Hot deformation is one of the primary methods for fabricating anisotropic rare earth permanent magnets. Firstly,rapidly quenched powder flakes with a nanocrystal structure are condensed into fully dense isotropic prec...Hot deformation is one of the primary methods for fabricating anisotropic rare earth permanent magnets. Firstly,rapidly quenched powder flakes with a nanocrystal structure are condensed into fully dense isotropic precursors using the hot-pressing process. The prepared isotropic precursors are then hot-deformed to produce high-anisotropy uniaxial bulk rare earth permanent magnets and a highly textured structure is produced via this process. The resulting magnets possess many advantages such as near-net-shape, outstanding corrosion resistance, and ultrafine-grain structure. The influence of the preparation parameters utilized in the hot-pressing and deformation processes on the magnetic properties and microstructure of the permanent magnets are systemically summarized in this report. As a near-net-shape technique, the hot deformation process has notable advantages with regard to the production of irregular shapes, especially for radially oriented ringshaped magnets with high length-diameter ratios or thin walls. The difficulties associated with the fabrication of crack-free,homogeneous, and non-decentered ring-shaped magnets are substantially resolved through an emphasis on mold design,adjustment of deformation parameters, and application of theoretical simulation. Considering the characteristics of hotdeformed magnets which include grain shape and size, anisotropic distribution of intergranular phases, etc., investigation and improvement of the mechanical and electric properties, in addition to thermal stability, with the objective of improving the application of hot-deformed magnets or ring-shaped magnets, is of practical significance.展开更多
Radially oriented Nd-Fe-B ring magnets were prepared by backward extrusion of MQ-C powder. The punch chamfer radius has a great impact on the microstructure and magnetic properties of the ring magnet. With the chamfer...Radially oriented Nd-Fe-B ring magnets were prepared by backward extrusion of MQ-C powder. The punch chamfer radius has a great impact on the microstructure and magnetic properties of the ring magnet. With the chamfer radius changing from 2, 5 to 8 mm, the cracks in the inner wall decrease obviously while the crystallographic alignment drops. Furthermore, the mechanism of caxis growth was suggested to be a combination of shear deformation in the corner and solution-precipitation under the stress parallel to radial direction. The alignment drops on the top of ring because the grains grow freely and some textured grains grow through nucleation and recrystallization. In the present work, the optimal punch chamfer radius is found to be 2 mm, and in this case, the remanence,coercivity, and maximum energy product of the ring magnet achieve 1.4 T, 670 kJám, and 342 kJám,respectively.展开更多
基金Project supported by the National Key Research and Development Program of China(Grant No.2016YFB0700902)the National Natural Science Foundation of China(Grant Nos.51671207,51601207,and 51501213)
文摘Hot deformation is one of the primary methods for fabricating anisotropic rare earth permanent magnets. Firstly,rapidly quenched powder flakes with a nanocrystal structure are condensed into fully dense isotropic precursors using the hot-pressing process. The prepared isotropic precursors are then hot-deformed to produce high-anisotropy uniaxial bulk rare earth permanent magnets and a highly textured structure is produced via this process. The resulting magnets possess many advantages such as near-net-shape, outstanding corrosion resistance, and ultrafine-grain structure. The influence of the preparation parameters utilized in the hot-pressing and deformation processes on the magnetic properties and microstructure of the permanent magnets are systemically summarized in this report. As a near-net-shape technique, the hot deformation process has notable advantages with regard to the production of irregular shapes, especially for radially oriented ringshaped magnets with high length-diameter ratios or thin walls. The difficulties associated with the fabrication of crack-free,homogeneous, and non-decentered ring-shaped magnets are substantially resolved through an emphasis on mold design,adjustment of deformation parameters, and application of theoretical simulation. Considering the characteristics of hotdeformed magnets which include grain shape and size, anisotropic distribution of intergranular phases, etc., investigation and improvement of the mechanical and electric properties, in addition to thermal stability, with the objective of improving the application of hot-deformed magnets or ring-shaped magnets, is of practical significance.
基金financially supported by the National High Technology Research and Development Program of China (No. 2011AA03A403)the National Natural Science Foundation of China (No. 51171122)the Sichuan Provence Science and Technology Support Program (Nos. 2011GZ0117 and 2013GZ0056)
文摘Radially oriented Nd-Fe-B ring magnets were prepared by backward extrusion of MQ-C powder. The punch chamfer radius has a great impact on the microstructure and magnetic properties of the ring magnet. With the chamfer radius changing from 2, 5 to 8 mm, the cracks in the inner wall decrease obviously while the crystallographic alignment drops. Furthermore, the mechanism of caxis growth was suggested to be a combination of shear deformation in the corner and solution-precipitation under the stress parallel to radial direction. The alignment drops on the top of ring because the grains grow freely and some textured grains grow through nucleation and recrystallization. In the present work, the optimal punch chamfer radius is found to be 2 mm, and in this case, the remanence,coercivity, and maximum energy product of the ring magnet achieve 1.4 T, 670 kJám, and 342 kJám,respectively.