An indirect tensile testing method is proposed for characterizing low strength graphite platelet reinforced vinyl ester nanocomposites at high-strain rate. In this technique, the traditional Brazilian disk (diametrica...An indirect tensile testing method is proposed for characterizing low strength graphite platelet reinforced vinyl ester nanocomposites at high-strain rate. In this technique, the traditional Brazilian disk (diametrical compression) test method for brittle materials is utilized along with conventional split-Hopkinson pressure bars (SHPB) for evaluating cylindrical disk specimens. The cylindrical disk specimen is held snugly in between two concave end fixtures attached to the incident and transmission bars. To eliminate the complexities of conventional strain gage application, a non-contact Laser Occluding Expansion Gage (LOEG) has been adapted for measuring the diametrical transverse expansion of the specimen under high-strain rate diametrical compressive loading. Failure diagnosis using high-speed digital photography validates the viability of utilizing this indirect test method for characterizing the tensile properties of xGnP (exfoliated graphite nanoplatelets) reinforced and additional CTBN (Carboxyl Terminated Butadiene Nitrile) toughened vinyl ester based nanocomposites. Also, quasi-static indirect tensile response agrees with previous investigations conducted using the traditional dog-bone specimen in direct tensile tests. Investigation of both quasi-static and dynamic indirect tensile test responses shows the strain rate effect on the tensile strength and energy absorbing capacity of the candidate materials. The contribution of reinforcement to the tensile properties of the candidate materials is presented.展开更多
The microstructures in the electroformed copper liners of shapedcharges after high-strain-rate plastic deformation were in-vestigated by transmission electron microscopy(TEM). Meanwhile, theorientation distribution of...The microstructures in the electroformed copper liners of shapedcharges after high-strain-rate plastic deformation were in-vestigated by transmission electron microscopy(TEM). Meanwhile, theorientation distribution of the grains in the recovered slug wasexamined by the electron backscattering Kikuchipattern(EBSP)technique. EBSP analysis illustrated that unlike theas-formed electro- formed copper liners of shaped charges the grainorientations in the recovered slug are distributed along randomly allthe directions after undergoing heavily strain deformation athigh-strain rate. Optical microscopy shows a typicalrecrystallization structure, and TEM exam- ination revealsdislocation cells existed in the thin foil specimen. These resultsindicate that dynamic recovery and recrystallization occur duringthis plastic deformation process, and the associated deformationtemperature is considered to be higher than 0.6 times the meltingpoint of copper.展开更多
The as-formed and post-deformed microstructures in both electroformed and spin-formed copper liners of shaped charge were studied by optical microscopy(OM), electron backscattering Kikuchi patterns(EBSP) technique and...The as-formed and post-deformed microstructures in both electroformed and spin-formed copper liners of shaped charge were studied by optical microscopy(OM), electron backscattering Kikuchi patterns(EBSP) technique and transmission electron microscopy(TEM). The deformation was carried out at an ultra-high strain rate. OM analysis shows that the initial grains of the electroformed copper liner are finer than those of the spin-formed copper liners. Meanwhile, EBSP analysis reveals that the fiber texture exists in the electroformed copper liners, whereas there is no texture observed in the spin-formed copper liners before deformation. Having undergone high-strain-rate deformation the grains in the recovered slugs, which are transformed from both the electroformed and spin-formed copper liners, all become small. TEM observations of the above two kinds of post-deformed specimens show the existence of cellular structures characterized by tangled dislocations and subgrain boundaries consisting of dislocation arrays. These experimental results indicate that dynamic recovery and recrystallization play an important role in the high-strain-rate deformation process.展开更多
A fictitious soil pile(FSP)model is developed to simulate the behavior of pipe piles with soil plugs undergoing high-strain dynamic impact loading.The developed model simulates the base soil with a fictitious hollow p...A fictitious soil pile(FSP)model is developed to simulate the behavior of pipe piles with soil plugs undergoing high-strain dynamic impact loading.The developed model simulates the base soil with a fictitious hollow pile fully filled with a soil plug extending at a cone angle from the pile toe to the bedrock.The friction on the outside and inside of the pile walls is distinguished using different shaft models,and the propagation of stress waves in the base soil and soil plug is considered.The motions of the pile—soil system are solved by discretizing them into spring-mass model based on the finite difference method.Comparisons of the predictions of the proposed model and conventional numerical models,as well as measurements for pipe piles in field tests subjected to impact loading,validate the accuracy of the proposed model.A parametric analysis is conducted to illustrate the influence of the model parameters on the pile dynamic response.Finally,the effective length of the FSP is proposed to approximate the affected soil zone below the pipe pile toe,and some guidance is provided for the selection of the model parameters.展开更多
The microstructure evolution and impact-toughness variation of heat-affected zone（HAZ）in X80 highstrain pipeline steel were investigated via a welding thermal-simulation technique,Charpy impact tests,and scanning el...The microstructure evolution and impact-toughness variation of heat-affected zone（HAZ）in X80 highstrain pipeline steel were investigated via a welding thermal-simulation technique,Charpy impact tests,and scanning electron microscopy observations under different welding heat inputs and peak temperatures.The results indicate that when heat input was between 17 and 25kJ·cm^（-1）,the coarse-grained heat-affected zone showed improved impact toughness.When the heat input was increased further,the martensite-austenite（M-A）islands transformed from fine lath into a massive block.Therefore,impact toughness was substantially reduced.When the heat input was 20kJ·cm^（-1） and the peak temperature of the first thermal cycle was between 900 and 1300°C,a higher impact toughness was obtained.When heat input was 20kJ·cm^（-1） and the peak temperature of the first thermal cycle was 1300°C,the impact toughness value at the second peak temperature of 900°C was higher than that at the second peak temperature of 800°C because of grain refining and uniformly dispersed M-A constituents in the matrix of bainite.展开更多
文摘An indirect tensile testing method is proposed for characterizing low strength graphite platelet reinforced vinyl ester nanocomposites at high-strain rate. In this technique, the traditional Brazilian disk (diametrical compression) test method for brittle materials is utilized along with conventional split-Hopkinson pressure bars (SHPB) for evaluating cylindrical disk specimens. The cylindrical disk specimen is held snugly in between two concave end fixtures attached to the incident and transmission bars. To eliminate the complexities of conventional strain gage application, a non-contact Laser Occluding Expansion Gage (LOEG) has been adapted for measuring the diametrical transverse expansion of the specimen under high-strain rate diametrical compressive loading. Failure diagnosis using high-speed digital photography validates the viability of utilizing this indirect test method for characterizing the tensile properties of xGnP (exfoliated graphite nanoplatelets) reinforced and additional CTBN (Carboxyl Terminated Butadiene Nitrile) toughened vinyl ester based nanocomposites. Also, quasi-static indirect tensile response agrees with previous investigations conducted using the traditional dog-bone specimen in direct tensile tests. Investigation of both quasi-static and dynamic indirect tensile test responses shows the strain rate effect on the tensile strength and energy absorbing capacity of the candidate materials. The contribution of reinforcement to the tensile properties of the candidate materials is presented.
基金financially supported by the National Natural Science Foundation of China (No.59971008).
文摘The microstructures in the electroformed copper liners of shapedcharges after high-strain-rate plastic deformation were in-vestigated by transmission electron microscopy(TEM). Meanwhile, theorientation distribution of the grains in the recovered slug wasexamined by the electron backscattering Kikuchipattern(EBSP)technique. EBSP analysis illustrated that unlike theas-formed electro- formed copper liners of shaped charges the grainorientations in the recovered slug are distributed along randomly allthe directions after undergoing heavily strain deformation athigh-strain rate. Optical microscopy shows a typicalrecrystallization structure, and TEM exam- ination revealsdislocation cells existed in the thin foil specimen. These resultsindicate that dynamic recovery and recrystallization occur duringthis plastic deformation process, and the associated deformationtemperature is considered to be higher than 0.6 times the meltingpoint of copper.
基金Project(571014569) supported by the National Natural Science Foundation of China
文摘The as-formed and post-deformed microstructures in both electroformed and spin-formed copper liners of shaped charge were studied by optical microscopy(OM), electron backscattering Kikuchi patterns(EBSP) technique and transmission electron microscopy(TEM). The deformation was carried out at an ultra-high strain rate. OM analysis shows that the initial grains of the electroformed copper liner are finer than those of the spin-formed copper liners. Meanwhile, EBSP analysis reveals that the fiber texture exists in the electroformed copper liners, whereas there is no texture observed in the spin-formed copper liners before deformation. Having undergone high-strain-rate deformation the grains in the recovered slugs, which are transformed from both the electroformed and spin-formed copper liners, all become small. TEM observations of the above two kinds of post-deformed specimens show the existence of cellular structures characterized by tangled dislocations and subgrain boundaries consisting of dislocation arrays. These experimental results indicate that dynamic recovery and recrystallization play an important role in the high-strain-rate deformation process.
基金This work was supported by the Key Project of Natural Science Foundation of Zhejiang Province(No.LXZ22E080001)National Natural Science Foundation of China(Grant Nos.51779217,52178358,and 52108349)China Scholarship Council(No.202006320262).We gratefully acknowledge this support.
文摘A fictitious soil pile(FSP)model is developed to simulate the behavior of pipe piles with soil plugs undergoing high-strain dynamic impact loading.The developed model simulates the base soil with a fictitious hollow pile fully filled with a soil plug extending at a cone angle from the pile toe to the bedrock.The friction on the outside and inside of the pile walls is distinguished using different shaft models,and the propagation of stress waves in the base soil and soil plug is considered.The motions of the pile—soil system are solved by discretizing them into spring-mass model based on the finite difference method.Comparisons of the predictions of the proposed model and conventional numerical models,as well as measurements for pipe piles in field tests subjected to impact loading,validate the accuracy of the proposed model.A parametric analysis is conducted to illustrate the influence of the model parameters on the pile dynamic response.Finally,the effective length of the FSP is proposed to approximate the affected soil zone below the pipe pile toe,and some guidance is provided for the selection of the model parameters.
基金Fundamental Research Funds for the Central Universities,China(No.2232022D-13)Fundamental Research Funds for the Central Universities and Graduate Student Innovation Fund of Donghua University,China(No.CUSF-DH-D-2022034)。
文摘The microstructure evolution and impact-toughness variation of heat-affected zone（HAZ）in X80 highstrain pipeline steel were investigated via a welding thermal-simulation technique,Charpy impact tests,and scanning electron microscopy observations under different welding heat inputs and peak temperatures.The results indicate that when heat input was between 17 and 25kJ·cm^（-1）,the coarse-grained heat-affected zone showed improved impact toughness.When the heat input was increased further,the martensite-austenite（M-A）islands transformed from fine lath into a massive block.Therefore,impact toughness was substantially reduced.When the heat input was 20kJ·cm^（-1） and the peak temperature of the first thermal cycle was between 900 and 1300°C,a higher impact toughness was obtained.When heat input was 20kJ·cm^（-1） and the peak temperature of the first thermal cycle was 1300°C,the impact toughness value at the second peak temperature of 900°C was higher than that at the second peak temperature of 800°C because of grain refining and uniformly dispersed M-A constituents in the matrix of bainite.
