for cement slurries with water / cement ratio of 1∶ 1,and0. 9∶ 1,respectively. When ethanol was used as the dispersant,the particle sizes of all cumulated percent decreased gradually with the increasing grinding time,and the particle sizes of cumulated percent of D97 decreased rapidly with the increasing grinding time. The grinding effect of big particle sizes of cement slurries is better than that of small particle sizes. 展开更多
关键词 fine cement slurry wet-ground pneumatic colloid mill particle size distribution fineness
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Cement Slurry with Silica Flour and Metakaolin for Cementation of Oil-Wells Subject to High Temperature 被引量:1
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作者 Marcos dos Anjos Tiago Renovato +3 位作者 Pablo de Souza Dulce Melo Marcus Melo Julio Freitas 《材料科学与工程(中英文版)》 2010年第12期1-5,共5页
关键词 偏高岭土 固井泥浆 水泥浆 高温井 硅粉 X射线衍射分析 压力温度 高温高压条件
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疏松砂岩多层气藏钻井难点及优化对策
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作者 宋维春 张闯 +2 位作者 赵维超 邢星 黄成贵 《能源与节能》 2024年第2期127-132,共6页
涩北气田是典型的疏松砂岩气藏,具有纵向气层多、储层疏松非均质性强、敏感性矿物多等地质特征。利用大量的气藏地质、动态监测和钻录测资料,剖析钻井施工中存在的问题和技术难点,开展优化对策研究。结果表明:1)储层疏松、薄互层多、矿... 涩北气田是典型的疏松砂岩气藏,具有纵向气层多、储层疏松非均质性强、敏感性矿物多等地质特征。利用大量的气藏地质、动态监测和钻录测资料,剖析钻井施工中存在的问题和技术难点,开展优化对策研究。结果表明:1)储层疏松、薄互层多、矿化度高和开发后期纵向压力系统紊乱是影响优快钻井施工的主要因素;2)针对钻井施工中井控风险大、井身结构确定困难的问题,通过优化研究确定了不同气藏、不同深度、不同部位井的井身结构;3)针对比较突出的井漏问题,研发适宜的低伤害、能有效抑制黏土膨胀的MEG (甲基葡萄糖苷)钻井液体系;4)针对固井质量难以保证的问题,采用纳米基低密度水泥浆、工艺改进和精细施工等措施得以解决。认为,优化技术对策应用效果明显,解决了钻井技术难点,实现了疏松砂岩多层气藏快速安全钻井。 展开更多
关键词 疏松砂岩气藏 井身结构 固井质量 井漏 低密度水泥浆
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基于电化学阻抗谱的石灰石粉硬化水泥浆体孔结构演化研究
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作者 朱鹏飞 余熠 +7 位作者 石研然 杨恒 何旸 徐菲 蒋林华 储洪强 徐天磊 徐宁 《硅酸盐通报》 CAS 北大核心 2024年第1期35-43,共9页
为了研究大掺量(质量分数为20%以上)石灰石粉硬化水泥浆体的孔结构演化行为,本文基于电化学阻抗谱(EIS)、压汞(MIP)测试分析,探究大掺量石灰石粉对硬化水泥浆体EIS拓扑结构和孔结构参数的影响规律,并建立大掺量石灰石粉硬化水泥浆体的... 为了研究大掺量(质量分数为20%以上)石灰石粉硬化水泥浆体的孔结构演化行为,本文基于电化学阻抗谱(EIS)、压汞(MIP)测试分析,探究大掺量石灰石粉对硬化水泥浆体EIS拓扑结构和孔结构参数的影响规律,并建立大掺量石灰石粉硬化水泥浆体的微观结构等效电路,研究等效电路中元器件和孔结构参数之间的关系。结果表明:随水化龄期的延长,石灰石粉掺量对EIS拓扑结构参数中Bode角和θ_(max)的影响规律显著,大掺量石灰石粉硬化水泥浆体的孔径分布整体由大孔和毛细孔向过渡孔和凝胶孔发展演化;另外,EIS等效电路中电阻随硬化水泥浆体中毛细孔含量的增加而减小,电容随硬化水泥浆体中凝胶孔含量的增加而减小。 展开更多
关键词 石灰石粉 硬化水泥浆体 孔结构 电化学阻抗谱 等效电路
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惰性浆性能优化及固结时变规律试验研究
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作者 闵凡路 宋帮红 +1 位作者 袁大军 陈健 《混凝土》 CAS 北大核心 2024年第6期6-11,共6页
针对富水粉细砂地层中由于惰性浆凝结时间长,早期强度低等引起的地层沉降及管片上浮控制难题,开展水泥改性惰性浆配制及固结试验研究,结果表明:随水泥掺量从0增加到40 kg/m^(3),浆体凝结时间从24 h缩短到14 h,3 d强度从35 kPa提高到180 ... 针对富水粉细砂地层中由于惰性浆凝结时间长,早期强度低等引起的地层沉降及管片上浮控制难题,开展水泥改性惰性浆配制及固结试验研究,结果表明:随水泥掺量从0增加到40 kg/m^(3),浆体凝结时间从24 h缩短到14 h,3 d强度从35 kPa提高到180 kPa,显著缩短浆体凝结时间,提高早期强度,但同时降低了浆体流动性。另外,在不掺加水泥时,聚羧酸减水剂对惰性浆性能影响不大,而在掺加水泥后,聚羧酸减水剂能提高浆体流动性能,延缓凝结时间,提高强度。水泥掺量从0增加到30 kg/m^(3),浆体渗透系数降低,进而降低固结排水速率,延长孔隙水压力消散时间,减小固结排水量,使固结轴向应变减小。在同一水泥掺量下,增大固结压力提升了固结排水量,使浆体水胶比降低,无侧限抗压强度提高。 展开更多
关键词 惰性浆 流动度 凝结时间 水泥改性 渗透系数 固结
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水泥水化影响水合物层稳定性定量评价装置及影响程度的评测
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作者 马睿 步玉环 +3 位作者 路畅 柳华杰 郭胜来 郭辛阳 《钻井液与完井液》 CAS 北大核心 2024年第2期246-255,共10页
针对海洋深水水合物层在固井过程水泥水化放热对水合物分解量的影响缺乏量化评价装置及方法的问题,充分考虑固井过程中水泥浆体系与水合物层的接触方式,建立了一套模拟水合物层固井的水合物稳定性评价实验装置,该装置实现了低温高压下... 针对海洋深水水合物层在固井过程水泥水化放热对水合物分解量的影响缺乏量化评价装置及方法的问题,充分考虑固井过程中水泥浆体系与水合物层的接触方式,建立了一套模拟水合物层固井的水合物稳定性评价实验装置,该装置实现了低温高压下水合物的生成、带压条件下水泥浆与水合物层接触的流动泵入,直观地测试了与水合物层直接接触下的水泥浆水化放热对地层温度、压力的影响。根据设计的实验装置,通过对水合物饱和度、水合物分解气量的推导计算,建立了一套水合物模拟地层的制作方法,并建立了水泥浆水化影响水合物层稳定性评价方法。根据南海地区浅层地质条件建立了模拟水合物地层,泵入G级油井水泥净浆、低密水泥浆体系和低热水泥浆体系等3组水泥浆体系,得出单位体积油井水泥候凝过程中分解水合物的气体的量分别为0.7356、0.1091和0.0649 mol/L,且评测表明,低热水泥浆体系能够大幅度缩短固井候凝的等待时间。该研究为油气固井过程中对浅层水合物的影响提供了直观测试方法,也证明了海洋深水水合物地层中使用低热水泥浆体系的必要性。 展开更多
关键词 模拟地层 水合物分解 流体带压泵入 评价方法 水泥浆体系
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基于紧密堆积理论的深水低密度三元固相水泥浆体系
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作者 郑少军 谷怀蒙 +7 位作者 刘天乐 陈宇 蒋国盛 王韧 代天 秦榜伟 徐浩 万涛 《天然气工业》 EI CAS CSCD 北大核心 2024年第2期122-131,共10页
深水浅表层固井作业过程中由于海底低温导致水泥环早期力学强度发展缓慢、内部密实度不高,易引发水气窜流,进而导致固井质量低劣甚至密封失效等复杂情况。为此,采用分形特征方程对G级油井水泥、纳米CaCO_(3)(NC)和漂珠(CS)进行紧密堆积... 深水浅表层固井作业过程中由于海底低温导致水泥环早期力学强度发展缓慢、内部密实度不高,易引发水气窜流,进而导致固井质量低劣甚至密封失效等复杂情况。为此,采用分形特征方程对G级油井水泥、纳米CaCO_(3)(NC)和漂珠(CS)进行紧密堆积,然后结合室内实验评价,优选出了一套密度为1.50 g/cm^(3)的具有低温早强性能的三元固相水泥浆体系,并利用抗压强度测试、XCT、SEM等方法对紧密堆积体系的增强机理进行了表征和分析。研究结果表明:(1)三元紧密堆积体系早期力学强度发展快速,在10℃的低温条件下,24 h抗压强度可达3.5 MPa以上;(2)相比于相同密度的NC二元体系和CS二元体系,孔隙率降低了19.10%~33.05%,抗压强度提高了7.0%~21.1%;(3) NC可以为水泥水化提供成核位点、填充细化孔隙,CS可以部分替代水而提高体系致密性,在两种材料的协同作用和紧密堆积效应下可实现早期力学强度的快速发展。结论认为,三元固相级配水泥浆体系利用紧密堆积理论发挥了3种材料的各自优势,进而实现了早期力学强度的快速发展,对于深水井表层套管固井作业防止水气窜流具有很好的理论指导意义和应用推广价值。 展开更多
关键词 深水 低温 低密度固井水泥浆 分形理论 抗压强度
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固井水泥浆共聚物类耐高温降失水剂的制备及其机理探究
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作者 唐雷 乔东宇 +3 位作者 王新东 代红 邓程文 石伟 《石油化工》 CAS CSCD 北大核心 2024年第7期1012-1019,共8页
以2-丙烯酰胺-2-甲基丙磺酸(AMPS)、丙烯酰胺(AM)、丙烯酸(AA)、N-乙烯基吡咯烷酮(NVP)为单体,通过自由基共聚制备了降失水剂FLA。考察了适宜的合成条件,利用FTIR,1H NMR,GPC,TG-DTG对FLA的结构等进行了表征,并研究了含FLA的水泥浆性能... 以2-丙烯酰胺-2-甲基丙磺酸(AMPS)、丙烯酰胺(AM)、丙烯酸(AA)、N-乙烯基吡咯烷酮(NVP)为单体,通过自由基共聚制备了降失水剂FLA。考察了适宜的合成条件,利用FTIR,1H NMR,GPC,TG-DTG对FLA的结构等进行了表征,并研究了含FLA的水泥浆性能。实验结果表明,合成FLA适宜的条件为:m(AMPS)∶m(AM)∶m(AA)∶m(NVP)=4∶3∶2∶1,反应温度50℃,pH=8,引发剂加量0.3%(w),反应时间4 h。FLA的添加降低了水泥浆的流变性能,但搭配分散剂时水泥浆的流变性能满足要求。FLA对水泥石的抗压强度无显著影响。含FLA的水泥浆具有较好的稠化性能。FLA加量为6%(w)的水泥浆在淡水中210℃下失水量小于60 mL,在18%(w)和36%(w)盐水中失水量小于100 mL。FLA各项性能均满足高温下固井技术要求。FLA可吸附在水泥颗粒表面,形成致密的吸附层,降低材料孔隙度,从而控制水泥浆过滤能力,有望应用于超深层油田固井工作中。 展开更多
关键词 固井水泥浆 四元共聚 耐高温 降失水剂 机理研究
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超低密度水泥浆固井质量改进方法研究
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作者 张常瑞 张景富 +3 位作者 朱胡佳 谢帅 谢雨辰 王建成 《中国矿业》 北大核心 2024年第5期181-186,共6页
随着油气田勘探和开发的不断深入,对于一些极低压力地层条件,有时低密度水泥浆也无法满足安全固井施工的需求,只能采用超低密度水泥浆解决平衡压力固井问题。由于现有低密度固井质量评价标准不能客观准确地反映超低密度水泥浆的真实胶... 随着油气田勘探和开发的不断深入,对于一些极低压力地层条件,有时低密度水泥浆也无法满足安全固井施工的需求,只能采用超低密度水泥浆解决平衡压力固井问题。由于现有低密度固井质量评价标准不能客观准确地反映超低密度水泥浆的真实胶结质量,因此,对超低密度水泥浆在不同养护条件下的水泥石的声学特性、力学参数等进行了实验检测,分析了影响超低密度水泥石力学及声学特性的因素及规律。研究结果表明:密度、温度、养护时间均会对超低密度水泥石的声速和抗压强度发展产生影响,其中,温度对水泥石早期影响较大,后期影响小;水泥石密度越高,声阻抗与抗压强度越高,声阻抗与弹性模量存在线性关系,与抗压强度呈指数关系;建立了超低密度水泥浆固井套管波相对声幅计算公式,研究结果为制定超低密度水泥浆固井质量评价指标提供了基础。 展开更多
关键词 超低密度 声阻抗 抗压强度 固井 水泥浆
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一种适用于油基钻井液堵漏水泥浆体系研发
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作者 王军 柳华杰 +5 位作者 王新东 殷慧 陈杰 步玉环 秦曦 王学良 《当代化工》 CAS 2024年第5期1166-1169,共4页
水泥浆堵漏是解决恶性漏失的有效措施之一,但是水泥浆在油基钻井液中难以凝结固化,致使其使用受限。从油基钻井液污染水泥浆机理出发,开发油水置换剂,并对胶凝体系和配套降失水剂和缓凝剂进行研选,开发油基钻井液堵漏水泥浆体系,并对水... 水泥浆堵漏是解决恶性漏失的有效措施之一,但是水泥浆在油基钻井液中难以凝结固化,致使其使用受限。从油基钻井液污染水泥浆机理出发,开发油水置换剂,并对胶凝体系和配套降失水剂和缓凝剂进行研选,开发油基钻井液堵漏水泥浆体系,并对水泥浆体系性能进行评价。研究表明:通过微乳液共聚法(即油相和水相同时引发聚合)制备了油水置换剂,在油井水泥中加入油水置换剂后,钻井液与水泥浆的相容性良好,水泥浆与油基钻井液体积比为50∶50的混浆体系在50℃条件下养护时间24 h,强度可达2 MPa左右,且油水置换剂具有很好的广谱性能,现场不同区域取的不同类型的油基钻井液,均发展强度;研选了配套降失水剂BXF-200LL和缓凝剂GH-9,开发出了适用于油基钻井液堵漏的水泥浆体系,油水置换剂对水泥浆稠化没有不良影响,且抗温达120℃。 展开更多
关键词 恶性漏失 油基钻井液 水泥浆堵漏 油水置换剂
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盐穴储气库老井封堵界面胶结强度试验研究
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作者 蔡楚楚 王江帅 +2 位作者 付盼 邓嵩 殷文 《石油机械》 北大核心 2024年第7期93-97,共5页
现阶段进行的水泥塞封堵界面胶结强度测试研究未考虑高温高压对其测试的影响,且大多数开展的是常温常压下水泥塞的剪切胶结强度测试。为此,设计了盐穴储气库老井封堵水泥塞综合胶结强度原位测试装置,并在80℃、15 MPa的模拟条件下,开展... 现阶段进行的水泥塞封堵界面胶结强度测试研究未考虑高温高压对其测试的影响,且大多数开展的是常温常压下水泥塞的剪切胶结强度测试。为此,设计了盐穴储气库老井封堵水泥塞综合胶结强度原位测试装置,并在80℃、15 MPa的模拟条件下,开展了不同界面、不同水泥塞长度和直径及水泥浆体系条件下的水泥塞胶结强度测试试验,明确了不同因素对胶结强度的影响规律。试验结果表明:水泥塞-岩石/套管界面的胶结强度受水泥浆体系影响较大,盐层水泥浆体系下的界面胶结强度大于盖层水泥浆体系下的界面胶结强度;水泥塞-岩石界面胶结强度略大于水泥塞-套管界面胶结强度;水泥塞-岩石/套管界面的拉伸胶结强度低于剪切胶结强度,且两者之比为0.41~0.45。研究成果可为盐穴储气库老井封堵界面密封失效的预测提供重要的理论支撑。 展开更多
关键词 盐穴储气库 界面胶结强度 水泥浆体系 水泥塞直径 水泥塞长度
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CaCl_(2)与BaCl_(2)复配对水泥浆抗负温劣化和硫酸盐侵蚀的试验研究
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作者 胡灿 杜军 +6 位作者 万勇 刘天乐 杨国坤 曲波 郑少军 寇俊辉 倪晓阳 《安全与环境工程》 CAS CSCD 北大核心 2024年第1期96-106,115,共12页
随着我国“西部大开发”和“一带一路”发展战略的深入推动,冻土区施工日渐增多,负温劣化和硫酸盐侵蚀对水泥浆性能的负面影响给工程建设带来了安全隐患。通过-20℃恒温无预养水泥浆水化试验,利用XRD、SEM、TG、CT和力学测试等手段对水... 随着我国“西部大开发”和“一带一路”发展战略的深入推动,冻土区施工日渐增多,负温劣化和硫酸盐侵蚀对水泥浆性能的负面影响给工程建设带来了安全隐患。通过-20℃恒温无预养水泥浆水化试验,利用XRD、SEM、TG、CT和力学测试等手段对水泥浆水化产物、孔隙结构、力学性质等进行分析,综合评价了CaCl_(2)-BaCl_(2)复配使用对水泥浆在负温和硫酸盐环境下水化性能的影响。试验结果表明:相比于单一使用CaCl_(2),添加BaCl_(2)不仅可以促进水泥浆水化程度,还可与SO_(4)^(2-)反应,减少高硫型水化硫铝酸钙(又称钙矾石,AFt)的生成,提升水泥浆抗硫酸盐侵蚀能力;CaCl_(2)-BaCl_(2)复配使用时BaCl_(2)的合理掺量为10wt%~15wt%,此时水泥浆具有相对最优的水化产物、孔隙结构和力学性质,其抗负温劣化和抗硫酸盐侵蚀能力也得到了显著提高。该研究结果可为冻土区工程建设提供理论参考和技术借鉴。 展开更多
关键词 水泥浆 负温劣化 硫酸盐侵蚀 CaCl_(2)-BaCl_(2)复配 水化性能评价 试验研究
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CaF_(2)污泥对硅酸盐水泥性能的影响及机理分析
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作者 胡川 杨文伟 赵环环 《硅酸盐通报》 CAS 北大核心 2024年第3期1030-1038,共9页
固废利用是实现“双碳”目标的重要途径之一。本文以固废CaF_(2)污泥为水泥掺合料,通过抗压强度、浆体流动度试验探讨了CaF_(2)污泥掺量对水泥胶凝材料性能的影响,并结合XRD、SEM及TGA-DSC等微观表征测试进行机理分析。结果表明,CaF_(2... 固废利用是实现“双碳”目标的重要途径之一。本文以固废CaF_(2)污泥为水泥掺合料,通过抗压强度、浆体流动度试验探讨了CaF_(2)污泥掺量对水泥胶凝材料性能的影响,并结合XRD、SEM及TGA-DSC等微观表征测试进行机理分析。结果表明,CaF_(2)污泥的掺加有利于提高水泥胶凝材料的早期强度,CaF_(2)污泥掺量为8%(质量分数)的胶凝材料抗压强度表现较好。CaF_(2)污泥的掺加会导致浆体流动度降低,但掺量低于10%(质量分数)时对浆体流动度影响并不显著,掺量为8%、10%(质量分数)时浆体流动度比未掺加CaF_(2)污泥时降低了3.0%。CaF_(2)污泥在胶凝材料中主要起物理效应,CaF_(2)污泥能够形成更多的结晶位点,促进水泥水化。CaF_(2)污泥掺量增加使水泥的稀释效应及团聚效应显著。掺量为8%(质量分数)的CaF_(2)污泥复合水泥的微观性能较好。 展开更多
关键词 CaF_(2)污泥 水泥 抗压强度 浆体流动度 微观机理
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