Research progress and application of deep in-situ condition preserved coring and testing

With the depletion of shallow resources,the exploration of deep earth resources has become a global strategy.The study of the different patterns in the physical mechanical properties of rocks at different occurrence depths is the basis for exploring deep into the earth,with the core and premise being the acquisition and testing of deep in-situ core specimens.Based on the original idea of deep in-situ condition preserved coring(ICP-Coring)and testing,combined with theoretical modeling,numerical analysis,test platform development,indoor testing and engineering application,the principles and technologies of deep ICP-Coring are developed.This principle and technology consists of five parts:in-situ pressurepreserved coring(IPP-Coring),in-situ substance-preserved coring(ISP-Coring),in-situ temperaturepreserved coring(ITP-Coring),in-situ light-preserved coring(ILP-Coring),and in-situ moisturepreserved coring(IMP-Coring).The theory and technology of temperature and pressure reconstruction at different occurrence depths and in different environments are proposed,and prototype trial production was completed by following the principle of displacement and tests based on the in-situ reconstructed environment.The notable advances are as follows:(1)Deep in-situ coring system:A pressure-preserved controller with an ultimate bearing capacity greater than 140 MPa,highperformance(temperature-resistant,pressure-resistant,and low thermally conductive)temperaturepreserved materials,an active temperature control system,and high-barrier quality-preserved membrane materials were developed;a deep ICP-Coring capacity calibration platform was independently developed,a deep in-situ coring technology system was developed,and the acquisition of deep in-situ cores was realized.(2)In-situ storage displacement system:Following the dual-circuit hydraulic design idea,a single-drive source push-pull composite grabbing mechanism was designed;the design of the overall structure for the deep in-situ displacement storage system and ultrahigh pressure cabin structure was completed,which could realize docking the coring device and core displacement in the in-situ reconstructed environment.(3)Test analysis system:A noncontact acoustic-electric-magnetic test system was developed under the in-situ reconstructed environment,and the errors between the test results and traditional contact test results were mostly less than 10%;a detachable deep in-situ core true triaxial test system was developed,which could perform loading tests for deep in-situ cores.The relevant technological achievements were successfully applied to the exploration and development of deep resources,such as deep mines,deep-sea natural gas hydrates,and deep oil and gas.The research results provide technical and equipment support for the construction of a theoretical system for deep in-situ rock mechanics,the development of deep earth resources and energy,and the scientific exploration of different layers and occurrence depths(deep and ultradeep)of the Earth.

Design and feasibility analysis of a new completion monitoring technical scheme for natural gas hydrate production tests

As a prerequisite and a guarantee for safe and efficient natural gas hydrates(NGHs)exploitation,it is imperative to effectively determine the mechanical properties of NGHs reservoirs and clarify the law of the change in the mechanical properties with the dissociation of NGHs during NGHs production tests by depressurization.Based on the development of Japan’s two offshore NGHs production tests in vertical wells,this study innovatively proposed a new subsea communication technology-accurate directional connection using a wet-mate connector.This helps to overcome the technical barrier to the communication between the upper and lower completion of offshore wells.Using this new communication technology,this study explored and designed a mechanical monitoring scheme for lower completion(sand screens).This scheme can be used to monitor the tensile stress and radial compressive stress of sand screens caused by NGHs reservoirs in real time,thus promoting the technical development for the rapid assessment and real-time feedback of the in-situ mechanical response of NGHs reservoirs during offshore NGHs production tests by depressurization.

基于SEM多级化孔隙特征研究——以重塑黄土为例

为了探究扫描电镜(SEM)下多尺度微观孔隙特征,确定孔隙定量分析的最佳放大倍数,利用IPP 6.0软件对12种不同放大倍数(包括100X、200X、300X、400X、500X、600X、800X、1000X、1200X、1500X、2000X、3000X)下8个不同干密度的重塑黄土试样的SEM图像进行孔隙多级化分析,并依据雷祥义的黄土孔隙分类标准对孔隙进行统计分类。结果表明:在放大倍数小于400X时,任何干密度试样的SEM图像都无法观察到微孔隙,在放大倍数大于1000X时,无法观察到大孔隙,而在放大倍数介于400~1000X时,基本可以观察到不同类型的孔隙;基于多元统计学中的聚类分析,得到放大倍数的分类结果与IPP 6.0软件对SEM图像的处理统计结果相一致;不同干密度试样多级化孔隙特征的差异主要是由土体密实度变化使得不同孔隙类型转化而引起的;随着放大倍数的增大,视域变小,大孔隙越难统计;反之,放大倍数越小,视域越大,微孔隙越容易被忽略;在综合考虑微孔隙和大孔隙的分布及其含量下,最佳观察倍数应介于500~800X之间。该研究不仅有助于揭示重塑黄土基于SEM多级化孔隙特征,同时对地质工程领域土体微结构定量表征具有借鉴价值。

SEMS系统引入机动车排放检测可行性研究

机动车排放实验室测试与实际道路测试结果间存在较大差距,目前实际道路测试普遍采用车载排放系统(portable emission measurement system,PEMS),但PEMS系统具有操作复杂、测试装置整体较重等缺点,急需简单易行的实际道路排放测试系统。基于传感器技术的机动车智能排放测试系统(smart emission measurement system,SEMS),结构简单,操作方便,将其引入机动车实际行驶排放检测非常必要,但国内缺乏SEMS系统测试应用相关研究。通过研究国内外SEMS系统现状,并开展相关对比测试试验,研究SEMS系统引入机动车排放检测可行性与存在的问题。结果表明:SEMS系统测试的颗粒物数量(PN)与PEMS测试结果的差异为10%~30%;氮氧化物(NO_(x))排放量与实际道路对比测试结果差异较大,特别是激烈驾驶情况下,最大差异高达369%;PN和NO_(x)排放测试结果瞬时分布和累计分布趋势较为一致。基于测试试验及结果分析,探讨了SEMS系统引入机动车排放检测的可行性,提出SEMS系统引入机动车排放检测具备一定可行性,可用于NO_(x)和PN高排放车辆筛查。

Research on in-situ condition preserved coring and testing systems

As shallow resources are increasingly depleted,the mechanics'theory and testing technology of deep insitu rock has become urgent.Traditional coring technologies obtain rock samples without retaining the in-situ environmental conditions,leading to distortion of the measured parameters.Herein,a coring and testing systems retaining in-situ geological conditions is presented:the coring system that obtains in-situ rock samples,and the transfer and testing system that stores and analyzes the rocks under a reconstructed environment.The ICP-Coring system mainly consists of the pressure controller,active insulated core reactor and insulation layer and sealing film.The ultimate bearing strength of 100 MPa for pressurepreservation,temperature control accuracy of 0.97%for temperature-retained are realized.CH_(4)and CO permeability of the optimized sealing film are as low as 3.85 and 0.33 ppm/min.The average tensile elongation of the film is 152.4%and the light transmittance is reduced to 0%.Additionally,the pressure and steady-state temperature accuracy for reconstructing the in-situ environment of transfer and storage system up to 1%and±0.2 is achieved.The error recorded of the noncontact sensor ring made of lowdensity polymer is less than 6%than that of the contact test.The system can provide technical support for the deep in-situ rock mechanics research,improving deep resource acquisition capabilities and further clarifying deep-earth processes.

Assessment of rapid impact compaction in ground improvement from in-situ testing

Ground improvement has been used on many construction sites to densify granular materials, in other word, to improve soil properties and reduce potential settlement. This work presents a case study of ground improvement using rapid impact compaction （RIC）. The research site comprises the construction of workshop and depots as part of railway development project at Batu Gajah-Ipoh, Malaysia. In-situ testing results show that the subsurface soil comprises mainly of sand and silty sand through the investigated depth extended to 10 m. Groundwater is approximately 0.5 m below the ground surface. Evaluation of improvement was based on the results of pre- and post-improvement cone penetration test （CPT）. Interpretation software has been used to infer soil properties. Load test was conducted to estimate soil settlement. It is found that the technique succeeds in improving soil properties namely the relative density increases from 45% to 70%, the friction angle of soil is increased by an average of 3°, and the soil settlement is reduced by 50%： The technique succeeds in improving soil properties to approximately 5.0 m in depth depending on soil uniformity with depth.

In-situ SEM observation on fracture behavior of austempered silicon alloyed steel

Crack initiation, propagation and microfracture processes of austempered high silicon cast steel have been investigated by using an in-situ tensile stage installed inside a scanning electron microscope chamber. It is revealed that micro cracks always nucleate at the yielding near imperfections and the boundary of matrix-inclusions due to the stress concentration. There are four types of crack propagations in the matrix: crack propagates along the boundary of two clusters of bainitic ferrite; crack propagates along the boundary of ferrite-austenite in bainitic ferrite laths; crack propagates into bainitic ferrite laths; crack nucleates and propagates in the high carbon brittle plate shape martensite which is transformed from some blocky retained austenite due to plastic deformation. Based on the observation and analysis of microfracture processes, a schematic diagram of the crack nucleation and propagation process of high silicon cast steel is proposed.

In-Situ Test on Fatigue Characteristics of Top-Mounted Dividable Pile-Board Subgrade for High-Speed Railway

To simulate the fatigue characteristics of the pile-board structure under long-term dynamic load, using the in-situ dynamic testing system DTS-1, the forced vibration loading was repeated one million times at different cross-sections of the pile-board structure for high-speed railway. The dynamic deformation, permanent deformation and dynamic stress of main reinforcements were measured. The test results show that the dynamic responses of the pile-board structure almost did not vary with the forced vibration times under the simulated trainload. After one million times of forced vibration, the permanent deformations of the midspan section of intermediate span and midspan section of side span were 0.7 mm and 0. 6 mm, respectively, and there was no accumulative plastic deformation at the bearing section of intermediate span.

SEM in-situ investigation on fatigue cracking behavior of P/M Rene95 alloy with surface inclusions

The low-cycle fatigue behavior of powder metallurgy Rene95 alloy containing surface inclusions was investigated by in-situ observation with scanning electron microscopy （SEM）. The process of fatigue crack initiation and early stage of propagation behavior indicates that fatigue crack mainly occurs at the interface between the inclusion and the matrix. The effect of inclusion on the fatigue crack initiation and the early stage of crack growth was very obvious. The fatigue crack growth path in the matrix is similar to the shape of inclusion made on the basis of fatigue fracture image analysis. The empiric relation between the surface and inside crack growth length, near a surface inclusion, can be expressed. Therefore, the fatigue crack growth rate or life of P/M Rene95 alloy including the inclusions can be evaluated on the basis of the measurable surface crack length parameter. In addition, the effect of two inclusions on the fatigue crack initiation behavior was investigated by the in-situ observation with SEM.

Effects of temperature and wavelength choice on in-situ dissolution test of Cimetidine tablets

The effects of temperature and wavelength choice on in-situ dissolution test instrument of Cimetidine were studied. Absorbance （A）〈 1.0 is required when using a fiber-optic dissolution test system. The detection wavelength of 2 （218 nm） was replaced by 244 nm to carry out this test. The absorbance of Cimetidine solution at different temperature showed an obvious change. Calibration of Cimetidine solution should be tested at the same temperature （37° C） with the test solution. A suitable wavelength with smaller tangent slope could be chosen for in-situ dissolution test of Cimetidine tablets.

Characterization of microstructure and strain response in Ti-6Al-4V plasma welding deposited material by combined EBSD and in-situ tensile test

Additive layer manufacturing （ALM） of aerospace grade titanium components shows great promise in supplying a cost-effective alternative to the conventional production routes. Complex microstructures comprised of columnar remnants of directionally solidifiedβ-grains, with interior inhabited by colonies of finerα-plate structures, were found in samples produced by layered plasma welding of Ti-6Al-4V alloy. The application of in-situ tensile tests combined with rapid offline electron backscatter diffraction （EBSD） analysis provides a powerful tool for understanding and drawing qualitative correlations between microstructural features and deformation characteristics. Non-uniform deformation occurs due to a strong variation in strain response between colonies and across columnar grain boundaries. Prismatic and basal slip systems are active, with the prismatic systems contributing to the most severe deformation through coarse and widely spaced slip lines. Certain colonies behave as microstructural units, with easy slip transmission across the entire colony. Other regions exhibit significant deformation mismatch, with local build-up of strain gradients and stress concentration. The segmentation occurs due to the growth morphology and variant constraints imposed by the columnar solidification structures through orientation relationships, interface alignment and preferred growth directions. Tensile tests perpendicular to columnar structures reveal deformation localization at columnar grain boundaries. In this work connections are made between the theoretical macro- and microstructural growth mechanisms and the observed microstructure of the Ti-6Al-4V alloy, which in turn is linked to observations during in-situ tensile tests.

The Quantification of Micro-structural Damage of Weak Muddy Intercalation in Dry-wet Cycles Combining in-situ SEM and DIP

In order to reflect truly the damage evolution mechanism of weak muddy intercalation in dry-wet cycles, two typical weak muddy intercalations were selected for dry-wet cycles. The mineral changes of specimens were analyzed via X-ray diffraction after dry-wet cycles. By combining in-situ SEM and digital image processing(DIP), the damage evolution process and damage characteristic parameters of each stage were obtained. The experimental results indicate that the hydration and dissolution of minerals can not be a determinant factor in structure damage. The micro-structural damage is due to disintegration of mineral aggregates, leading to changes in the number and size of cracks and pores. The damage degree of specimens is related to its initial structure, and the micro-structural damage intensifies and finally tends to stabilize with cycle times increased.

Research of in-situ hydraulic test method by using double packer equipment

Double packer equipment for hydraulic test can be used to measure pressure of test zone directly, and it is frequently used to perform many kinds of hydraulic tests and take groundwater sample from borehole. The test method of this equipment mainly includes the test design, implementation, interpretation and synthetic analysis. By adopting the double packer equipment for hydraulic test, the parameter distribution of rock permeability along borehole can be acquired, as well as the connectivity, water conductivity and water bearing capacity of the disclosed structure and the chemical characteristics of the deep groundwater. It is a necessary method for the research and evaluation of the complex hypotonicity terrace site selection under geological conditions. This method is not only suitable for the geological disposal of high level radioactive waste, but also can be used in the site selection of underground facilities such as storage of petroleum and carbon dioxide. Meanwhile, it has a good application prospect in other hydrogeological investigation fields.

SEM in-situ Fatigue Observation on Crack Initiation and Growth from Inclusion in P/M Rene95 Superalloy

A special designed experiment was conducted for observing crack initiation and growth in P/M Rene95 superalloy under tension-tension loading by self-made SEM in-situ fatigue loading stag. Several alumina inclusion particles exposed at the specimen surface were observed carefully. During fatigue test inclusions led to cracks initiation. The cracks can be formed by two mechanisms. Generally, the cracks nucleated at the interface between inclusion and matrix. Sometimes, cracks were also formed inside the inclusion. As the increase of cycles, some cracks at the interface between inclusion and matrix broadened and propagated along the direction about 45 degrees to the loading axis. On the other hand, the cracks inside the inclusion propagated in the inclusion and towards matrix.

SEM In-situ Observation at Tensile Loading on Surface Inclusion in PM Rene95 Superalloy

The observation on crack initiation and propagation of surface inclusion Al2O3 in seeded PM Rene95 was conducted by SEM in-situ tension test. The results show that the cracks often initiate at the inclusion/matrix interface vertical to the applied stress direction, and easily propagate along the interface into the matrix. The interface of inclusion/matrix is just mechanically bounded on the base of SEM observation. The weak bonding of inclusion/matrix interface and stress concentration around inclusions are the main reasons of the matrix/inclusion interface debonding and local plastic deformation under the tensile loading in the in-situ tension test. Surface inclusion does not definitely lead to the failure of in-situ tension test. But the early surface crack initiation caused by ceramic inclusion is critically harmful to the LCF property of PM Rene95 superalloy, which can't be ignored.

SEM in-situ Fracture Observation and the Reinforcing Effect of Composite SiC_p/ZA22

The strengthening effect of a Zn alloy reinforced by SiC particulate was examined. Based on the results of SEM in-situ fracture observation and stress field analysis by finite element method, it is believed that the reinforcing effect of this composite is due to the combination of strain and stress hardening in the matrix.

Discussion on bearing capacity of soft rock ground based on in-situ load test

The suitability of five methods was discussed here,taking the typical results from in-situ load test of Renshou Mansion and Caifu Plaza in Yueyang City for example.It shows that bearing capacity can be obtained by the proportion load and limit load from p-s curve with the first and the second point of contraflexure easily.It is recommended that the accurate value of bearing capacity can be obtained by hyperbola fitting method and minimum curvature radius method theoretically.The rebound method is clear in principle,in which the elastoplasticity characteristic is thought about.Out of consideration for the unsteadiness and unobviousness of bearing capacity from relative settlement method,it can be only adopted as reference.So bearing capacity of soft rock ground should be determined by weathering condition of soft rock and curve type.

Study on determination method of in-situ stress using formation fracturing test and Kaiser effect method

A new method, which is based on formation fracturing test and Kaiser effect method, has been developed for confirming the oilfield in-situ stress in this paper. The new method has been used in a certain oilfield of China and the determined oilfield in-situ stresses is more accurate than that based on one single method.

胶粉纤维改性水泥稳定碎石抗裂性能研究

针对水泥稳定碎石基层易开裂问题,在混合料中掺入适量胶粉及聚乙烯醇(PVA)纤维,开展强度、抗压回弹模量、干缩性能和扫描电镜试验(SEM);分别掺入橡胶粉、改性胶粉、PVA纤维、不同水泥剂量的胶粉纤维,对比其对混合料抗裂性能的影响。发现掺入材料对水泥稳定碎石混合料性能具有明显影响。掺入胶粉、改性胶粉后会降低混合料强度和抗压回弹模量,提升抗干缩性能;掺入纤维能增强混合料强度、模量和抗干缩性能;加入不同水泥剂量的胶粉纤维对混合料强度、抗压回弹模量提升效果明显,但降低了抗干缩性能;宏观力学指标试验和SEM试验结果显示出改性胶粉纤维与水泥基具有良好的黏结性,可以提升水泥稳定碎石混合料的抗裂能力。

含泥量对砂类硫酸盐渍土工程特性的影响分析

为了明确含泥量对砂类硫酸盐渍土的盐胀和力学特性的影响,人工配制了不同细粒土含量的砂类硫酸盐渍土,在1%和3%(质量分数,下同)含盐量单向冻结盐胀试验的基础上,选取了细粒土含量为5%、15%、30%和40%的砂样进行常温、低温三轴剪切试验。研究结果表明:此试验条件下,不同级配砂类硫酸盐渍土的冻结温度为-0.7~-0.1℃,当砂样孔隙溶液浓度在冻结温度之上达到饱和时,降温过程中会首先生成盐结晶;1%含盐量条件下,高细粒土含量(≥30%)砂样的起胀温度在4~9℃之内,而低细粒土含量砂样的起胀温度在0℃附近,3%含盐量砂样的起胀温度为20~23℃;试验含水率和细粒土含量通过影响土体中自由水的含量对盐冻胀产生显著影响。在力学特性方面,随着细粒土掺量的增加,砂类硫酸盐渍土的抗剪强度表现出先增大后减小的趋势,细粒土由增强摩擦转变为颗粒间的“润滑”作用;此外,冻结后砂土转变为承载能力更强的“土-盐-冰骨架结构”,抗剪强度大幅提高,并呈现出明显的脆性破坏特征,由于冻结砂土受相对温度的影响,随着含盐量的增加,破坏应力呈先减小后增大的趋势。