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Hot Compressive Deformation Characteristics of Al-9.3Zn-2.4Mg-1.1Cu Alloy
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作者 刘鹏茹 郝世明 XIE Jingpei 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第3期754-765,共12页
To understand the hot compression deformation characteristics of the self-developed Al-9.3Zn-2.4Mg^(-1).1Cu alloy,the hot compression tests of Al-9.3Zn-2.4Mg^(-1).1Cu alloy were investigated by Gleeble 1500 thermo-mec... To understand the hot compression deformation characteristics of the self-developed Al-9.3Zn-2.4Mg^(-1).1Cu alloy,the hot compression tests of Al-9.3Zn-2.4Mg^(-1).1Cu alloy were investigated by Gleeble 1500 thermo-mechanical simulator to determine the best hot processing conditions.The hot deformation temperatures were 300,350,400,and 450℃,and the strain rates were 1,0.1,0.01,and 0.003 s^(-1),respectively.Based on the experimental results,the constitutive equation and hot processing maps are established,and the corresponding strain rate and temperature-sensitive index are analyzed.The results show that Al-9.3Zn-2.4Mg^(-1).1Cu alloy has a dynamic softening trend and high strain rate sensitivity during the isothermal compression process.The hot deformation behavior can be described by an Arrhenius-type equation after strain compensation.The temperature has a negligible effect on the hot processing properties,while a low strain rate is favorable for the hot working of alloy.The processing maps and microstructure show that the optimal processing conditions were in the temperature range of 400-450℃and strain rate range of 0.003-0.005 s^(-1). 展开更多
关键词 Al-Zn-Mg-Cu alloy hot working hot deformation behavior constitutive equations processing maps
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Flow characteristics and hot workability of a typical low-alloy high-strength steel during multi-pass deformation 被引量:1
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作者 Mingjie Zhao Lihong Jiang +4 位作者 Changmin Li Liang Huang Chaoyuan Sun Jianjun Li Zhenghua Guo 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第2期323-336,共14页
Heavy components of low-alloy high-strength(LAHS) steels are generally formed by multi-pass forging. It is necessary to explore the flow characteristics and hot workability of LAHS steels during the multi-pass forging... Heavy components of low-alloy high-strength(LAHS) steels are generally formed by multi-pass forging. It is necessary to explore the flow characteristics and hot workability of LAHS steels during the multi-pass forging process, which is beneficial to the formulation of actual processing parameters. In the study, the multi-pass hot compression experiments of a typical LAHS steel are carried out at a wide range of deformation temperatures and strain rates. It is found that the work hardening rate of the experimental material depends on deformation parameters and deformation passes, which is ascribed to the impacts of static and dynamic softening behaviors. A new model is established to describe the flow characteristics at various deformation passes. Compared to the classical Arrhenius model and modified Zerilli and Armstrong model, the newly proposed model shows higher prediction accuracy with a confidence level of 0.98565. Furthermore, the connection between power dissipation efficiency(PDE) and deformation parameters is revealed by analyzing the microstructures. The PDE cannot be utilized to reflect the efficiency of energy dissipation for microstructure evolution during the entire deformation process, but only to assess the efficiency of energy dissipation for microstructure evolution in a specific deformation parameter state.As a result, an integrated processing map is proposed to better study the hot workability of the LAHS steel, which considers the effects of instability factor(IF), PDE, and distribution and size of grains. The optimized processing parameters for the multi-pass deformation process are the deformation parameters of 1223–1318 K and 0.01–0.08 s^(-1). Complete dynamic recrystallization occurs within the optimized processing parameters with an average grain size of 18.36–42.3 μm. This study will guide the optimization of the forging process of heavy components. 展开更多
关键词 low-alloy high-strength steel work hardening rate constitutive model hot workability multi-pass deformation
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Effect of Gd Addition on Hot Deformation Behavior and Microstructure Evolution of 7075 Aluminum Alloy
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作者 LI Yajie FAN Xuran +2 位作者 QIN Fengming ZHAO Xiaodong CAO Kefan 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第6期1595-1612,共18页
In order to clarify the effect of rare earth Gd on the microstructure evolution and deformation behavior of 7075 aluminum alloy during hot compression,uniaxial compression tests of Al-Zn-Mg-Cu-0.5%Gd were conducted at... In order to clarify the effect of rare earth Gd on the microstructure evolution and deformation behavior of 7075 aluminum alloy during hot compression,uniaxial compression tests of Al-Zn-Mg-Cu-0.5%Gd were conducted at strain rates of 0.001,0.01,0.1,and 1 s^(-1)with the temperatures ranging from 350 to 450℃.The microstructural evolution during deformation was characterized using optical microscopy and electron backscatter diffraction(EBSD)techniques.The experimental results indicate that the addition of the rare earth element Gd significantly increases the peak flow stress and thermal activation energy of the alloy.Due to the pinning effect of rare earth phases,dislocation movement is hindered,leading to an increased level of work hardening in the alloy.However,the dynamic recrystallization of the alloy is complicated.At a high Z(Zener-Hollomon parameter)values,recrystallization occurs in the form of DDRX(Discontinuous Dynamic Recrystallization),making it easier to nucleate at grain boundaries.As the Z value decreases gradually,the recrystallization mechanism transitions from discontinuous dynamic recrystallization(DDRX)to continuous dynamic recrystallization(CDRX).At a low Z values with the strain rate of 0.001 s^(-1),the inhibitory effect of rare earths weakens,resulting in a comparable recrystallization ratio between Al-Zn-Mg-Cu-Gd alloy and 7075 aluminum alloy.Moreover,the average grain size of the aluminum alloy with Gd addition is only half that of 7075 aluminum.The addition of Gd provides Orowan and substructure strengthening for the alloy,which greatly improves the work-hardening of the alloy compared with 7075 aluminum alloy and improves the strength of the alloy. 展开更多
关键词 Al-Zn-Mg-Cu-Gd hot deformation behavior constitutive model dynamic recrystallization microstructure evolution
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Effect of hot isostatic pressure on the microstructure and tensile properties of γ'-strengthened superalloy fabricated through induction-assisted directed energy deposition
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作者 Jianjun Xu Hanlin Ding +1 位作者 Xin Lin Feng Liu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第5期1089-1097,共9页
The microstructure characteristics and strengthening mechanism of Inconel738LC(IN-738LC) alloy prepared by using induction-assisted directed energy deposition(IDED) were elucidated through the investigation of samples... The microstructure characteristics and strengthening mechanism of Inconel738LC(IN-738LC) alloy prepared by using induction-assisted directed energy deposition(IDED) were elucidated through the investigation of samples subjected to IDED under 1050℃ preheating with and without hot isostatic pressing(HIP,1190℃,105 MPa,and 3 h).Results show that the as-deposited sample mainly consisted of epitaxial columnar crystals and inhomogeneously distributed γ’ phases in interdendritic and dendritic core regions.After HIP,grain morphology changed negligibly,whereas the size of the γ’ phase became increasingly even.After further heat treatment(HT,1070℃,2 h + 845℃,24 h),the γ’ phase in the as-deposited and HIPed samples presented a bimodal size distribution,whereas that in the as-deposited sample showed a size that remained uneven.The comparison of tensile properties revealed that the tensile strength and uniform elongation of the HIP + HTed sample increased by 5% and 46%,respectively,due to the synergistic deformation of bimodal γ’phases,especially large cubic γ’ phases.Finally,the relationship between phase transformations and plastic deformations in the IDEDed sample was discussed on the basis of generalized stability theory in terms of the trade-off between thermodynamics and kinetics. 展开更多
关键词 directed energy deposition Ni-based superalloys high-temperature preheating hot isostatic pressing MICROSTRUCTURE tensile properties
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Hot Deformation Behavior of Ti-6Al-4V-0.5Ni-0.5Nb Titanium Alloy
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作者 ZHU Guochuan LIU Qiang +6 位作者 SONG Shengyin HUI Songxiao YU Yang YE Wenjun QI Jun TANG Zhengwei XU Penghai 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第5期1270-1277,共8页
Characterization of hot deformation behavior of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy was investigated through isothermal compression at various temperatures from 750 to 1050℃and strain rate from 0.01 to 10 s^(-1).The... Characterization of hot deformation behavior of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy was investigated through isothermal compression at various temperatures from 750 to 1050℃and strain rate from 0.01 to 10 s^(-1).The isothermal compression experiment results showed that the peak stress of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy decreased with the temperature increasing and the strain rate decreasing.The softening mechanism was dynamic recovery below T_(β)and changed to dynamic recrystallization above T_(β).The arrheniustype relationship was used to calculate the constitutive equation of Ti-6Al-4V-0.5Ni-0.5Nb alloy in two-phase regions.It was found that the apparent activation energies were 427.095 kJ·mol^(-1)in theα+βphase region and 205.451 kJ·mol^(-1)in theβphase region,respectively.On the basis of dynamic materials model,the processing map is generated,which shows that the highest peak efficiency of power dissipation of 56%occurs at about 1050℃/0.01 s^(-1).It can be found in the processing maps that the strain had significant effect on the peak region of power dissipation efficiency of Ti-6Al-4V-0.5Ni-0.5Nb alloy.Furthermore,optimized hot working regions were investigated and validated through microstructure observation.The optimum thermo mechanical process condition for hot working of Ti-6Al-4V-0.5Ni-0.5Nb titanium alloy was suggested to be in the temperature range of 950-1000℃with a strain rate of 0.01-0.1 s^(-1). 展开更多
关键词 titanium alloy hot deformation processing map dynamic recrystallization
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Enhancing constitutive description and workability characterization of Mg alloy during hot deformation using machine learning-based Arrhenius-type model
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作者 Jinchuan Long Lei Deng +6 位作者 Junsong Jin Mao Zhang Xuefeng Tang Pan Gong Xinyun Wang Gangfeng Xiao Qinxiang Xia 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2024年第7期3003-3023,共21页
Hot deformation is a commonly employed processing technique to enhance the ductility and workability of Mg alloy.However,the hot deformation of Mg alloy is highly sensitive to factors such as temperature,strain rate,a... Hot deformation is a commonly employed processing technique to enhance the ductility and workability of Mg alloy.However,the hot deformation of Mg alloy is highly sensitive to factors such as temperature,strain rate,and strain,leading to complex flow behavior and an exceptionally narrow processing window for Mg alloy.To overcome the shortcomings of the conventional Arrhenius-type(AT)model,this study developed machine learning-based Arrhenius-type(ML-AT)models by combining the genetic algorithm(GA),particle swarm optimization(PSO),and artificial neural network(ANN).Results indicated that when describing the flow behavior of the AQ80 alloy,the PSO-ANN-AT model demonstrates the most prominent prediction accuracy and generalization ability among all ML-AT and AT models.Moreover,an activation energy-processing(AEP)map was established using the reconstructed flow stress and activation energy fields based on the PSO-ANN-AT model.Experimental validations revealed that this AEP map exhibits superior predictive capability for microstructure evolution compared to the one established by the traditional interpolation methods,ultimately contributing to the precise determination of the optimum processing window.These findings provide fresh insights into the accurate constitutive description and workability characterization of Mg alloy during hot deformation. 展开更多
关键词 Constitutive description Workability characterization Machine learning Mg alloy hot deformation
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Ballistic performance of titanium-based layered composites made using blended elemental powder metallurgy and hot isostatic pressing
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作者 Pavlo Markovsky Jacek Janiszewski +5 位作者 Dmytro Savvakin Oleksandr Stasyuk Bartosz Fikus Victor Samarov Vianey Ellison Sergey V.Prikhodko 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第9期1-14,共14页
Metal matrix composites tiles based on Ti-6Al-4V(Ti64)alloy,reinforced with 10,20,and 40(vol%)of either TiC or TiB particles were made using press-and-sinter blended elemental powder metallurgy(BEPM)and then bonded to... Metal matrix composites tiles based on Ti-6Al-4V(Ti64)alloy,reinforced with 10,20,and 40(vol%)of either TiC or TiB particles were made using press-and-sinter blended elemental powder metallurgy(BEPM)and then bonded together into 3-layer laminated plates using hot isostatic pressing(HIP).The laminates were ballistically tested and demonstrated superior performance.The microstructure and properties of the laminates were analyzed to determine the effect of the BEPM and HIP processing on the ballistic properties of the layered plates.The effect of porosity in sintered composites on further diffusion bonding of the plates during HIP is analyzed to understand the bonding features at the interfaces between different adjacent layers in the laminate.Exceptional ballistic performance of fabricated structures was explained by a significant reduction in the residual porosity of the BEPM products by their additional processing using HIP,which provides an unprecedented increase in the hardness of the layered composites.It is argued that the combination of the used two technologies,BEPM and HIP is principally complimentary for the materials in question with the abilities to solve the essential problems of each used individually. 展开更多
关键词 Metal matrix composites Powder metallurgy Titanium hydride powder Master alloy Titanium carbide Titanium boride hot isostatic pressing Ballistic tests
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Prediction of Hot Deformation Behavior of 7Mo Super Austenitic Stainless Steel Based on Back Propagation Neural Network
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作者 WANG Fan WANG Xitao +1 位作者 XU Shiguang HE Jinshan 《材料导报》 EI CAS CSCD 北大核心 2024年第17期165-171,共7页
The hot compression tests of 7Mo super austenitic stainless(SASS)were conducted to obtain flow curves at the temperature of 1000-1200℃and strain rate of 0.001 s^(-1)to 1 s^(-1).To predict the non-linear hot deformati... The hot compression tests of 7Mo super austenitic stainless(SASS)were conducted to obtain flow curves at the temperature of 1000-1200℃and strain rate of 0.001 s^(-1)to 1 s^(-1).To predict the non-linear hot deformation behaviors of the steel,back propagation-artificial neural network(BP-ANN)with 16×8×8 hidden layer neurons was proposed.The predictability of the ANN model is evaluated according to the distribution of mean absolute error(MAE)and relative error.The relative error of 85%data for the BP-ANN model is among±5%while only 42.5%data predicted by the Arrhenius constitutive equation is in this range.Especially,at high strain rate and low temperature,the MAE of the ANN model is 2.49%,which has decreases for 18.78%,compared with conventional Arrhenius constitutive equation. 展开更多
关键词 7Mo super austenitic stainless steel hot deformation behavior flow stress BP-ANN Arrhenius constitutive equation
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Effect of the capsule on deformation and densification behavior of nickel-based superalloy compact during hot isostatic pressing 被引量:3
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作者 Lebiao Yang Xiaona Ren +4 位作者 Chao Cai Pengju Xue MIrfan Hussain Yusheng Shi Changchun Ge 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第1期122-130,共9页
The Shima yield criterion used in finite element analysis for nickel-based superalloy powder compact during hot isostatic pressing(HIP) was modified through uniaxial compression experiments. The influence of cylindric... The Shima yield criterion used in finite element analysis for nickel-based superalloy powder compact during hot isostatic pressing(HIP) was modified through uniaxial compression experiments. The influence of cylindrical capsule characteristics on FGH4096M superalloy powder compact deformation and densification behavior during HIP was investigated through simulations and experiments. Results revealed the simulation shrinkage prediction fitted well with the experimental shrinkage including a maximum shrinkage error of 1.5%. It was shown that the axial shrinkage was 1.7% higher than radial shrinkage for a cylindrical capsule with the size of ∮50 mm × 100 mm due to the force arm difference along the axial and radial direction of the capsule. The stress deviated from the isostatic state in the capsule led to the uneven shrinkage and non-uniform densification of the powder compact. The ratio of the maximum radial displacement to axial displacement increased from0.47 to 0.75 with the capsule thickness increasing from 2 to 4 mm. The pressure transmission is related to the capsule thickness, the capsule material performance, and physical parameters in the HIP process. 展开更多
关键词 hot isostatic pressing nickel-based superalloy compact CAPSULE DENSIFICATION deformATION
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OBSERVATION OF DISLOCATION CONFIGURATIONS IN AGED & DEFORMED NiAl ALLOY AFTER HOT ISOSTATIC PRESSING (HIP)
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作者 Cui Yuexian Dong Shangli +3 位作者 Liu Bo Li Daoming Yang Dezhuang(Schwa of Materials Sccience and Engineering, Harbin instituteOf Technology, Harbin, China, 150001 )Bi Geping Wang Qin(Central iron and Steel Research institute, Beijing China, 100081 ) 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 1996年第4期278-283,共6页
Observation of dislocation configurations was conducted for aged and compressive deformed (Ni64A136) FeMoB alloy after hot isostatic pressing (HIP). It isshown that short and straight parallel dislocations are present... Observation of dislocation configurations was conducted for aged and compressive deformed (Ni64A136) FeMoB alloy after hot isostatic pressing (HIP). It isshown that short and straight parallel dislocations are present in the matrix of NiAI alloy.Long and tortuous dislocations and superdislocations appear in the 1%-deformed specimen. As the compressive strain increases to 2. 6%, high-densities dislocations appear inand between the deformation bands. The dislocations become tangled up in the specimencompressed to a strain of 6. 2 %. 展开更多
关键词 NIAL hot isostatic press compressive deformation dislocations(materials) aging (metallurgy)
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Hot deformation behavior of TC11/Ti-22Al-25Nb dual-alloy in isothermal compression 被引量:7
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作者 秦春 姚泽坤 +2 位作者 宁永权 石志峰 郭鸿镇 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第7期2195-2205,共11页
The high-temperature flow behavior of TCll/Ti-22Al-25 Nb electron beam(EB) weldments was investigated by the isothermal compression tests at the temperature of 900-1060℃ and the strain rate of 0.001-10 s-(-1).Bas... The high-temperature flow behavior of TCll/Ti-22Al-25 Nb electron beam(EB) weldments was investigated by the isothermal compression tests at the temperature of 900-1060℃ and the strain rate of 0.001-10 s-(-1).Based on the experimental data,the constitutive equation that describes the flow stress as a function of strain rate and deformation temperature is obtained.The apparent activation energy of deformation is calculated,which decreases with increasing the strain and the value is 334 kJ/mol at strain of 0.90.The efficiency of power dissipation η changes obviously with the variation of deformation conditions.Under the strain rates of 0.01,0.1 and 1 s-(-1),the value of η increases with increasing the true strain for different deformation temperatures.While the value of η decreases with increasing the strain under the strain rates of 0.001 and 10 s-(-1).The optimum processing condition is(t(opi)=1060℃,ε(opi)=0.1 s-(-1)) with the peak efficiency of 0.51.Under this deformation,dynamic recrystallization(DRX) is observed obviously in the microstructure of welding zone.Under the condition of 1060℃ and 0.001 s-(-1),the deformation mechanism is dominated by dynamic recovery(DRV) and the value of η decreases sharply(η=0.02).The flow instability is predicted to occur since the instability parameter ξ(ε)becomes negative.The hot working process can be carried out safely in the domain with the strain rate of 0.001-0.6 s-(-1) and the temperature of 900-1060℃. 展开更多
关键词 dual-alloy hot deformation processing map apparent activation energy MICROSTRUCTURE
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Dynamic recovery and dynamic recrystallization of NiTi shape memory alloy under hot compression deformation 被引量:12
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作者 江树勇 张艳秋 赵亚楠 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第1期140-147,共8页
Mechanical behavior of nickel?titanium shape memory alloy(NiTi SMA) under hot deformation was investigated according to the true stress—strain curves of NiTi samples under compression at the strain rates of 0.001-... Mechanical behavior of nickel?titanium shape memory alloy(NiTi SMA) under hot deformation was investigated according to the true stress—strain curves of NiTi samples under compression at the strain rates of 0.001-1 s-1 and at the temperatures of 600?1000℃.Dynamic recovery and dynamic recrystallization of NiTi SMA were systematically investigated by microstructural evolution.The influence of the strain rates,the deformation temperatures and the deformation degree on the dynamic recovery and dynamic recrystallization of NiTi SMA was obtained as well.NiTi SMA was characterized by the combination of dynamic recovery and dynamic recrystallization at 600℃ and 700℃,but the complete dynamic recrystallization occurred at other deformation temperatures.Increasing the deformation temperatures or decreasing the stain rates leads to larger equiaxed grains.The deformation degree has an important influence on the dynamic recrystallization of NiTi SMA.There exists the critical deformation degree during the dynamic recrystallization of NiTi SMA,beyond which the larger deformation degree contributes to obtaining the finer equiaxed grains. 展开更多
关键词 NiTi alloy shape memory alloy dynamic recovery dynamic recrystallization hot deformation
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Constitutive equation and processing map for hot compressed as-cast Ti-43Al-4Nb-1.4W-0.6B alloy 被引量:5
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作者 李建波 刘咏 +3 位作者 王岩 刘彬 卢斌 梁霄鹏 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第11期3383-3391,共9页
High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated... High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated that the true stress-true strain curves show a dynamic flow softening behavior. The flow curves after the friction and the temperature compensations were employed to develop constitutive equations. The effects of temperature and the strain rate on the deformation behavior were represented by Zener-Holloman exponential equation. The influence of strain was incorporated in the constitutive analysis by considering the effect of the strain on material constants by a five-order polynomial. A revised model was proposed to describe the relationships among the flow stress, strain rate and temperature and the predicted flow stress curves were in good agreement with experimental results. Appropriate deformation processing parameters were suggested based on the processing map which was constructed from friction and temperature corrected flow curves, determined as 1343 K, 0.02 s-1 and were successfully applied in the canned forging of billets to simulate industrial work condition. 展开更多
关键词 TiAl alloy flow stress hot deformation constitutive equation processing map
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High temperature deformation behavior and optimization of hot compression process parameters in TC11 titanium alloy with coarse lamellar original microstructure 被引量:4
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作者 鲁世强 李鑫 +2 位作者 王克鲁 董显娟 傅铭旺 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第2期353-360,共8页
The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the tem... The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a+fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α+β phase field. The peak of efficiency of power dissipation in α+β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α+β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a+β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results. 展开更多
关键词 titanium alloy coarse lamellar microstructure high temperature deformation behavior processing map hot compression process parameter optimization
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Hot deformation behavior and microstructural evolution of Al-Zn-Mg-0.25Sc-Zr alloy during compression at elevated temperatures 被引量:2
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作者 张志野 潘清林 +2 位作者 周坚 刘晓艳 陈琴 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第7期1556-1562,共7页
The hot deformation behavior of Al-Zn-Mg-0.25Sc-Zr alloy and its microstructural evolution were investigated by isothermal axisymmetric hot compression tests at temperatures from 340 to 500°C and strain rates ran... The hot deformation behavior of Al-Zn-Mg-0.25Sc-Zr alloy and its microstructural evolution were investigated by isothermal axisymmetric hot compression tests at temperatures from 340 to 500°C and strain rates ranging from 0.001 to 10 s -1 .The steady flow stress increased with increasing the strain rate or decreasing the deformation temperature,which can be described by a hyperbolic-sine constitutive equation with the deformation activation energy of 150.25 kJ/mol.The tendency of dynamic recrystallization enhanced at high deforming temperatures and low strain rates,which corresponded to low Z values.With decreasing Z value,the main softening mechanism of the alloy transformed from dynamic recovery to dynamic recrystallization, correspondingly,the subgrain size increased and the dislocation density decreased. 展开更多
关键词 Al-Zn-Mg-Sc-Zr alloy hot deformation flow behavior microstructural evolution
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Two-stage dynamic recrystallization and texture evolution in Al-7Mg alloy during hot torsion
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作者 Kwang Tae Son Chang Hee Cho +1 位作者 Myoung Gyun Kim Ji Woon Lee 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第8期1900-1911,共12页
Hot torsion tests were performed on the Al-7Mg alloy at the temperature ranging from 300 to 500℃ and strain rates between 0.05 and 5 s^(-1) to explore the progressive dynamic recrystallization(DRX)and texture behavio... Hot torsion tests were performed on the Al-7Mg alloy at the temperature ranging from 300 to 500℃ and strain rates between 0.05 and 5 s^(-1) to explore the progressive dynamic recrystallization(DRX)and texture behaviors.The DRX behavior of the alloy manifested two distinct stages:Stage 1 at strain of≤2 and Stage 2 at strains of≥2.In Stage 1,there was a slight increase in the DRXed grain fraction(X_(DRX))with predominance of discontinuous DRX(DDRX),followed by a modest change in X_(DRX) until the transition to Stage 2.Stage 2 was marked by an accelerated rate of DRX,culminating in a substantial final X_(DRX) of~0.9.Electron backscattered diffraction(EBSD)analysis on a sample in Stage 2 revealed that continuous DRX(CDRX)predominantly occurred within the(121)[001]grains,whereas the(111)[110]grains underwent a geometric DRX(GDRX)evolution without a noticeable sub-grain structure.Furthermore,a modified Avrami’s DRX kinetics model was utilized to predict the microstructural refinement in the Al-7Mg alloy during the DRX evolution.Although this kinetics model did not accurately capture the DDRX behavior in Stage 1,it effectively simulated the DRX rate in Stage 2.The texture index was employed to assess the evolution of the texture isotropy during hot-torsion test,demonstrating significant improvement(>75%)in texture randomness before the commencement of Stage 2.This initial texture evolution is attributed to the rotation of parent grains and the substructure evolution,rather than to an increase in X_(DRX). 展开更多
关键词 Al-7Mg alloys hot deformation hot torsion tests dynamic recrystazlliation microstructure texture
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Hot deformation behavior of Fe–27.34Mn–8.63Al–1.03C lightweight steel 被引量:5
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作者 Haitao Lu Dazhao Li +1 位作者 Siyuan Li Yong’an Chen 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第4期734-743,共10页
Hot compression tests were performed to investigate the hot deformation behavior of Fe–27.34Mn–8.63Al–1.03C lightweight steel and optimize the hot workability parameters. The temperature range was 900–1150℃ and t... Hot compression tests were performed to investigate the hot deformation behavior of Fe–27.34Mn–8.63Al–1.03C lightweight steel and optimize the hot workability parameters. The temperature range was 900–1150℃ and the strain rate range was 0.01–5 s^(-1)on a Gleeble-3800 thermal simulator machine. The results showed that the flow stress increased with decreasing deformation temperature and increasing strain rate. According to the constitutive equation, the activation energy of hot deformation was 422.88 kJ·mol^(-1). The relationship between the critical stress and peak stress of the tested steel was established, and a dynamic recrystallization kinetic model was thus obtained. Based on this model, the effects of strain rate and deformation temperature on the volume fraction of dynamically recrystallized grains were explored. The microstructural examination and processing map results revealed that the tested steel exhibited a good hot workability at deformation temperatures of 1010–1100℃ and strain rate of 0.01 s^(-1). 展开更多
关键词 Fe–Mn–Al–C steel hot deformation activation energy microstructural evolution processing map
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Influence of rare earth Ce on hot deformation behavior of as-cast Mn18Cr18N high nitrogen austenitic stainless steel 被引量:4
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作者 Yushuo Li Yanwu Dong +3 位作者 Zhouhua Jiang Qingfei Tang Shuyang Du Zhiwen Hou 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第2期324-334,共11页
The hot deformation behavior of Mn18Cr18N and Mn18Cr18N+Ce high nitrogen austenitic stainless steels at 1173-1473 K and 0.01-1 s^(-1) were investigated by thermal compression tests.The influence mechanism of Ce on the... The hot deformation behavior of Mn18Cr18N and Mn18Cr18N+Ce high nitrogen austenitic stainless steels at 1173-1473 K and 0.01-1 s^(-1) were investigated by thermal compression tests.The influence mechanism of Ce on the hot deformation behavior was analyzed by Ce-containing inclusions and segregation of Ce.The results show that after the addition of Ce,large,angular,hard,and brittle inclusions(TiN-Al_(2)O_(3),TiN,and Al_(2)O_(3)) can be modified to fine and dispersed Ce-containing inclusions(Ce-Al-O-S and TiN-Ce-Al-O-S).During the solidification,Ce-containing inclusions can be used as heterogeneous nucleation particles to refine as-cast grains.During the hot deformation,Ce-containing inclusions can pin dislocation movement and grain boundary migration,induce dynamic recrystallization(DRX)nucleation,and avoid the formation and propagation of micro cracks and gaps.In addition,during the solidification,Ce atoms enrich at the front of solid-li-quid interface,resulting in composition supercooling and refining the secondary dendrites.Similarly,during the hot deformation,Ce atoms tend to segregate at the boundaries of DRX grains,inhibiting the growth of grains.Under the synergistic effect of Ce-containing inclusions and Ce segregation,although the hot deformation resistance and hot deformation activation energy are improved,DRX is more likely to occur and the size of DRX grains is significantly refined,and the problem of hot deformation cracking can be alleviated.Finally,the microhardness of the samples was measured.The results show that compared with as-cast samples,the microhardness of hot-deformed samples increases signific-antly,and with the increase of DRX degree,the microhardness decreases continuously.In addition,Ce can affect the microhardness of Mn18Cr18N steel by affecting as-cast and hot deformation microstructures. 展开更多
关键词 rare earth hot deformation Mn18Cr18N steel non-metallic inclusions element segregation MICROHARDNESS
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Effects of microstructure characteristics on the tensile properties and fracture toughness of TA15 alloy fabricated by hot isostatic pressing 被引量:2
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作者 Langping Zhu Yu Pan +6 位作者 Yanjun Liu Zhiyu Sun Xiangning Wang Hai Nan Muhammad-Arif Mughal Dong Lu Xin Lu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第4期697-706,共10页
Powder hot isostatic pressing(HIP) is an effective method to achieve near-net-shape manufacturing of high-quality complex thinwalled titanium alloy parts, and it has received extensive attention in recent years. Howev... Powder hot isostatic pressing(HIP) is an effective method to achieve near-net-shape manufacturing of high-quality complex thinwalled titanium alloy parts, and it has received extensive attention in recent years. However, there are few reports about the microstructure characteristics on the strengthening and toughening mechanisms of powder hot isostatic pressed(HIPed) titanium alloys. Therefore, TA15powder was prepared into alloy by HIP approach, which was used to explore the microstructure characteristics at different HIP temperatures and the corresponding tensile properties and fracture toughness. Results show that the fabricated alloy has a “basket-like structure” when the HIP temperature is below 950℃, consisting of lath clusters and surrounding small equiaxed grains belts. When the HIP temperature is higher than 950℃, the microstructure gradually transforms into the Widmanstatten structure, accompanied by a significant increase in grain size. The tensile strength and elongation are reduced from 948 MPa and 17.3% for the 910℃ specimen to 861 MPa and 10% for the 970℃ specimen.The corresponding tensile fracture mode changes from transcrystalline plastic fracture to mixed fracture including intercrystalline cleavage.The fracture toughness of the specimens increases from 82.64 MPa·m^(1/2)for the 910℃ specimen to 140.18 MPa·m^(1/2)for the 970℃ specimen.Specimens below 950℃ tend to form holes due to the prior particle boundaries(PPBs), which is not conducive to toughening. Specimens above 950℃ have high fracture toughness due to the crack deflection, crack branching, and shear plastic deformation of the Widmanstatten structure. This study provides a valid reference for the development of powder HIPed titanium alloy. 展开更多
关键词 POWDER titanium alloy hot isostatic pressing STRENGTH fracture toughness
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Revealing the grain size dependent hot workability and deformation mechanisms in a Mg-Zn-Y alloy 被引量:2
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作者 Ruiqing Lu Zhiming Xu +4 位作者 Fulin Jiang Shiwei Xu Dingfa Fu Hui Zhang Jie Teng 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第4期1461-1471,共11页
Despite the industrial significance of grain size for enhancing mechanical properties and formability,the in-depth deformation mechanisms at elevated temperature are still unclear.To investigate the functions of grain... Despite the industrial significance of grain size for enhancing mechanical properties and formability,the in-depth deformation mechanisms at elevated temperature are still unclear.To investigate the functions of grain size on hot workability and deformation mechanisms,three groups of Mg-1.2Zn-0.2Y alloy specimens with different grain sizes were hot compressed and then studied by combining constitutive model,processing map and microstructural observations.The results showed that the enhanced hot workability accompanying low deformation activation energy and small instability regime was obtained with refined grain size.During hot deformation,the decreased grain size in Mg1.2Zn-0.2Y alloy mainly improved the plastic deformation homogeneity,especially for the weakened local straining around grain boundaries.As a result,the dynamic recrystallization nucleation and texture development at lower strain level were influenced by the initial grain size.At higher strain magnitude,the growth and coarsening of dynamic recrystallized grains would further release strain localization and improve hot workability,while the texture was less impacted.Further,unlike the primary basal slip and deformation twinning in the specimen with coarse grain at low temperature,non-basal slips of dislocations were initiated with less deformation twins in the specimens with refined grain size. 展开更多
关键词 Mg-Zn-Y alloy hot workability Plastic deformation Grain size TEXTURE
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