The microstructure of 40Cr steel sample and its surface is ultra-fined through salt-bath cyclic quenching and high frequency hardening, then the superplasticity is studied under isothermal superplastic compressive def...The microstructure of 40Cr steel sample and its surface is ultra-fined through salt-bath cyclic quenching and high frequency hardening, then the superplasticity is studied under isothermal superplastic compressive deformation condition. The experimental results indicate that the stress-strain curves are shown to take place obvious superplastic flow characteristic at the temperature of 750-770℃ and at the initial strain rate of (1.7-5.0)×10-4 s-1. Its strain rate sensitivity is 0.30-0.38, the steady superplastic flow stress is 60-70MPa, the superplastic flow activation energy is 198-217kJ/mol, and it is close to α-Fe grain boundary self-diffusion activation energy. The super-plastic compressive constitute equations of this steel are correspondingly set up. Due to the finer microstructure of high frequency hardening, it appears bigger strain rate sensitivity value, smaller the steady superplastic flow stress and the superplastic flow activation energy, so it has better superplastic deformation capability.展开更多
The superplastic behavior of a commercial duplex stainless steel has beenstudied by means of isothermal hot tensile test at temperatures of 850-1050 deg C for the initialstrain rates ranging from 3X10^(-4) s^(-1) to 5...The superplastic behavior of a commercial duplex stainless steel has beenstudied by means of isothermal hot tensile test at temperatures of 850-1050 deg C for the initialstrain rates ranging from 3X10^(-4) s^(-1) to 5X10^(-2) s^(-1). At 960 deg C, the best superplasticdeformation that caused the maximum elongation greater than 840 percent was obtained for an initialstrain rate of 1.2X10^(-3) s^(-1). At 850 deg C, the best elongation 500 percent was achieved for aninitial strain rate of 2.5X10^(-3) s^(-1) During the deformation in higher temperature region,coarse gamma grains formed during the prior treatments were broken into spherical particles,resulting in a homogeneous dispersion of gamma particles within the delta-ferrite matrix. However,at lower temperatures between 800 and 950 deg C, the sigma phase was formed through the eutectoiddecomposition of delta->gamma+sigma, resulting finally in the stable equiaxed micro-duplexstructures with delta/gamma and gamma/sigma respectively. The precipitation of the sigma phaseplayed an important role in improving the superplasticity at 850 deg C. The strain-rate sensitivitycoefficient, m-values, were also determined by the strain rate change tests. The microstructurestudies show that the superplastic process occurs mainly by the local work hardening and thesubsequent dynamic recrystallization and a grain boundary sliding and grain switching mechanism.展开更多
The investigation on the superplastic bugling capability of 1.5?mm mill annealed Ti 6Al 4V buttcover plate by means of manual gas tungsten arc welding (M GTAW) and fusion type plasma arc welding (F PAW) have been eval...The investigation on the superplastic bugling capability of 1.5?mm mill annealed Ti 6Al 4V buttcover plate by means of manual gas tungsten arc welding (M GTAW) and fusion type plasma arc welding (F PAW) have been evaluated respectively. The result shows that untreated Ti 6Al 4V buttcover plate by M GTAW exhibits no superplasticity, while the same untreated plate by F PAW, shows good superplastic ability because of extremely fine acicular martensite microstructure of weld metal. To the buttcover plate by M GTAW, the microstructure of weld metal changed into streaky α structure which exhibits good superplasticity from the original β structure under the condition of the constant temperature of 940?℃ with the deformation degree of 45%, and changed into the fine equiaxed grain which possesses excellent superplastic ability under the condition of the constant temperature of 800?℃ with the deformation degree of 40%.展开更多
基金supported by State Key Laboratory of New Nonferrous Metal Materials Natural Science Foundation of He'nan Province,China(No.984040900)Natural Science Foundation of the Education Department of He'nan Province,China(No.2003430211).
文摘The microstructure of 40Cr steel sample and its surface is ultra-fined through salt-bath cyclic quenching and high frequency hardening, then the superplasticity is studied under isothermal superplastic compressive deformation condition. The experimental results indicate that the stress-strain curves are shown to take place obvious superplastic flow characteristic at the temperature of 750-770℃ and at the initial strain rate of (1.7-5.0)×10-4 s-1. Its strain rate sensitivity is 0.30-0.38, the steady superplastic flow stress is 60-70MPa, the superplastic flow activation energy is 198-217kJ/mol, and it is close to α-Fe grain boundary self-diffusion activation energy. The super-plastic compressive constitute equations of this steel are correspondingly set up. Due to the finer microstructure of high frequency hardening, it appears bigger strain rate sensitivity value, smaller the steady superplastic flow stress and the superplastic flow activation energy, so it has better superplastic deformation capability.
文摘The superplastic behavior of a commercial duplex stainless steel has beenstudied by means of isothermal hot tensile test at temperatures of 850-1050 deg C for the initialstrain rates ranging from 3X10^(-4) s^(-1) to 5X10^(-2) s^(-1). At 960 deg C, the best superplasticdeformation that caused the maximum elongation greater than 840 percent was obtained for an initialstrain rate of 1.2X10^(-3) s^(-1). At 850 deg C, the best elongation 500 percent was achieved for aninitial strain rate of 2.5X10^(-3) s^(-1) During the deformation in higher temperature region,coarse gamma grains formed during the prior treatments were broken into spherical particles,resulting in a homogeneous dispersion of gamma particles within the delta-ferrite matrix. However,at lower temperatures between 800 and 950 deg C, the sigma phase was formed through the eutectoiddecomposition of delta->gamma+sigma, resulting finally in the stable equiaxed micro-duplexstructures with delta/gamma and gamma/sigma respectively. The precipitation of the sigma phaseplayed an important role in improving the superplasticity at 850 deg C. The strain-rate sensitivitycoefficient, m-values, were also determined by the strain rate change tests. The microstructurestudies show that the superplastic process occurs mainly by the local work hardening and thesubsequent dynamic recrystallization and a grain boundary sliding and grain switching mechanism.
文摘The investigation on the superplastic bugling capability of 1.5?mm mill annealed Ti 6Al 4V buttcover plate by means of manual gas tungsten arc welding (M GTAW) and fusion type plasma arc welding (F PAW) have been evaluated respectively. The result shows that untreated Ti 6Al 4V buttcover plate by M GTAW exhibits no superplasticity, while the same untreated plate by F PAW, shows good superplastic ability because of extremely fine acicular martensite microstructure of weld metal. To the buttcover plate by M GTAW, the microstructure of weld metal changed into streaky α structure which exhibits good superplasticity from the original β structure under the condition of the constant temperature of 940?℃ with the deformation degree of 45%, and changed into the fine equiaxed grain which possesses excellent superplastic ability under the condition of the constant temperature of 800?℃ with the deformation degree of 40%.
