Aviation turbine engine oils require excellent thermal-oxidative stability because of their high-temperature environments.High-temperature bearing deposit testing is a mandatory method for measuring the thermal-oxidat...Aviation turbine engine oils require excellent thermal-oxidative stability because of their high-temperature environments.High-temperature bearing deposit testing is a mandatory method for measuring the thermal-oxidative performance of aviation lubricant oils,and the relevant apparatus was improved in the present study.Two different commercial aviation turbine engine oils were tested,one with standard performance(known as the SL oil)and the other with high thermal stability,and their thermal-oxidative stability characteristics were evaluated.After 100 h of high-temperature bearing testing,the SL oil was analyzed by using various analytical techniques to investigate its thermal-oxidative process in the bearing test,with its thermal-oxidative degradation mechanism also being discussed.The results indicate that the developed high-temperature bearing apparatus easily meets the test requirements of method 3410.1 in standard FED-STD-791D.The viscosity and total acid number(TAN)of the SL oil increased with the bearing test time,and various deposits were produced in the bearing test,with the micro-particles of the carbon deposits being sphere-like,rod-like,and sheet-like in appearance.The antioxidant additives in the oil were consumed very rapidly in the first 30 h of the bearing test,with N-phenyl-1-naphthylamine being consumed faster than dioctyldiphenylamine.Overall,the oil thermal-oxidative process involves very complex physical and chemical mechanisms.展开更多
Testing of large-sized specimens is becoming increasingly important in deep underground rock mechanics and engineering.In traditional mechanical loading,stresses on large-sized specimens are achieved by large host fra...Testing of large-sized specimens is becoming increasingly important in deep underground rock mechanics and engineering.In traditional mechanical loading,stresses on large-sized specimens are achieved by large host frames and hydraulic pumps,which could lead to great investment.Low-cost testing machines clearly always have great appeal.In this study,a new approach is proposed using thermal expansion stress to load rock specimens,which may be particularly suitable for tests of deep hot dry rock with high temperatures.This is a different technical route from traditional mechanical loading through hydraulic pressure.For the rock mechanics test system of hot dry rock that already has an investment in heating systems,this technology may reduce the cost of the loading subsystem by fully utilizing the temperature changes.This paper presents the basic principle and a typical design of this technical solution.Preliminary feasibility analysis is then conducted based on numerical simulations.Although some technical details still need to be resolved,the feasibility of this loading approach has been preliminarily confirmed.展开更多
A finite-element model of the thermosetting epoxy asphalt mixture(EAM) microstructure is developed to simulate the indirect tension test(IDT).Image techniques are used to capture the EAM microstructure which is di...A finite-element model of the thermosetting epoxy asphalt mixture(EAM) microstructure is developed to simulate the indirect tension test(IDT).Image techniques are used to capture the EAM microstructure which is divided into two phases:aggregates and mastic.A viscoelastic constitutive relationship,which is obtained from the results of a creep test,is used to represent the mastic phase at intermittent temperatures.Model simulation results of the stiffness modulus in IDT compare favorably with experimental data.Different loading directions and velocities are employed in order to account for their influence on the modulus and the localized stress of the microstructure model.It is pointed out that the modulus is not consistent when the loading direction changes since the heterogeneous distribution of the mixture internal structure,and the loading velocity affects the localized stress as a result of the viscoelasticity of the mastic.The study results can provide a theoretical basis for the finite-element method,which can be extended to the numerical simulations of asphalt mixture micromechanical behavior.展开更多
High-temperature corrosion is a serious problem for the water-wall tubes of boilers used in thermal power plants. Oxidation, sulfidation and molten salt corrosion are main corrosion ways.Thereinto, the most severe cor...High-temperature corrosion is a serious problem for the water-wall tubes of boilers used in thermal power plants. Oxidation, sulfidation and molten salt corrosion are main corrosion ways.Thereinto, the most severe corrosion occurs in molten salt corrosion environment. Materials rich in oxides formers, such as chromium and aluminum, are needed to resist corrosion in high-temperature and corrosive environment, but processability of such bulk alloys is very limited. High velocity electric arc spraying (HVAS) technology is adopted to produce coatings with high corrosion resistance. By comparison, NiCr (Ni-45Cr-4Ti) is recommended as a promising alloy coating for the water-wall tubes, which can even resist molten salt corrosion attack. In the study of corrosion mechanism, the modern material analysis methods, such as scanning electron microscopy (SEM), X-ray diffractometry (XRD) and energy dispersive spectrometry (EDS), are used. It is found that the corrosion resistances of NiCr and FeCrAI coatings are much better than that of 20g steel, that the NiCr coatings have the best anti-corrosion properties, and that the NiCr coatings have slightly lower pores than FeCrAI coatings.It is testified that corrosion resistance of coatings is mainly determined by chromium content, and the microstructure of a coating is as important as the chemical composition of the material. In addition, the fracture mechanisms of coatings in the cycle of heating and cooling are put forward. The difference of the thermal physical properties between coatings and base metals results in the thermal stress inside the coatings. Consequently, the coatings spall from the base metal.展开更多
Asphalt-rubber pavements often become dam-aged in high-temperature regions and appear rutted or wavy, and experience slippage. To improve the high-temperature performance of the asphalt-rubber mixture, technical measu...Asphalt-rubber pavements often become dam-aged in high-temperature regions and appear rutted or wavy, and experience slippage. To improve the high-temperature performance of the asphalt-rubber mixture, technical measurements, such as, the optimal adjustment of gradation, technique of composite modification, and control of compaction were investigated. An optimal adjustment of aggregate gradation based on stone matrix asphalt improves the high-temperature stability of the asphaltrubber mixture significantly. Through composite modifi- cation, the effect of asphalt-rubber modification was enhanced, and the dynamic stability and relative defor- mation indices of the asphalt-rubber mixture were improved significantly. Furthermore, compaction parame- ters had a significant influence on the high-temperature stability of the asphalt-rubber mixture. The rolling times for compacting the asphalt-rubber mixture should be controlled to within 18-20 round-trips at a molding temperature at 180℃; if the rolling time is a 12 round-trip, the compaction temperature of the asphalt-rubber mixture should be controlled between 180 and 190℃.展开更多
The sealing integrity of cement sheath in offshore wells is seriously threatened under high-temperature conditions,resulting in gas channeling and other problems.Given the lack of experimental results,in this study re...The sealing integrity of cement sheath in offshore wells is seriously threatened under high-temperature conditions,resulting in gas channeling and other problems.Given the lack of experimental results,in this study relevant samples of a cement slurry sealing section of a typical offshore high-temperature well have been prepared and analyzed.In particular,the mechanical properties have been assessed with a triaxial pressure servo instrument and a high-temperature curing kettle.The density and the Poisson’s ratio of the samples have also been tested.The stress-strain curve has been drawn to obtain the elastic modulus and the compressive strength.The rock brittleness index has been calculated according to the measured elastic modulus and the Poisson’s ratio,together with the brittleness and the compressibility of the cement samples.The test results show that the mechanical properties and bonding strength of the cement samples are optimal at 130°C,medium at 150°C,and poor at 180°C.展开更多
In this study,nitrogen doped electrochemically exfoliated reduced graphene oxide and carbon black supported platinum(Pt/Nr EGO_(2)-CB_(3))has been prepared to enhance the performance and durability of hightemperature ...In this study,nitrogen doped electrochemically exfoliated reduced graphene oxide and carbon black supported platinum(Pt/Nr EGO_(2)-CB_(3))has been prepared to enhance the performance and durability of hightemperature PEMFCs with lower Pt loading.On the one hand,Pt/Nr EGO_(2)-CB_(3)with the strong interaction between the Pt and nitrogen(N)prevent agglomeration of Pt particles and Pt particles is 5.46±1.46 nm,which is smaller than that of 6.78±1.34 nm in Pt/C.Meanwhile,ECSA of Pt/Nr EGO_(2)-CB_(3)decrease 13.65%after AST,which is much lower than that of 97.99%in Pt/C.On the other hand,the Nr EGO flakes in MEAac act as a barrier to mitigate phosphoric acid redistribution,which improves the formation of triple-phase boundaries(TPBs)and gives stable operation of the MEAacwith a lower decay rate of 0.02 mV h^(-1)within100 h.After steady-state operation,the maximum power density of Pt/Nr EGO_(2)-CB_(3)(0.411 W cm^(-2))is three times higher than that of conventional Pt/C(0.134 W cm^(-2))in high-temperature PEMFCs.After AST,the mass transfer resistance of Pt/Nr EGO_(2)-CB_(3)electrode(0.560Ωcm^(2))is lower than that in Pt/C(0.728Ωcm^(2)).展开更多
In order to investigate the high-temperature performances of the asphalt pavement hot-applied sealant, as well as to reduce failures of the sealant pullout, the softening point test and the flow test(two existing met...In order to investigate the high-temperature performances of the asphalt pavement hot-applied sealant, as well as to reduce failures of the sealant pullout, the softening point test and the flow test(two existing methods for evaluating high-temperature performances) were conducted. It was found that both tests could not accurately reflect the adhesion performances of the sealant at high temperatures. For this purpose, the adhesion test for PSAT(pressure sensitive adhesive tape) has been taken as a reference to develop a device that is suitable for evaluating the adhesion performances, by modifying relevant test parameters according to the road conditions at high temperatures. Thirteen common sealants were tested in the modified adhesion test, softening point test and f low test. The experimental results show that no significant correlation(p〉0.05) exists between the adhesion value, softening point, adhesion value and flow value; while a significant correlation(p〈0.05) exists between the softening point and flow value. The modified adhesion test is efficient in distinguishing the hightemperature adhesion performances of different sealants, and can be used as a standard method for evaluating such performances.展开更多
The anchor stress extent of a prestress anchor cable project has a direct relation with the project safety and performance. Prestressed tensioning method is a kind of nondestructive testing method, by which a reverse ...The anchor stress extent of a prestress anchor cable project has a direct relation with the project safety and performance. Prestressed tensioning method is a kind of nondestructive testing method, by which a reverse stretching load is applied on the external exposure section of anchor cable under construction or in service, and then the elongation variation of stress bars is measured to determine the anchor stress. We elaborated the theory and testing mechanism of prestressed tensioning method, and systematically studied key issues during the prestressed tensioning process of anchor cable by using physical model test, including the composition of tension stress-elongation curve, the variation of anchor stress, the compensation of locked anchor stress, and the judgment of anchor stress, and verified the theory feasibility of prestressed tensioning method. A case study on slope anchor cable of one highway project was conducted to further discuss on the test method, operation procedures and judgment of prestressed tensioning method on obtaining anchor stress, and then the test data of three situations were analyzed. The result provides a theoretical basis and technical base for the application of prestressed tensioning method to the evaluation of construction quality and operation conditions of anchor cable project.展开更多
High-temperature performance tests of chromium-containing stuffing sand for a steel ladle w ith different ratios w ere performed. A high-temperature simulation test furnace w as used to analyze the influence of the co...High-temperature performance tests of chromium-containing stuffing sand for a steel ladle w ith different ratios w ere performed. A high-temperature simulation test furnace w as used to analyze the influence of the composition ratio of ladle filler sand and sintering time on the high-temperature compression resistance of chromium-containing stuffing sand in the temperature range of 1 500- 1 600 ℃. The results show that the refractoriness of ladle filler sand w as the low est( only 1 610 ℃) w hen the composition ratio of chromite sand and silica sand w as 6∶ 4. M oreover,the high-temperature compression resistance w as high w hen the content of chromite sand w as at 70%; the resistance increased w ith increasing sintering time. When the sintering time w as extended at a temperature of 1 600 ℃,the high-temperature compression resistance of ladle filler sand first increased and then decreased after being overburnt.展开更多
With the redesigned jigs for the Thermecmastor-Z thermal simulator,the feasibility of using 3 kinds of Gleeble specimens in the Thermecmastor-Z simulator was investigated. Results show that Gleeble specimens can be us...With the redesigned jigs for the Thermecmastor-Z thermal simulator,the feasibility of using 3 kinds of Gleeble specimens in the Thermecmastor-Z simulator was investigated. Results show that Gleeble specimens can be used in the Thermecmastor-Z simulator. The tension tests in the Gleeble and Thermecmastor-Z simulators produced results with the same trend,which proves that the high temperature ductility of Gleeble specimens can be reflected by the Thermecmastor- Z simulator. In addition,as the Thermecmastor-Z simulator offers a wider heating zone,better cross-section shrinkage and elongation of specimens can be achieved under the same test conditions.展开更多
This paper discussed the setting up of a comeuter automatic system for testing the dy-namic dissociating tension of cooked cocoon filament by means of microcomputer tech-niques.The dynamic dissociating tension of two ...This paper discussed the setting up of a comeuter automatic system for testing the dy-namic dissociating tension of cooked cocoon filament by means of microcomputer tech-niques.The dynamic dissociating tension of two kinds of row cocoons with differentreelability was tested and analysed under different cocoon cooking conditions.More relia-ble data have been obtained by quantitative tests.The conclusions reached by analysingthese data are of practical significance to perfecting the cocoon cooking theory,assessingcocoon quality,improving the cocoon cooking process,etc.展开更多
The exhaust and flame from a supersonic airborne missile high-energy smoke-born engine (SAMHSE) may lead to high-temperature ablation, supersonic-erosion, dreg-adherence (HTASED) and corrosion on the launcher slide tr...The exhaust and flame from a supersonic airborne missile high-energy smoke-born engine (SAMHSE) may lead to high-temperature ablation, supersonic-erosion, dreg-adherence (HTASED) and corrosion on the launcher slide track, causing serious problems to the operation and decreasing the lifetime of the launcher. Therefore, it is imperative to study the destructive mechanism so as to guarantee the smooth operation and increase the lifetime of military equipments. Accordingly, HTASED and corrosion were systematically observed and analyzed with the emphasis placed on the mechanism investigations making use of a series evaluation tests, typical missile engine simulation tests, national military standard methods, scanning electron microscopy and electrochemical corrosion tests. It is found that the thermal impact of high-temperature flame and supersonic erosion of corrosive melting particle jet of the SAMHSE lead to surface defects of micro-cracks, denudation and corrosive residue. Some defects reach to metal base becoming to "corrosive channels". Repetitive HTASED may cause ablation-adhesion fatigue stress, which enhances the surface corrosion and destruction. HTASED and corrosion are related to the type of a SAMHSE fuel and experience of the launcher. Surface destruction is related to synergistic effects of the HTASED. The ablated and failed Al or steel surface is liable to electrochemical corrosion characterized by pitting in humid and salt-spray environment.展开更多
AIM: To investigate the reliability of a modified threedimensional distraction test(3D-DT) and three-dimensional pinch test(3D-PT) for assessing lower eyelid tension(LET).METHODS: A cross-sectional study was conducted...AIM: To investigate the reliability of a modified threedimensional distraction test(3D-DT) and three-dimensional pinch test(3D-PT) for assessing lower eyelid tension(LET).METHODS: A cross-sectional study was conducted among 97 volunteer s including 97 eyelids with no history of trauma, tumor, or reconstructive surgeries. Six three-dimensional photographs were acquired for each par ticipant, including two photographs obtained in a neutral position(NP), two using a modified 3D-DT with a 15.9-grammes stainless steel eyelid hook performed, and two using 3D-PT.RESULTS: The mean absolute differences between NP, 3D-DT, and 3D-PT measurements varied between 0.07 and 7.42, 0.10 and 13.10, and 0.07 and 15.97, respectively;technical error of measurement varied between 0.05 and 7.81, 0.09 and 10.19, and 0.07 and 12.47, respectively;and relative error measurements varied between 0.10% and 11.50%, 0.16% and 30.51%, and 0.11% and 38.75%, respectively. For intra-rater reliability, the intraclass correlation coefficients(ICCs) were more than 0.80 in seven out of eight measurements obtained in the NP and 3D-DT, whereas those obtained in the 3D-PT were as low as less than 0.30 by rater 1;the ICCs of all the measurements obtained in all the positions(NP, 3D-DT, and 3D-PT) were more than 0.80 by rater 2. For inter-rater reliability six out of eight NP and 3D-DT measurements had an ICC greater than 0.80, whereas those of 3D-PT measurements were less than 0.30. For intra-method reliability, the ICCs of all the NP measurements were more than 0.87, whereas those of the six 3D-DT measurements and four 3D-PT measurements were more than 0.80.CONCLUSION: Our study results prove that the modified 3D-DT, which involves the use of an eyelid hook, can be a highly reliable method for evaluating LET. Furthermore, this novel and simple method may be utilized as the basis for further investigation and routine pre-and postoperative clinical evaluation.展开更多
The contact pressure acting on the sheet/tools interface has been studied because of growing the concern about the wear of tools. Recent studies make use of numerical simulation software to evaluate and correlate this...The contact pressure acting on the sheet/tools interface has been studied because of growing the concern about the wear of tools. Recent studies make use of numerical simulation software to evaluate and correlate this pressure with the friction and wear generated. Since there are many studies that determine the coefficient of friction in sheet metal forming by bending under tension (BUT) test, the contact pressure between the pin and the sheet was measured using a film that has the ability to record the applied pressure. The vertical force applied to pin was also measured. The results indicate that the vertical force is more accurate to set the contact pressure that using equations predetermined. It was also observed that the contact area between the sheet and the pin is always smaller than the area calculated geometrically. The friction coefficient was determined for the BUT test through several equations proposed by various authors in order to check if there is much variation between the results. It was observed that the friction coefficient showed little variation for each equation, and each one can be used. The material used was the commercially pure aluminum, alloy Al1100.展开更多
基金supported by the National Key Research and Development Program of China(2022YFB3809005)by SINOPEC(120060-6,121027,and 122042).
文摘Aviation turbine engine oils require excellent thermal-oxidative stability because of their high-temperature environments.High-temperature bearing deposit testing is a mandatory method for measuring the thermal-oxidative performance of aviation lubricant oils,and the relevant apparatus was improved in the present study.Two different commercial aviation turbine engine oils were tested,one with standard performance(known as the SL oil)and the other with high thermal stability,and their thermal-oxidative stability characteristics were evaluated.After 100 h of high-temperature bearing testing,the SL oil was analyzed by using various analytical techniques to investigate its thermal-oxidative process in the bearing test,with its thermal-oxidative degradation mechanism also being discussed.The results indicate that the developed high-temperature bearing apparatus easily meets the test requirements of method 3410.1 in standard FED-STD-791D.The viscosity and total acid number(TAN)of the SL oil increased with the bearing test time,and various deposits were produced in the bearing test,with the micro-particles of the carbon deposits being sphere-like,rod-like,and sheet-like in appearance.The antioxidant additives in the oil were consumed very rapidly in the first 30 h of the bearing test,with N-phenyl-1-naphthylamine being consumed faster than dioctyldiphenylamine.Overall,the oil thermal-oxidative process involves very complex physical and chemical mechanisms.
基金National Natural Science Foundation of ChinaGrant/Award Number:41972316+3 种基金Sichuan Science&Technology FoundationGrant/Award Number:2022YFSY0007Joint Funds of the National Natural Science Foundation of ChinaGrant/Award Number:U2344226。
文摘Testing of large-sized specimens is becoming increasingly important in deep underground rock mechanics and engineering.In traditional mechanical loading,stresses on large-sized specimens are achieved by large host frames and hydraulic pumps,which could lead to great investment.Low-cost testing machines clearly always have great appeal.In this study,a new approach is proposed using thermal expansion stress to load rock specimens,which may be particularly suitable for tests of deep hot dry rock with high temperatures.This is a different technical route from traditional mechanical loading through hydraulic pressure.For the rock mechanics test system of hot dry rock that already has an investment in heating systems,this technology may reduce the cost of the loading subsystem by fully utilizing the temperature changes.This paper presents the basic principle and a typical design of this technical solution.Preliminary feasibility analysis is then conducted based on numerical simulations.Although some technical details still need to be resolved,the feasibility of this loading approach has been preliminarily confirmed.
基金Program for New Century Excellent Talents in University(No. NCET-08-0118)Specialized Research Fund for the Doctoral Program of Higher Education (No. 20090092110049)
文摘A finite-element model of the thermosetting epoxy asphalt mixture(EAM) microstructure is developed to simulate the indirect tension test(IDT).Image techniques are used to capture the EAM microstructure which is divided into two phases:aggregates and mastic.A viscoelastic constitutive relationship,which is obtained from the results of a creep test,is used to represent the mastic phase at intermittent temperatures.Model simulation results of the stiffness modulus in IDT compare favorably with experimental data.Different loading directions and velocities are employed in order to account for their influence on the modulus and the localized stress of the microstructure model.It is pointed out that the modulus is not consistent when the loading direction changes since the heterogeneous distribution of the mixture internal structure,and the loading velocity affects the localized stress as a result of the viscoelasticity of the mastic.The study results can provide a theoretical basis for the finite-element method,which can be extended to the numerical simulations of asphalt mixture micromechanical behavior.
文摘High-temperature corrosion is a serious problem for the water-wall tubes of boilers used in thermal power plants. Oxidation, sulfidation and molten salt corrosion are main corrosion ways.Thereinto, the most severe corrosion occurs in molten salt corrosion environment. Materials rich in oxides formers, such as chromium and aluminum, are needed to resist corrosion in high-temperature and corrosive environment, but processability of such bulk alloys is very limited. High velocity electric arc spraying (HVAS) technology is adopted to produce coatings with high corrosion resistance. By comparison, NiCr (Ni-45Cr-4Ti) is recommended as a promising alloy coating for the water-wall tubes, which can even resist molten salt corrosion attack. In the study of corrosion mechanism, the modern material analysis methods, such as scanning electron microscopy (SEM), X-ray diffractometry (XRD) and energy dispersive spectrometry (EDS), are used. It is found that the corrosion resistances of NiCr and FeCrAI coatings are much better than that of 20g steel, that the NiCr coatings have the best anti-corrosion properties, and that the NiCr coatings have slightly lower pores than FeCrAI coatings.It is testified that corrosion resistance of coatings is mainly determined by chromium content, and the microstructure of a coating is as important as the chemical composition of the material. In addition, the fracture mechanisms of coatings in the cycle of heating and cooling are put forward. The difference of the thermal physical properties between coatings and base metals results in the thermal stress inside the coatings. Consequently, the coatings spall from the base metal.
文摘Asphalt-rubber pavements often become dam-aged in high-temperature regions and appear rutted or wavy, and experience slippage. To improve the high-temperature performance of the asphalt-rubber mixture, technical measurements, such as, the optimal adjustment of gradation, technique of composite modification, and control of compaction were investigated. An optimal adjustment of aggregate gradation based on stone matrix asphalt improves the high-temperature stability of the asphaltrubber mixture significantly. Through composite modifi- cation, the effect of asphalt-rubber modification was enhanced, and the dynamic stability and relative defor- mation indices of the asphalt-rubber mixture were improved significantly. Furthermore, compaction parame- ters had a significant influence on the high-temperature stability of the asphalt-rubber mixture. The rolling times for compacting the asphalt-rubber mixture should be controlled to within 18-20 round-trips at a molding temperature at 180℃; if the rolling time is a 12 round-trip, the compaction temperature of the asphalt-rubber mixture should be controlled between 180 and 190℃.
基金The authors gratefully acknowledge the research project from Engineering Research Center of Rock-Soil Drilling&Excavation and Protection,Ministry of EducationChina University of Geosciences,Wuhan(Grant No.202106).
文摘The sealing integrity of cement sheath in offshore wells is seriously threatened under high-temperature conditions,resulting in gas channeling and other problems.Given the lack of experimental results,in this study relevant samples of a cement slurry sealing section of a typical offshore high-temperature well have been prepared and analyzed.In particular,the mechanical properties have been assessed with a triaxial pressure servo instrument and a high-temperature curing kettle.The density and the Poisson’s ratio of the samples have also been tested.The stress-strain curve has been drawn to obtain the elastic modulus and the compressive strength.The rock brittleness index has been calculated according to the measured elastic modulus and the Poisson’s ratio,together with the brittleness and the compressibility of the cement samples.The test results show that the mechanical properties and bonding strength of the cement samples are optimal at 130°C,medium at 150°C,and poor at 180°C.
基金supported by the Engineering and Physical Sciences Research Council(EPSRC)(EP/P009050/1 and EP/S021531/1)Tthe Henry Royce Institute for Advanced Materials,funded through the EPSRC grants(EP/R00661X/1,EP/S019367/1,EP/P025021/1 and EP/P025498/1)。
文摘In this study,nitrogen doped electrochemically exfoliated reduced graphene oxide and carbon black supported platinum(Pt/Nr EGO_(2)-CB_(3))has been prepared to enhance the performance and durability of hightemperature PEMFCs with lower Pt loading.On the one hand,Pt/Nr EGO_(2)-CB_(3)with the strong interaction between the Pt and nitrogen(N)prevent agglomeration of Pt particles and Pt particles is 5.46±1.46 nm,which is smaller than that of 6.78±1.34 nm in Pt/C.Meanwhile,ECSA of Pt/Nr EGO_(2)-CB_(3)decrease 13.65%after AST,which is much lower than that of 97.99%in Pt/C.On the other hand,the Nr EGO flakes in MEAac act as a barrier to mitigate phosphoric acid redistribution,which improves the formation of triple-phase boundaries(TPBs)and gives stable operation of the MEAacwith a lower decay rate of 0.02 mV h^(-1)within100 h.After steady-state operation,the maximum power density of Pt/Nr EGO_(2)-CB_(3)(0.411 W cm^(-2))is three times higher than that of conventional Pt/C(0.134 W cm^(-2))in high-temperature PEMFCs.After AST,the mass transfer resistance of Pt/Nr EGO_(2)-CB_(3)electrode(0.560Ωcm^(2))is lower than that in Pt/C(0.728Ωcm^(2)).
基金Funded by the National Natural Science Foundation of China(Nos.51378242 and 51008146)the Transportation Industry Science and Technology Project of Beijing(No.kj2013-2-14)
文摘In order to investigate the high-temperature performances of the asphalt pavement hot-applied sealant, as well as to reduce failures of the sealant pullout, the softening point test and the flow test(two existing methods for evaluating high-temperature performances) were conducted. It was found that both tests could not accurately reflect the adhesion performances of the sealant at high temperatures. For this purpose, the adhesion test for PSAT(pressure sensitive adhesive tape) has been taken as a reference to develop a device that is suitable for evaluating the adhesion performances, by modifying relevant test parameters according to the road conditions at high temperatures. Thirteen common sealants were tested in the modified adhesion test, softening point test and f low test. The experimental results show that no significant correlation(p〉0.05) exists between the adhesion value, softening point, adhesion value and flow value; while a significant correlation(p〈0.05) exists between the softening point and flow value. The modified adhesion test is efficient in distinguishing the hightemperature adhesion performances of different sealants, and can be used as a standard method for evaluating such performances.
基金Funded by the Science and Technolog Program of Ministry of Transport of P.R.China(No.2012318352100)
文摘The anchor stress extent of a prestress anchor cable project has a direct relation with the project safety and performance. Prestressed tensioning method is a kind of nondestructive testing method, by which a reverse stretching load is applied on the external exposure section of anchor cable under construction or in service, and then the elongation variation of stress bars is measured to determine the anchor stress. We elaborated the theory and testing mechanism of prestressed tensioning method, and systematically studied key issues during the prestressed tensioning process of anchor cable by using physical model test, including the composition of tension stress-elongation curve, the variation of anchor stress, the compensation of locked anchor stress, and the judgment of anchor stress, and verified the theory feasibility of prestressed tensioning method. A case study on slope anchor cable of one highway project was conducted to further discuss on the test method, operation procedures and judgment of prestressed tensioning method on obtaining anchor stress, and then the test data of three situations were analyzed. The result provides a theoretical basis and technical base for the application of prestressed tensioning method to the evaluation of construction quality and operation conditions of anchor cable project.
文摘High-temperature performance tests of chromium-containing stuffing sand for a steel ladle w ith different ratios w ere performed. A high-temperature simulation test furnace w as used to analyze the influence of the composition ratio of ladle filler sand and sintering time on the high-temperature compression resistance of chromium-containing stuffing sand in the temperature range of 1 500- 1 600 ℃. The results show that the refractoriness of ladle filler sand w as the low est( only 1 610 ℃) w hen the composition ratio of chromite sand and silica sand w as 6∶ 4. M oreover,the high-temperature compression resistance w as high w hen the content of chromite sand w as at 70%; the resistance increased w ith increasing sintering time. When the sintering time w as extended at a temperature of 1 600 ℃,the high-temperature compression resistance of ladle filler sand first increased and then decreased after being overburnt.
文摘With the redesigned jigs for the Thermecmastor-Z thermal simulator,the feasibility of using 3 kinds of Gleeble specimens in the Thermecmastor-Z simulator was investigated. Results show that Gleeble specimens can be used in the Thermecmastor-Z simulator. The tension tests in the Gleeble and Thermecmastor-Z simulators produced results with the same trend,which proves that the high temperature ductility of Gleeble specimens can be reflected by the Thermecmastor- Z simulator. In addition,as the Thermecmastor-Z simulator offers a wider heating zone,better cross-section shrinkage and elongation of specimens can be achieved under the same test conditions.
文摘This paper discussed the setting up of a comeuter automatic system for testing the dy-namic dissociating tension of cooked cocoon filament by means of microcomputer tech-niques.The dynamic dissociating tension of two kinds of row cocoons with differentreelability was tested and analysed under different cocoon cooking conditions.More relia-ble data have been obtained by quantitative tests.The conclusions reached by analysingthese data are of practical significance to perfecting the cocoon cooking theory,assessingcocoon quality,improving the cocoon cooking process,etc.
基金Project(59925513) supported by the National Natural Science Foundation of China through the Excellent Youth Scientist Fund
文摘The exhaust and flame from a supersonic airborne missile high-energy smoke-born engine (SAMHSE) may lead to high-temperature ablation, supersonic-erosion, dreg-adherence (HTASED) and corrosion on the launcher slide track, causing serious problems to the operation and decreasing the lifetime of the launcher. Therefore, it is imperative to study the destructive mechanism so as to guarantee the smooth operation and increase the lifetime of military equipments. Accordingly, HTASED and corrosion were systematically observed and analyzed with the emphasis placed on the mechanism investigations making use of a series evaluation tests, typical missile engine simulation tests, national military standard methods, scanning electron microscopy and electrochemical corrosion tests. It is found that the thermal impact of high-temperature flame and supersonic erosion of corrosive melting particle jet of the SAMHSE lead to surface defects of micro-cracks, denudation and corrosive residue. Some defects reach to metal base becoming to "corrosive channels". Repetitive HTASED may cause ablation-adhesion fatigue stress, which enhances the surface corrosion and destruction. HTASED and corrosion are related to the type of a SAMHSE fuel and experience of the launcher. Surface destruction is related to synergistic effects of the HTASED. The ablated and failed Al or steel surface is liable to electrochemical corrosion characterized by pitting in humid and salt-spray environment.
基金Supported by the Project of National Key Research and Development (No.2018YFC1106103)Chongqing Science and Health Joint Medical Research Project-Youth Project (No.2022QNXM016)The Fundamental Research Funds for the Central Universities (No.2021FZZX005-15)。
文摘AIM: To investigate the reliability of a modified threedimensional distraction test(3D-DT) and three-dimensional pinch test(3D-PT) for assessing lower eyelid tension(LET).METHODS: A cross-sectional study was conducted among 97 volunteer s including 97 eyelids with no history of trauma, tumor, or reconstructive surgeries. Six three-dimensional photographs were acquired for each par ticipant, including two photographs obtained in a neutral position(NP), two using a modified 3D-DT with a 15.9-grammes stainless steel eyelid hook performed, and two using 3D-PT.RESULTS: The mean absolute differences between NP, 3D-DT, and 3D-PT measurements varied between 0.07 and 7.42, 0.10 and 13.10, and 0.07 and 15.97, respectively;technical error of measurement varied between 0.05 and 7.81, 0.09 and 10.19, and 0.07 and 12.47, respectively;and relative error measurements varied between 0.10% and 11.50%, 0.16% and 30.51%, and 0.11% and 38.75%, respectively. For intra-rater reliability, the intraclass correlation coefficients(ICCs) were more than 0.80 in seven out of eight measurements obtained in the NP and 3D-DT, whereas those obtained in the 3D-PT were as low as less than 0.30 by rater 1;the ICCs of all the measurements obtained in all the positions(NP, 3D-DT, and 3D-PT) were more than 0.80 by rater 2. For inter-rater reliability six out of eight NP and 3D-DT measurements had an ICC greater than 0.80, whereas those of 3D-PT measurements were less than 0.30. For intra-method reliability, the ICCs of all the NP measurements were more than 0.87, whereas those of the six 3D-DT measurements and four 3D-PT measurements were more than 0.80.CONCLUSION: Our study results prove that the modified 3D-DT, which involves the use of an eyelid hook, can be a highly reliable method for evaluating LET. Furthermore, this novel and simple method may be utilized as the basis for further investigation and routine pre-and postoperative clinical evaluation.
文摘The contact pressure acting on the sheet/tools interface has been studied because of growing the concern about the wear of tools. Recent studies make use of numerical simulation software to evaluate and correlate this pressure with the friction and wear generated. Since there are many studies that determine the coefficient of friction in sheet metal forming by bending under tension (BUT) test, the contact pressure between the pin and the sheet was measured using a film that has the ability to record the applied pressure. The vertical force applied to pin was also measured. The results indicate that the vertical force is more accurate to set the contact pressure that using equations predetermined. It was also observed that the contact area between the sheet and the pin is always smaller than the area calculated geometrically. The friction coefficient was determined for the BUT test through several equations proposed by various authors in order to check if there is much variation between the results. It was observed that the friction coefficient showed little variation for each equation, and each one can be used. The material used was the commercially pure aluminum, alloy Al1100.