Hot compression bonding was first used to join oxide-dispersion-strengthened ferrite steels(14 YWT)under temperatures of 750–1100℃ with a true strain range of 0.11–0.51. Subsequently, the microstructure evolution a...Hot compression bonding was first used to join oxide-dispersion-strengthened ferrite steels(14 YWT)under temperatures of 750–1100℃ with a true strain range of 0.11–0.51. Subsequently, the microstructure evolution and mechanical properties of the joints were characterized, revealing that the 14 YWT steels could be successfully bonded at a temperature of at least 950℃ with a true strain of 0.22, without degrading the fine grain and nanoparticle distribution, and the presence of inclusions or micro-voids along the bonding interface. Moreover, the joints had nearly the same tensile properties at room temperature and exhibited a similar fracture morphology with sufficient dimples compared to that of the base material. An electron backscattered diffraction technique and transmission electron microscopy were systematically employed to study the evolution of hot deformed microstructures. The results showed that continuous dynamic recrystallization characterized by progressive subgrain rotation occurred in this alloy, but discontinuous dynamic recrystallization characterized by strain-induced grain boundary bulging and subsequent bridging sub-boundary rotation was the dominant nucleation mechanism. The nuclei will grow with ongoing deformation, which will contribute to the healing of the original bonding interface.展开更多
In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were ...In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were performed on the joints to evaluate the reliability of the joints formed.Detailed microstructural analyses suggest that two different competing dynamic recrystallization(DRX) mechanisms occur during the bonding process depending on the strain rate, and the joints obtained at different strain rate exhibits distinct healing effect.At a low strain rate(0.01 s^(-1)), continuous DRX occurs, as expected in high-stackingfault-energy materials, and is characterized by the progressive conversion of the sub-boundaries into larger-angle boundaries, which involves very limited grain boundaries migration.In addition, straininduced precipitation(SIP) is sufficient under this condition, further impeding the healing of bonding interface.Hence, the joints obtained at low strain rate fractured at the bonding interface easily.Whereas discontinuous DRX is activated at high strain rates(10 and 30 s^(-1)).Under this condition, the formation of sub-boundaries is severely suppressed, resulting in the piling-up of dislocations and hence the storage of a greater amount of stored energy for nucleation and subsequent nuclei growth via the long-distance grain boundaries migration.Meanwhile, the SIP process is sluggish, making the conditions much more favorable for grain boundaries migration which plays a key role in the healing of the original bonding interface.Thus, the joints can be successfully bonded when a high strain rate is applied, with the joints exhibiting tensile properties similar to that of the base material.展开更多
基金financial support from National Key Research and Development program (Grant No.2016YFB0300401)National Natural Science Foundation of China (Grant Nos. U1508215, 51774265)key Program of the Chinese Academy of Sciences (Grant No. ZDRW-CN-2017-1)
文摘Hot compression bonding was first used to join oxide-dispersion-strengthened ferrite steels(14 YWT)under temperatures of 750–1100℃ with a true strain range of 0.11–0.51. Subsequently, the microstructure evolution and mechanical properties of the joints were characterized, revealing that the 14 YWT steels could be successfully bonded at a temperature of at least 950℃ with a true strain of 0.22, without degrading the fine grain and nanoparticle distribution, and the presence of inclusions or micro-voids along the bonding interface. Moreover, the joints had nearly the same tensile properties at room temperature and exhibited a similar fracture morphology with sufficient dimples compared to that of the base material. An electron backscattered diffraction technique and transmission electron microscopy were systematically employed to study the evolution of hot deformed microstructures. The results showed that continuous dynamic recrystallization characterized by progressive subgrain rotation occurred in this alloy, but discontinuous dynamic recrystallization characterized by strain-induced grain boundary bulging and subsequent bridging sub-boundary rotation was the dominant nucleation mechanism. The nuclei will grow with ongoing deformation, which will contribute to the healing of the original bonding interface.
基金financial support from the National Key Research and Development Program of China(Grant No.2018YFA0702900)the National Natural Science Foundation of China(Grant Nos.U1508215,51774265)+2 种基金the Key Program of the Chinese Academy of Sciences(Grant No.ZDRW-CN-2017-1)the National Science and Technology Major Project of China(Grant No.2019ZX06004010)the CAS Interdisciplinary Innovation Team。
文摘In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were performed on the joints to evaluate the reliability of the joints formed.Detailed microstructural analyses suggest that two different competing dynamic recrystallization(DRX) mechanisms occur during the bonding process depending on the strain rate, and the joints obtained at different strain rate exhibits distinct healing effect.At a low strain rate(0.01 s^(-1)), continuous DRX occurs, as expected in high-stackingfault-energy materials, and is characterized by the progressive conversion of the sub-boundaries into larger-angle boundaries, which involves very limited grain boundaries migration.In addition, straininduced precipitation(SIP) is sufficient under this condition, further impeding the healing of bonding interface.Hence, the joints obtained at low strain rate fractured at the bonding interface easily.Whereas discontinuous DRX is activated at high strain rates(10 and 30 s^(-1)).Under this condition, the formation of sub-boundaries is severely suppressed, resulting in the piling-up of dislocations and hence the storage of a greater amount of stored energy for nucleation and subsequent nuclei growth via the long-distance grain boundaries migration.Meanwhile, the SIP process is sluggish, making the conditions much more favorable for grain boundaries migration which plays a key role in the healing of the original bonding interface.Thus, the joints can be successfully bonded when a high strain rate is applied, with the joints exhibiting tensile properties similar to that of the base material.
基金supported by the National Key Research and Development Program(2018YFA0702900)the National Natural Science Foundation of China(52173305,52101061,52233017,and 52203384)+4 种基金the Strategic Priority Research Program of the Chinese Academy of Sciences(XDC04000000)China Postdoctoral Science Foundation(2020M681004,2021M703276,and 2022T150662)the IMR Innovation Foundation(2022-PY12)LingChuang Research Project of China National Nuclear Corporationthe Youth Innovation Promotion Association,Chinese Academy of Sciences。
基金Fundamental Research Funds for the Central Universities (N2107001)China Postdoctoral Science Foundation (2019M651129, 2019TQ0053)National Natural Science Foundation of China (52001060)。
