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Morphology and quantitative analysis of O phase during heat treatment of hot-deformed Ti_2AlNb-based alloy 被引量:3
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作者 Hong-yu Zhang Chong Li +3 位作者 Zong-qing Ma Li-ming Yu Hui-jun Li Yong-chang Liu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2018年第10期1191-1200,共10页
A 1040°C-hot-deformed Ti_2AlNb-based alloy solution-treated at 950°C and aged at different temperatures was quantitatively investigated. The microstructure, size of the phase, and microhardness of the deform... A 1040°C-hot-deformed Ti_2AlNb-based alloy solution-treated at 950°C and aged at different temperatures was quantitatively investigated. The microstructure, size of the phase, and microhardness of the deformed alloys were measured. The results indicated that the microstructure of the deformed Ti_2AlNb-based alloy specimens comprise coarse O lath, fine O lath, equiaxed O/α_2, and acicular O phase. More O phase was generated in the deformed alloy after heat treatment because the acicular O phase was more likely to nucleate and grow along the deformation-induced crystal defects such as dislocations and subgrain boundaries. After deformation and subsequent heat treatment, the acicular O phase of the resultant alloy became finer compared to that of the undeformed alloy, and the acicular O phase became coarser and longer with the elevated aging temperature, while the width of the O lath exhibited unobvious variations. The hot deformation facilitated the dissolution of the O lath but accelerated the precipitation of the acicular O phase. When the 950°C-solution-treated deformed Ti_2AlNb-based alloy was then aged at 750°C for different periods, the phase content was nearly invariable, O and B2 phases eventually reached equilibrium, and the microstructure became stable and homogeneous. 展开更多
关键词 Ti2AlNb-based alloys hot deformation solution treatment aging microstructure
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Influence of melt-treatment on material constants of aluminum sheet used for easy-open can during hot deformation 被引量:6
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作者 陈永禄 傅高升 陈文哲 《中国有色金属学会会刊:英文版》 EI CSCD 2006年第2期304-310,共7页
The isothermal compression test at elevated temperature was carried out for aluminum sheets prepared by different melt-treatment methods with aid of dynamic hot/mechanical simulation experimental technology. The mater... The isothermal compression test at elevated temperature was carried out for aluminum sheets prepared by different melt-treatment methods with aid of dynamic hot/mechanical simulation experimental technology. The material constants of hot deformation have been solved by multivariate regression directly. Influence of metallurgy factors on the constants was analyzed. The results show that at some strain, the relationship of sheets’ flow stress with deformation temperature and strain rate can be expressed more suitably with Arrhenius equation modified by hyperbolic sine function. Structure factor A1, stress-level coefficient α, strain rate sensibility exponent m and deformation activation energy Q all increase with increment of strain, while stress exponent n decreases gradually. The bigger α value or the smaller n value is, the more obvious the dynamic softening is, but the α value will increase for the metallurgy defects existing in the sheets. Influence of melt-treatment on Q depends upon the synthesis effect of all kinds of metallurgy defects. The Q and n values of the sheet prepared by high-efficient melt-treatment are the least, while the m value is the biggest, and the sheet can deform easily and evenly. 展开更多
关键词 铝合金 易拉罐 材料常数 熔化 热变形
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Influence of Different Surface Treatments of H13 Hot Work Die Steel on Its Thermal Fatigue Behaviors 被引量:3
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作者 MINYong-an WUXiao-chun 《Journal of Shanghai University(English Edition)》 CAS 2001年第4期326-330,共5页
Thermal fatigue checking is the general failure of hot work die steels, which is relative with the structures and properties of the steels and the stress alternated during the employment. The Uddeholm test method on t... Thermal fatigue checking is the general failure of hot work die steels, which is relative with the structures and properties of the steels and the stress alternated during the employment. The Uddeholm test method on thermal fatigue is used to compare the behaviors of different samples, which are treated with plasma nitriding、plasma sulfur carbon nitriding、boronizing or not treated. The results show that the nitriding improves the thermal fatigue property of the tool steel, while the plasma sulfur carbon nitriding and the boronizing impair the property. The mechanisms are induced as follows. By increasing the hardness and changing the stress distribution in the surface layer, surface treatment can decrease the plastic deformation and the tensile stress during the cycling. Therefore, the generation and growth of the cracks are restrained. On the other hand, as results of surface treating, in the surface layer the toughness declines and the expanding coefficient ascendes; the latter change caused the strengthening of the tensile and compressive stress during the cycling. Thus the resistance to thermal fatigue is weakened. Whether or not the surface treatment is favor to thermal fatigue of tool steels relies on which factor is dominant. 展开更多
关键词 thermal fatigue hot work die surface treatment
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Synergistic Influence of Pre-Harvest Calcium Sprays and Postharvest Hot Water Treatment on Fruit Firmness, Decay, Bitter Pit Incidence and Postharvest Quality of Royal Delicious Apples (<i>Malus x domestica</i>Borkh) 被引量:1
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作者 R. R. Sharma D. Singh R. K. Pal 《American Journal of Plant Sciences》 2013年第1期153-159,共7页
Experiments were conducted to observe the effect of pre-harvest calcium (Ca) applied as calcium chloride (1% W/V) and postharvest hot water treatment (HWT) on “Royal Delicious” apples. For this, apples were divided ... Experiments were conducted to observe the effect of pre-harvest calcium (Ca) applied as calcium chloride (1% W/V) and postharvest hot water treatment (HWT) on “Royal Delicious” apples. For this, apples were divided in 4 lots viz., untreated (neither Ca nor HWT), Ca alone (pre-harvest 3 sprays of CaCl2 (1.0% w/v) in the orchard), HWT (42℃ for 2 h). Apples of all four lots were stored in cold storage maintained at 0℃ ± 1℃ and 90% - 95% relative humidity for 6 months. After storage, fruits were removed to ambient conditions for 5 days, and then observations on decay area and incidence, bitter pit incidence, fruit Ca content, lipoxygenase (LOX) and antioxidant (AOX) activity, fruit firmness and fruit quality parameters were recorded. After 6 months in cold storage plus 5 day at 22℃ ± 2℃ and 70% + 4% RH, apples, which received Ca as pre-harvest spray or those which received postharvest hot water treatment or Ca + HWT had significantly lesser decay area (decay lesions) caused by Penicillium expansum or Botrytis cinerea than untreated ones (control). Ca + HWT treatment was significantly more effective on B. cinerea than P. expansum. Untreated apples exhibited higher incidence of bitter pit (18.2%) than those treated with Ca or HWT or both. Fruit Ca content (2.92% DM) were significantly lower and conversely the LOX activity (6.9 μmoles min–1×g–1FW) was higher in untreated apples. Similarly, total phenolics and AOX activity were also lower in the untreated apples than Ca or HWT treated. HWT or Ca treated apples have beneficial effects on fruit firmness, peel colour and quality parameters like TSS and ascorbic acid content. Thus, it is concluded that pre-harvest sprays of calcium chloride with postharvest HWT is highly useful for “Royal Delicious” for reducing decay loss, maintaining firmness, high levels of antioxidants and fruit quality. 展开更多
关键词 hot Water treatment LIPOXYGENASE ACTIVITY Antioxidant ACTIVITY BITTER Pit Fruit Quality
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Effect of Hot Water Treatment on Postharvest Shelf Life and Quality of Broccoli
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作者 WU Ping and LI WuBeijing Vegetable Research Center, Beijing 100089 , P. R. China 《Agricultural Sciences in China》 CAS CSCD 2003年第4期469-472,共4页
Broccoli was stored at 0, 10, or 20℃after immersion in hot water (38 - 52℃) for 10 or 30 min. Yellowing of broccoli was significantly slowed and shelf life significantly increased when broccoli was treated with hot ... Broccoli was stored at 0, 10, or 20℃after immersion in hot water (38 - 52℃) for 10 or 30 min. Yellowing of broccoli was significantly slowed and shelf life significantly increased when broccoli was treated with hot water at 42 - 46℃and then stored at 10 or 20℃. Heat injury occurred when treatment was higher than 46℃in some varieties. Broccoli lasted 2-3 days longer when stored at 10℃ and 1-2 days longer when stored at 20℃ after hot water treatment at 46℃. There was no significant effect of treatment on shelf life after long time storage at 0℃. Weight loss was reduced by hot water treatment and the respiration behavior of the broccoli was also changed. 展开更多
关键词 BROCCOLI hot water treatment STORAGE RESPIRATION
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Influence of thermo hydrogen treatment on hot deformation behavior of Ti600 alloy 被引量:1
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作者 赵敬伟 丁桦 +1 位作者 王耀奇 侯红亮 《中国有色金属学会会刊:英文版》 EI CSCD 2009年第1期65-71,共7页
Hot compressive deformation of Ti600 alloy after thermo hydrogen treatment (THT) was carried out within hydrogen content range of 0-0.5%, temperature range of 760-920 ℃ and strain rate range of 0.01-10 s-1. The flow ... Hot compressive deformation of Ti600 alloy after thermo hydrogen treatment (THT) was carried out within hydrogen content range of 0-0.5%, temperature range of 760-920 ℃ and strain rate range of 0.01-10 s-1. The flow stress of Ti600 alloy after THT was obtained under hot deformation condition, and the influence of hydrogen on work-hardening rate (S*), strain energy density (U*), and deformation activation energy (Q) was analysed. The results show that the flow stress of Ti600 alloy decreases remarkably with the increase of hydrogen when the hydrogen content is less than 0.3%. Both S* and U* decrease with the increase of hydrogen when the hydrogen content is less than 0.3%, and when the hydrogen content is more than 0.3%, S* and U* increase with hydrogen addition. The value of Q decreases with the increase of strain at the same hydrogen content. The addition of small quantity of hydrogen leads to an increase of Q at small strain values, and when the strain reaches 0.6, the value of Q decreases gradually with the increase of hydrogen. When the hydrogen content is within the range of 0.1%-0.3%, the flow stress of Ti600 alloy is decreased when being deformed at the temperature range of 760-920 ℃. 展开更多
关键词 TI600合金 热处理 钛合金 金属材料
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APPLICATION OF RARE EARTH IN SURFACE HEAT TREATMENT OF HOT-WORKING DIE STEELS 被引量:1
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作者 胡正前 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 1997年第Z1期138-145,共8页
This paper studies a compound treatment. i. e. liquid S , N,C co-diffusing with rare earth (RE) and then oxidization , for hot-working die steels , and the effect of RE on thermal fatigue behavior of the diffused laye... This paper studies a compound treatment. i. e. liquid S , N,C co-diffusing with rare earth (RE) and then oxidization , for hot-working die steels , and the effect of RE on thermal fatigue behavior of the diffused layer. XRD and SEM energy spectrum prove that trace RE element actually penetrates into the surface layer of steels. The result shows that RE can reduce the gradient of change of hardness in diffused layer, improve the morphology and distribution of compounds , and reduce the degree of surface alligator crack for thermal fatigue. The behavior of thermal fatigue of hot-working die steels is raised by 70% or so after the application of RE. The effect of RE is analysed according to the theory. 展开更多
关键词 rare earth chemical heat treatment hot -working die steel behavior of thermal fatigue.
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“FENG QI AI” HOT COMPRESS TREATMENT
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作者 Zhang Hongsheng, Cui YanHebei College of Traditional Chinese Medicine, Hebei 050011, China 《World Journal of Acupuncture-Moxibustion》 1995年第2期32-35,共4页
Hot medicated cornpress treatment belongs to an external treatment and is a kindof moxibustion. ″Feng Qi Ai″ prescription was recorded in Yi Fang Lei Ju. Zhu Xu Men, Rui ZhuTang Fang. In the treatment, pain in the l... Hot medicated cornpress treatment belongs to an external treatment and is a kindof moxibustion. ″Feng Qi Ai″ prescription was recorded in Yi Fang Lei Ju. Zhu Xu Men, Rui ZhuTang Fang. In the treatment, pain in the loin and the knees, cold-pain around the navel and in theabdornen,diarrhea due to deficiency and cold and other diseases are treated by combination of drugswith hot compress- We have irnproved the treatment and extended the range of its indication. It wasused for treatment 0f menorrhalgia due to cold uterine, gastralgia due to coId of rniddle-jiao, sciatica’periarthritis of shoulder, systremma,piriformis syndrome with good results. 展开更多
关键词 Feng QI AI hot medicated compress treatment Deficiency-cold type
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CLINICAL OBSERVATION ON TREATMENT OF 60 CASES OF ASTHMA WITH RED-HOT NEEDLE IN THE DOG DAYS
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作者 MA Xin- ping(马新平) 《World Journal of Acupuncture-Moxibustion》 2003年第4期50-52,共3页
In the present paper, a total of 109 asthma patients were randomly divided into treatment group (red hot needle, n=62) and control group (conventional acupuncture, n=47). The treatment was conducted beginning from the... In the present paper, a total of 109 asthma patients were randomly divided into treatment group (red hot needle, n=62) and control group (conventional acupuncture, n=47). The treatment was conducted beginning from the first day of the first 10 day period of the Dog Days. After successive two years’ treatment, results showed that of the 62 and 47 cases in treatment and control groups, 16 and 7 were cured basically, 37 and 16 had remarkable improvement, 8 and 12 were ameliorated, 1 and 10 failed in the treatment, with the effective rate being 98.4% and 78.7% respectively, displaying that the therapeutic effect of treatment group was significantly superior to that of control group (P<0.01). 展开更多
关键词 Asthma Red-hot NEEDLE therapy treatment in the three 10-day PERIODS of dog DAYS
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Hot Water Treatment Enhances the Bioherbicidal Efficacy of a Fungus
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作者 C. Douglas Boyette Robert E. Hoagland Kenneth C. Stetina 《American Journal of Plant Sciences》 2018年第10期2063-2076,共14页
Hemp sesbania (Sesbania exaltata) plants (>30 cm tall) sprayed with hot water (45&deg;C – 95&deg;C), followed by spray applications of fungal spores of Colletotrichum truncatum (CT) at 1.0 × 107 spore... Hemp sesbania (Sesbania exaltata) plants (>30 cm tall) sprayed with hot water (45&deg;C – 95&deg;C), followed by spray applications of fungal spores of Colletotrichum truncatum (CT) at 1.0 × 107 spores/ml-1 and 22&deg;C – 25&deg;C, suspended either in: 0.2% Silwet L-77 surfactant (SW);unrefined corn oil (CO)/distilled water (1:1, v:v);or 0.2% SW in CO were controlled by 80% - 95%, 12 days after treatment (DAT) under greenhouse conditions. These treatments also reduced dry weight accumulation of this weed. Plants treated with hot water without CT were also injured at temperatures ≥35&deg;C (5% mortality), and 60% mortality at 95&deg;C. Artificial dew treatments (25&deg;C, 12 h), imposed on plants after the treatment protocols above, had little or no effect on weed mortality or dry weight reduction compared to treated plants without dew. Under field conditions, 85% control of hemp sesbania was achieved 12 - 15 DAT when a pre-treatment with hot water (65&deg;C) was followed immediately with a CT application at the spore concentration as described above. Plants in field tests treated with CT without a hot water treatment were visually unaffected, with no mortality or plant biomass reductions recorded 15 DAT. These results suggest that use of hot water may be an important tool for improving the infectivity and bioherbicidal potential of some plant pathogens. 展开更多
关键词 BIOHERBICIDE MYCOHERBICIDE HEMP SESBANIA SESBANIA exaltata COLLETOTRICHUM truncatum hot Water Pre-treatment Improved BIOHERBICIDE EFFICACY Weed Control
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Vacuum Treatment for Simultaneous Desulphurization and Dephosphorization of Hot Metal and Molten Steel 被引量:1
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作者 WANG Hai-chuan WANG Shi-jun +2 位作者 ZHOU Yun WU Bao-guo DONG Yuan-chi 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2004年第2期14-17,共4页
The vacuum treatment for simultaneous desulphurization and dephosphorization of hot metal and molten steel with pre-melted CaO-based slag was carried out.For pre-treatment of hot metal,both desulphurization and dephos... The vacuum treatment for simultaneous desulphurization and dephosphorization of hot metal and molten steel with pre-melted CaO-based slag was carried out.For pre-treatment of hot metal,both desulphurization and dephosphorization are improved with the increase of CaO in slag,but deteriorated with the increase of CaF2 in slag.The average desulphurization and dephosphorization rate is 68.83 % and 78.46 %,respectively.For molten steel,the substitution of BaO for CaO in slag has minor effect on simultaneous desulphurization and dephosphorization.The desulphurization and dephosphorization rate is higher than 90% and 50% respectively with the lowest final sulfur and phosphorus mass percent being 0.001 2% and 0.010%,respectively.The overall effect of simultaneous desulphurization and dephosphorization of molten steel is better than that of hot metal. 展开更多
关键词 hot metal molten steel DESULPHURIZATION DEPHOSPHORIZATION CaO-based slag vacuum treatment
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一种新型纤维素基包装材料的研制与应用设计
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作者 岳花娟 王欢 《粘接》 CAS 2024年第2期69-72,共4页
针对生物可降解包装材料的高成本、性能低等问题,制备一种以黄麻纤维、粘胶纤维和聚乳酸玉米纤维为主要原料的的纤维素基包装材料,并对其力学性能进行探究。结果表明,热压处理有利于增强纤维抱合性,从而增加材料的稳定性;黄麻/粘胶/玉... 针对生物可降解包装材料的高成本、性能低等问题,制备一种以黄麻纤维、粘胶纤维和聚乳酸玉米纤维为主要原料的的纤维素基包装材料,并对其力学性能进行探究。结果表明,热压处理有利于增强纤维抱合性,从而增加材料的稳定性;黄麻/粘胶/玉米纤维最佳配比方案为50∶35∶15,此时,制备的复合包装材料的纵向断裂强力为212.35 N,横向断裂强力为126.78 N,纵向撕破强力为29.26 N,横向撕破强力为13.06 N,顶破强力为77.61 N。试验制备的黄麻/粘胶/玉米纤维素基包装材料不仅成本低、绿色环保,还具备较好的力学性能,能作为一种生物可降解包装材料应用于实际生活中。 展开更多
关键词 可降解 聚乳酸玉米纤维 热压处理 纤维素 力学性能
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桥梁缆索用87MnSi钢线材微观组织演变对力学性能的影响
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作者 屈小波 王淼 +7 位作者 曹磊 王鲁义 饶子才 纪文杰 吴彦欣 武晓燕 王天祥 江海涛 《特殊钢》 2024年第3期114-118,共5页
针对桥梁缆索用87MnSi钢线材的异常断裂现象,对其盘条和生产工艺过程中钢丝的微观组织和力学性能演变规律进行系统分析。结果表明,盘条组织由珠光体和少量的先共析铁素体组成,且渗碳体片层随机分布。冷拉拔后,渗碳体片层发生扭转弯曲或... 针对桥梁缆索用87MnSi钢线材的异常断裂现象,对其盘条和生产工艺过程中钢丝的微观组织和力学性能演变规律进行系统分析。结果表明,盘条组织由珠光体和少量的先共析铁素体组成,且渗碳体片层随机分布。冷拉拔后,渗碳体片层发生扭转弯曲或减薄纤维化,且部分渗碳体发生破碎溶解,溶解量为1.40%(占比9.69%)。热镀锌后,溶解的渗碳体发生球化。盘条(329.8HV)在冷拉拔-热镀锌-稳定化处理过程中的显微硬度呈现先增大(450.2HV)后减小(447.9HV)再增大(469.6HV)的变化趋势;冷拉拔过程中溶解的渗碳体使得钢丝硬度值上升至468.3HV,而热镀锌过程渗碳体的球化,导致硬度值下降至439.8HV,并恶化拉伸性能。当边部的渗碳体球化程度明显时,使得钢丝内外组织和力学性能存在较大差异,并在稳定化处理过程中因受力不均匀而导致断裂。 展开更多
关键词 桥梁缆索 87MnSi钢 热镀锌 稳定化处理 断裂 渗碳体球化
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4Cr5MoSiV1热作模具钢循环渗氮及热疲劳行为研究 被引量:2
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作者 刘海建 韩笑 陈杰 《热加工工艺》 北大核心 2024年第2期24-29,共6页
针对4Cr5MoSiV1热作模具钢在使用过程中经受熔融铝液及冷却液的循环冲击,在热应力作用下容易产生热疲劳失效的问题。采用可控循环气体渗氮的方法分别在回火态和热疲劳态模具钢表面制备无铁氮化合物和有化合物的渗层,进行热疲劳性能测试... 针对4Cr5MoSiV1热作模具钢在使用过程中经受熔融铝液及冷却液的循环冲击,在热应力作用下容易产生热疲劳失效的问题。采用可控循环气体渗氮的方法分别在回火态和热疲劳态模具钢表面制备无铁氮化合物和有化合物的渗层,进行热疲劳性能测试。结果表明:循环渗氮制备的无化合物的渗层可以有效延缓热疲劳裂纹的萌生,抗热疲劳性能优于有化合物的渗层。同时,在裂纹产生前进行二次渗氮可以补充氮原子,重置压应力并增加硬度,进一步提升热疲劳抗性。 展开更多
关键词 热作模具钢 可控循环气体渗氮 铁氮化合物 热疲劳性能
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原位生成周期性层片结构镀层及其在NaCl溶液中的腐蚀形貌
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作者 张先满 李星涛 +2 位作者 季坤鹏 陈再雨 罗洪峰 《材料导报》 EI CAS CSCD 北大核心 2024年第12期162-168,共7页
金属在海洋氯离子环境中极易发生腐蚀,并造成巨大的经济损失。通过制备新型Fe-Cr-B铸钢,采用热浸镀铝-扩散热处理原位生成含有周期性层片结构(PLSs)的镀层,并利用扫描电子显微镜(SEM)、电子探针X射线显微分析仪(EPMA)等手段研究了该镀... 金属在海洋氯离子环境中极易发生腐蚀,并造成巨大的经济损失。通过制备新型Fe-Cr-B铸钢,采用热浸镀铝-扩散热处理原位生成含有周期性层片结构(PLSs)的镀层,并利用扫描电子显微镜(SEM)、电子探针X射线显微分析仪(EPMA)等手段研究了该镀层的组织结构及其在3.5%(质量分数)NaCl溶液中的腐蚀行为。结果表明,该铸钢的显微组织主要由粗大的初生(Cr,Fe)_(2)B及α-Fe组成;热浸镀铝时在(Cr,Fe)_(2)B/Al界面上生成由FeAl3和Cr-Al-B相组成的PLSs,在α-Fe/Al界面上生成FeAl3;扩散热处理使得反应层增厚,且PLSs在反应层中大量生成;相比FeAl3,镀层中的PLSs在腐蚀过程中充当阳极优先腐蚀,并表现出腐蚀各向异性,尤其是其中的Cr-Al-B相可明显阻挡氯离子腐蚀,使得PLSs通过延长腐蚀路径进而提高镀层的耐氯离子腐蚀性能。 展开更多
关键词 Fe-Cr-B铸钢 热浸镀铝 扩散热处理 周期性层片结构(PLSs) 氯离子
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Effect of solution plus aging heat treatment on microstructural evolution and mechanical properties of near-β titanium alloy 被引量:22
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作者 Chuan WU Mei ZHAN 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第5期997-1006,共10页
The microstructural evolution, mechanical properties and fracture mechanism of a Ti.5Al.5Mo.5V.3Cr.1Zr (Ti-55531) alloy after solution (760.820℃) plus aging (580.640℃) treatments were investigated. The results show ... The microstructural evolution, mechanical properties and fracture mechanism of a Ti.5Al.5Mo.5V.3Cr.1Zr (Ti-55531) alloy after solution (760.820℃) plus aging (580.640℃) treatments were investigated. The results show that the volume fraction of the primary α(αp) phase decreases with the increase of solution temperature, and the length of the secondary α phase (αs) decreases while its width increases with the increase of aging temperature. Yield and tensile strengths decrease with the increase of solution temperature, while increase with the increase of aging temperature. A good balance of tensile strength and ductility of the alloy is obtained under solution of 800℃ for 2 h plus aging of 640℃ for 8 h, in which the tensile strength is 1434 MPa and the elongation is 7.7%. The coarsening αs phase makes crack propagation paths deflected and tortuous, which increases the crack propagation resistance and improves the ductility and fracture toughness. 展开更多
关键词 Ti.5Al.5Mo.5V.3Cr.1Zr titanium alloy hot treatment SOLUTION AGING microstructural evolution mechanical properties fracture mechanism
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贮前延迟联合热水处理对黄瓜果实冷藏期间冷害和生理代谢的影响
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作者 贾淼 张敏 +3 位作者 李奇勋 李玉申 王红婷 陈一锋 《安徽农业大学学报》 CAS CSCD 2024年第1期159-166,共8页
为探究黄瓜果实经热水处理后延迟方式对其冷藏期间品质和生理代谢的影响,根据前期利用二次正交旋转组合试验设计优化得出的延迟条件,以新鲜黄瓜为对照(CK),分别研究了水浴延迟(T1)、空气延迟(T2)和未延迟处理(T3)对经热激处理的黄瓜果实... 为探究黄瓜果实经热水处理后延迟方式对其冷藏期间品质和生理代谢的影响,根据前期利用二次正交旋转组合试验设计优化得出的延迟条件,以新鲜黄瓜为对照(CK),分别研究了水浴延迟(T1)、空气延迟(T2)和未延迟处理(T3)对经热激处理的黄瓜果实在(4±1)℃,相对湿度(80±5)%的冷库贮藏期间冷害(chilling injury,CI)症状、品质及抗氧化系统的影响。结果表明,低温贮藏3 d时,各组冷害指数最高仅为0.37,然而贮藏9 d时,CK和T3组果实冷害指数迅速升高至0.76和0.71,此时CK组冷害指数为T1和T2的1.25倍和1.21倍。而且T1和T2组能显著减缓果实失重率和电解质外渗率(electrolyte leakage,EL)的上升以及硬度的下降,同时能使果实保持较好色泽,维持较高的可溶性蛋白含量,有效减轻了丙二醛(malondialdehyde,MDA)、超氧阴离子(superoxide anion,O_(2)^(-)·)和过氧化氢(hydrogen peroxide,H_(2)O_(2))对果实的损伤;到贮藏末期,相比于CK,T1和T2组果实的H_(2)O_(2)含量分别降低了7.86%和11.64%。此外,T1和T2处理也能在一定程度上延缓过氧化氢酶(catalase,CAT)、过氧化物酶(peroxidase,POD)和还原型谷胱甘肽(reducedglutathione,GSH)含量的下降。综合分析,T1和T2处理组对于减轻黄瓜果实冷害,缓解品质劣变均有显著影响,可根据实际情况灵活选择适用性更高的处理方式。该研究对黄瓜贮藏保鲜技术的进一步完善有一定的理论和实践参考价值。 展开更多
关键词 贮前延迟 热水处理 黄瓜 抗氧化系统 冷害
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热处理技术对3D打印钛合金试件机械性能的影响 被引量:1
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作者 于露翔 张若槿 谭发兵 《中国组织工程研究》 CAS 北大核心 2024年第29期4741-4747,共7页
背景:近年来,增材制造(又称3D打印)逐渐成为制作可摘局部义齿钛合金支架的主流方式。热处理作为改善3D打印钛合金支架机械性能的重要方法而成为目前的关注热点。目的:总结目前应用于3D打印钛合金试件的主要热处理技术(包括退火处理、固... 背景:近年来,增材制造(又称3D打印)逐渐成为制作可摘局部义齿钛合金支架的主流方式。热处理作为改善3D打印钛合金支架机械性能的重要方法而成为目前的关注热点。目的:总结目前应用于3D打印钛合金试件的主要热处理技术(包括退火处理、固溶时效处理、热等静压处理及其他热处理)以及这些热处理技术对3D打印钛合金试件机械性能、微观结构的影响,为改进可摘局部义齿钛合金支架的热处理技术提供理论依据。方法:采用计算机检索中国知网、PubMed和ScienceDirect数据库中有关3D打印钛合金热处理试件的文献资料,检索时限为2012-2023年,根据纳入和排除标准,最终选取61篇文献进行综述分析。结果与结论:①使用常规退火技术处理3D打印钛合金试件,使其在500-900℃下保持2-4 h,能有效增加3D打印钛合金试件的延伸率。②固溶时效处理相较于常规退火技术更复杂,固溶时效处理后的钛合金试件在屈服强度方面表现突出,并且有更好的耐腐蚀性;但固溶时效处理后的3D打印钛合金试件在延伸性方面没有优势。③热等静压处理可以减少3D打印钛合金试件的内部缺陷,可明显增加3D打印钛合金试件延伸率,并增加其疲劳寿命。④快速热处理可以明显提高3D打印钛合金试件的延伸率,并且速度更快,在延伸率提升和热处理效率方面,比以往常规的退火更具优势。⑤循环热处理对3D打印钛合金试件延伸率的提升超过了常规退火,循环热处理可明显改善3D打印钛合金试件的晶粒结构,但热处理时间过长,效率较低。 展开更多
关键词 3D打印 钛合金 机械性能 可摘局部义齿 固溶时效处理 热等静压 退火 微观结构
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La处理对H13热作模具钢中夹杂物的影响 被引量:1
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作者 任吉 燕云 +4 位作者 田家龙 王礼超 蒋成钢 王琳 姜周华 《特殊钢》 2024年第4期117-123,共7页
采用真空感应炉熔炼H13模具钢,在氩气保护下加入稀土镧处理钢液并浇铸成钢锭,研究了La处理对H13钢中夹杂物转变的影响。结果表明,La对H13钢中夹杂物具有很好的改性效果,随La含量的提高,夹杂物的数量呈上升趋势,夹杂物的平均尺寸先减小... 采用真空感应炉熔炼H13模具钢,在氩气保护下加入稀土镧处理钢液并浇铸成钢锭,研究了La处理对H13钢中夹杂物转变的影响。结果表明,La对H13钢中夹杂物具有很好的改性效果,随La含量的提高,夹杂物的数量呈上升趋势,夹杂物的平均尺寸先减小后增大。不添加稀土时,H13钢中夹杂物主要为Al_(2)O_(3)和MnS;当H13钢中w[La]为0.016%时,钢中夹杂物以La_(2)O_(2)S为主;当w[La]为0.045%和0.073%时,钢中夹杂物主要为LaP和La_(2)O_(2)S。热力学计算表明,在1600℃下钢液中,La处理后夹杂物的转变过程为Al_(2)O_(3)→LaAlO_(3)→La_(2)O_(2)S。在凝固过程中,钢液中首先析出La_(2)S_(3),当温度继续降低,LaP开始在La_(2)S_(3)和La_(2)O_(2)S表面析出,最终形成复合夹杂物La_(2)O_(2)S-LaP和La_(2)S_(3)-LaP。 展开更多
关键词 H13热作模具钢 La处理 夹杂物 热力学计算
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热轧工艺对S32101经济型双相不锈钢低温冲击韧性的影响
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作者 梁祥祥 韩培德 李国平 《热加工工艺》 北大核心 2024年第17期118-121,126,共5页
为研究热轧工艺对S32101经济型双相不锈钢低温冲击韧性的影响,设计不同的展宽系数(1.0、1.1、1.4)和压下率(75%、90%)进行热轧试验。在计算热力学相图并分析不同温度组织转变规律的基础上,选择合理的固溶处理工艺,研究热轧工艺对固溶处... 为研究热轧工艺对S32101经济型双相不锈钢低温冲击韧性的影响,设计不同的展宽系数(1.0、1.1、1.4)和压下率(75%、90%)进行热轧试验。在计算热力学相图并分析不同温度组织转变规律的基础上,选择合理的固溶处理工艺,研究热轧工艺对固溶处理后S32101双相不锈钢低温冲击韧性的影响。结果表明:不同热轧工艺下,S32101双相不锈钢低温冲击韧性随展宽系数和压下率的增加而提高;随固溶处理温度的升高和保温时间的延长而降低。随展宽系数和压下率的增加,奥氏体和铁素体条带间距减小并沿轧向分布。减小两相条带间距,提高奥氏体相比例可提高低温冲击韧性。 展开更多
关键词 双相不锈钢 热轧 固溶处理 冲击韧性
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