A review of ^(17)O isotopic labeling techniques for solid-state NMR structural studies of metal oxides in lithium-ion batteries

Recent advances in utilizing ^(17)O isotopic labeling methods for solid-state nuclear magnetic resonance(NMR)investigations of metal oxides for lithium-ion batteries have yielded extensive insights into their structural and dynamic details.Herein,we commence with a brief introduction to recent research on lithium-ion battery oxide materials studied using ^(17)O solid-state NMR spectroscopy.Then we delve into a review of ^(17)O isotopic labeling methods for tagging oxygen sites in both the bulk and surfaces of metal oxides.At last,the unresolved problems and the future research directions for advancing the ^(17)O labeling technique are discussed.

Influence of ear tags on the results of body composition analysis in mice

Background:The aim of this study was to investigate the influence of marking meth-ods on the outcomes of body composition analysis and provide guidance for the se-lection of marking methods in mouse body composition analysis.Methods:Male C57BL/6J mice aged 6 weeks were randomly assigned for pre-and post-ear tagging measurements.The body composition of the mice was measured using a small animal body composition analyzer,which provided measurements of the mass of fat,lean,and free fluid.Then,the mass of fat,lean and free fluid to body weight ratio was gained.Further data analysis was conducted to obtain the range and coeffi-cient of variation in body composition measurements for each mouse.The distribution of fat and lean tissue in the mice was also analyzed by comparing the fat-to-lean ratio.Results:(1)The mass of all body composition components in the ear tagging group was significantly lower than that in the control group.(2)There was a significant in-crease in the range and coefficient of variation of body composition measurements between the ear tagging group and the control group.(3)The fat-to-lean ratio in the ear tagging group was significantly lower than that in the control group.Conclusions:Ear tagging significantly lowered the results of body composition analy-sis in mice and higher the results of measurement error.Therefore,ear tagging should be avoided as much as possible when conducting body composition analysis experi-ments in mice.

First-Arrival Picking Method for Active Source Data with Ocean Bottom Seismometers Based on Spatial Waveform Variation Characteristics

The precision and reliability of first-arrival picking are crucial for determining the accuracy of geological structure inversion using active source ocean bottom seismometer(OBS)refraction data.Traditional methods for first-arrival picking based on sample points are characterized by theoretical errors,especially in low-sampling-frequency OBS data because the travel time of seismic waves is not an integer multiple of the sampling interval.In this paper,a first-arrival picking method that utilizes the spatial waveform variation characteristics of active source OBS data is presented.First,the distribution law of theoretical error is examined;adjacent traces exhibit variation characteristics in their waveforms.Second,a label cross-correlation superposition method for extracting highfrequency signals is presented to enhance the first-arrival picking precision.Results from synthetic and field data verify that the proposed approach is robust,successfully overcomes the limitations of low sampling frequency,and achieves precise outcomes that are comparable with those of high-sampling-frequency data.

High-temperature thermal stability of C/C−ZrC−SiC composites via region labeling method

To investigate the thermal stability of ceramic-matrix composites,three kinds of C/C−ZrC−SiC composites with different Zr/Si molar ratios were synthesized by reactive melt infiltration.Employing region labeling method,the high-temperature thermal stability of the composites was systematically studied by changing the temperature and holding time of thermal treatment.Results show that the mass loss rate of low Si composites has a growth trend with increasing temperature,and a crystal transformation from β-SiC toα-SiC occurs in the composites.In the calibrated area,SiC phase experiences Ostwald ripening and volume change with location migration,while ZrC phase experiences a re-sintering process with diffusion.Moreover,it is found that increasing temperature has a more obvious effect on the thermal stability than extending holding time,which is mainly attributed to the faster diffusion rate of atoms.

Full Friendly Index Sets of a Family of Cubic Graphs

Let G=(V,E)be a graph.For a vertex labeling f:V→Z2,it induces an edge labeling f+:E→Z2,where for each edge v1 v2∈E we have f+(v1 v2)=f(v1)+f(v2).For each i∈Z2,we use vf(i)(respectively,ef(i))to denote the number of vertices(respectively,edges)with label i.A vertex labeling f of G is said to be friendly if vertices with different labels differ in size by at most one.The full friendly index set of a graph G,denoted by F F I(G),consists of all possible values of ef(1)-ef(0),where f ranges over all friendly labelings of G.In this paper,motivated by a problem raised by[6],we study the full friendly index sets of a family of cubic graphs.

EXPERIMENTAL INVESTIGATION OF THE FAILURE OF CASCADE LANDSLIDE DAMS

This paper presents results of model tests for the landslide dam failure of a single dam and cascade dams in a sloping channel. The dams were designed to be regular trapezoid with fine sand. A new measuring method named the labeled line locating method was used to digitalize the captured instantaneous pictures. Under two different inflow discharges, the morphological evolution and the flow patterns during one dam failure and the failure of cascade dams were investigated. The results indicate that when the inflow discharge is large, the deformation pattern of the downstream dam is similar to that of the upstream dam, and both dams are characterized with the overtopping scour throughout the dam failure process. When the inflow discharge is small, the upstream dam is scoured mainly through a sluice slot formed by the longitudinal incision, and the downstream dam is characterized with the overtopping scour. The data set presented in this paper can be used for the validation of numerical models and provide a reference for the flood risk management of cascade landslide dams.

Analysis of the Diagnostic Consistency of Chinese Medicine Specialists in Cardiovascular Disease Cases and Syndrome Identification Based on the Relevant Feature for Each Label Learning Method

Objective：To analyze the diagnostic consistency of Chinese medicine（CM） specialists in patients with cardiovascular disease and to study syndrome classification and identification based on the multi-label learning method.Methods：Using self-developed CM clinical scales to collect cases,inquiry information,complexity,tongue manifestation and pulse manifestation were assessed.The number of cases collected was 2,218.Firstly,each case was differentiated by two CM specialists according to the same diagnostic criteria.The consistency of the diagnosis based on Cohen’s Kappa coefficient was analyzed.Secondly,take the same diagnosis syndromes of two specialists as the results of the cases.According to injury information in the CM scale ＂yes＂ or ＂no＂ was assigned ＂1＂ or ＂0＂,and according to the syndrome type in each case ＂yes＂ or ＂no＂ was assigned ＂1＂ or ＂0＂.CM information data on cardiovascular disease cases were established.We studied CM syndrome classification and identification based on the relevant feature for each label（REAL） leaming method,and the diagnostic rate of the syndrome was studied using the REAL method when the number of features selected was 5,10,15,20,30,50,70,and 100,respectively.Results：The syndromes with good diagnostic consistency were Heart（Xin）-qi deficiency,Heart-yang deficiency,Heart-yin deficiency,phlegm,stagnation of blood and stagnation of qi.Syndromes with poor diagnostic consistency were heartblood deficiency and blood deficiency of Heart and Liver（Gan）.The highest diagnostic rates using the REAL method were Heart-yang deficiency followed by Heart-qi deficiency.A different number of features,such as 5,10,15,20,30,40,50,70,and 100,respectively,were selected and the diagnostic accuracy based on five features showed the highest diagnostic accuracy.The top five features which had a strong correlation with the syndromes were in accordance with the CM theory.Conclnsions：CM syndrome differentiation is strongly subjective and it is difficult to obtain good diagnostic consistency.The REAL method fully considers the relationship between syndrome types and injury symptoms,and is suitable for the establishment of models for CM syndrome classification and identification.This method can probably provide the prerequisite for objectivity and standardization of CM differentiation.