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Fabrication of UV-Curing Linalool-Polysiloxane Hybrid Films with High Refractive Index and Transparency
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作者 Wenqing Xiao Lewen Tan +2 位作者 Xunjun Chen Qiaoguang Li Yunqing Ruan 《Journal of Renewable Materials》 EI CAS 2024年第3期569-583,共15页
In this article,a series of high refractive indices(1.50-1.53)thiol phenyl polysiloxane(TPS)were synthesized via hydrolytic sol-gel reaction.The Fourier transform infrared spectra(FT-IR)and nuclear magnetic resonance ... In this article,a series of high refractive indices(1.50-1.53)thiol phenyl polysiloxane(TPS)were synthesized via hydrolytic sol-gel reaction.The Fourier transform infrared spectra(FT-IR)and nuclear magnetic resonance spectra(NMR)results showed that TPS conformed to the predicted structures.Natural terpene linalool was exploited as photocrosslinker to fabricate UV-curing linalool-polysiloxane hybrid films(LPH)with TPS via photoinitiated thiol-ene reaction.LPH rapidly cured under UV irradiation at the intensity of 80 mW/cm^(2) in 30 s,exhibiting good UV-curing properties.The optical transmittance of LPH in the wavelength of 300-800 nm was over 90%,exhibiting good optical transparency.The water contact angle and water vapor permeability results showed that the introduction of phenyl groups enhance the hydrophobicity and water vapor barrier properties of LPH.The results indicated the potential of LPHs in the applications of optical functional coatings. 展开更多
关键词 UV-CURING polysiloxane hybrid films high refractive index TRANSPARENCY
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Synthesis and Characterization of Side-Chain Liquid Crystalline Polysiloxanes 被引量:1
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作者 戴荣继 傅若农 《Journal of Beijing Institute of Technology》 EI CAS 1997年第1期43-51,共9页
Side chain liquid crystalline golysiloxanes conta ing biphenyl and benzyl ether mesogen were synthesized by the hydrosilation of poly(methylhydrcsiloxane) with 4-(4-allyloxybenzytoxy)-4'- methoxybiphenyl(M_1),4-(4... Side chain liquid crystalline golysiloxanes conta ing biphenyl and benzyl ether mesogen were synthesized by the hydrosilation of poly(methylhydrcsiloxane) with 4-(4-allyloxybenzytoxy)-4'- methoxybiphenyl(M_1),4-(4-allyloxybenzyloxy)-4'-ethoxybiphenyl(M_2),4-(4-allyloxybenzyloxy)-4'- propoxybiphenyl(M_3),4-(4-allyloxybenzyloxy)-4'-butoxybiphenyl(M_4),4-(4-allyloxybenzyloxy)-4'- pentyloxybiphenyl(M_5).The phase behavior of monomeric and polymeric liquid crystals was chararcterized by differential scanning calorimetry and optical polarization microscopy.Both the monomeric and polymeric liquid crystals exhibit liquid crystal behaviors. 展开更多
关键词 liquid crystal polysiloxane benzyl ether
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降解检材STR分型Ladder-Like条带形成原因的探讨 被引量:1
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作者 楼迪栋 余纯应 +3 位作者 黄代新 赵贵森 任文 杨庆恩 《中国法医学杂志》 CSCD 2005年第6期332-334,共3页
目的探讨降解DNA短串联重复序列PCR扩增产物在PAGE中Ladder-L ike条带的形成原因。方法用一组人工合成的不同长度的D8S1179DNA单链,模拟降解检材中的断裂DNA;利用John M设计的D8S1179引物对模拟模板的DNA单链进行PCR扩增,PAGE分离。结... 目的探讨降解DNA短串联重复序列PCR扩增产物在PAGE中Ladder-L ike条带的形成原因。方法用一组人工合成的不同长度的D8S1179DNA单链,模拟降解检材中的断裂DNA;利用John M设计的D8S1179引物对模拟模板的DNA单链进行PCR扩增,PAGE分离。结果不同模拟模板的DNA单链的组合可以扩增出不同的Lad-der-L ike条带。结论短串联重复序列Ladder-like条带是PCR过程中降解DNA多态区互补扩增的产物。 展开更多
关键词 法医物证学 短串联重复序 ladder-like条带 PCR—STR分型降解检材 降解检材
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Separation Properties of a New Polysiloxane-Anchored β-Cyclodextrin Derivative as Gas Chromatography Stationary Phase 被引量:1
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作者 史雪岩 傅若农 顾峻岭 《Journal of Beijing Institute of Technology》 EI CAS 2002年第3期285-289,共5页
A new capillary gas chromatography stationary phase, monokis (2,6 di O benzyl 3 O propyl (3’)) hexakis(2,6 di O benzyl 3 O methyl) β CD bonded polysiloxane, was synthesized. It ex... A new capillary gas chromatography stationary phase, monokis (2,6 di O benzyl 3 O propyl (3’)) hexakis(2,6 di O benzyl 3 O methyl) β CD bonded polysiloxane, was synthesized. It exhibited separation abilities to disubstituted benzene isomers and some chiral solutes. It was also found that the polarity of CD derivatives can be lowered both by chemically bonding it to polysiloxane and by diluting it in polysiloxane. The separation abilities of the polysiloxane anchored CDs (SP CD) are higher than that of the unbonded CDs (S CD) and the diluted S CD at lower column temperature. Hydrosilylation reaction is one of the best methods to lower the operating temperature of CDs. 展开更多
关键词 capillary gas chromatography stationary phase polysiloxane anchored β cyclodextrin derivative di substituted benzene isomers separation enantiomers separation
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INFLUENCE OF SILOXANE CO-SEGMENT LENGTH AND CONTENT OF WATERBORNE POLYSILOXANE-URETHANE COPOLYMERS ON THEIR WATER RESISTANCE,THERMAL STABILITY AND MECHANICAL PROPERTIES 被引量:7
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作者 郑强 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2010年第2期219-229,共11页
A series of stable waterborne polysiloxaneurethane (WPSUR) dispersions were prepared using amino-terminated polydimethylsiloxane (NS), dimethylolpropionic acid (DMPA), castor oil, polypropylene glycol and toluen... A series of stable waterborne polysiloxaneurethane (WPSUR) dispersions were prepared using amino-terminated polydimethylsiloxane (NS), dimethylolpropionic acid (DMPA), castor oil, polypropylene glycol and toluene diisocyanate. Meanwhile, NS with different molecular weights was synthesized and used as the soft co-segment. Effects of types and contents of soft co-segments as well as chain extenders on the thermal degradation and stability for WPSUR films were examined. Results reveal that WPSUR films exhibit excellent water resistance and mechanical properties as compared with pure polyurethane (PU) films, and the NS soft co-segment possesses a remarkable effect on the second stage (stage Ⅱ), while the content of the hard segment is propitious to the initial stage (stage Ⅰ). Moreover, the highest temperature of stage Ⅱ (T2m) for WPSUR films using NS as soft co-segment is 413℃, approximately being 30℃ higher than that of those typical PUs using HDA and APDMS as the chain extenders, respectively. 展开更多
关键词 WATERBORNE polysiloxane Polyurethane Castor oil Thermal properties Water resistance.
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Film Morphology,Emulsification of Dodecyl/Carboxyl Modified Polysiloxane and Its Application Performance on Cotton Fabrics 被引量:6
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作者 安秋凤 门靖 +3 位作者 王科峰 丁洋 亢玲娟 刘爽 《Journal of Donghua University(English Edition)》 EI CAS 2011年第4期375-378,共4页
The film morphology of dodecyl/carboxyl modified polysiloxane(RCAS) on cotton fabric or the silicon wafer was investigated and characterized by field emission scanning electron microscopy(FESEM),atomic force microscop... The film morphology of dodecyl/carboxyl modified polysiloxane(RCAS) on cotton fabric or the silicon wafer was investigated and characterized by field emission scanning electron microscopy(FESEM),atomic force microscope(AFM),and Fourier transform infrared spectrometer(FTIR).Experimental results indicate that RCAS is a good film forming material on different substrates.Relatively smooth film was formed on cotton fabric surface,on which the grooves disappeared.In addition,RCAS formed a micromorphology inhomogeneous and unsmooth film on the silicon wafer.Many high or low bright peaks distributed randomly on the film surface,especially as the field was 2μm×2 μm and the date scale was 5 nm in AFM observation.Then RCAS was emulsified with nonionic surfactant alkyl polyoxyethylene ether in order to achieve a transparent organosilicon emulsion-RCAS emulsion(RCSE),which possessed good stability.The properties of RCSE and its application performance on cotton fabrics were investigated and characterized by transmission electron microscope(TEM),particle size analysis,and voltage test instrument.The results show that the average particle size of RCAS emulsion is 28.32 nm,while the ζ voltage is-37.88 mV.Compared with untreatd cotton fabric,the softness of treated fabric can be improved with RCSE to a certain extent.At the same time,the fabric treated with RCSE acquires unique fluffy and soft handle. 展开更多
关键词 amino functional polysiloxane carboxyl containing polysiloxane film morphology polysiloxane emulsion cotton fabrics
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Synthesis of a New Polysiloxane Modified Polyurethane 被引量:4
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作者 Wei Feng JIANG Shi Gui ZHAO Yun Xia QI 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第5期581-583,共3页
In this paper, a new polymer of polysiloxane modified polyurethane was synthesized by using H-containing silicone oil, toluene diisocyanate(TDI), 1,4-butanediol and unsaturated polyether.
关键词 POLYURETHANE polysiloxane synthesis.
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Preparation of Nano-SiO_2/Amino-modified Polysiloxane Hybrid Superhydrophobic Coating and Thermal-stability Characterization 被引量:3
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作者 李金桦 翁睿 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2014年第1期35-39,共5页
We put forward a large-area and cost-effective method to fabricate superhydrophobic coating by introducing in-situ functionalized nano-SiO2 into side-amino modified hydroxy-terminated polydimethylsiloxane (SA-HTPDMS... We put forward a large-area and cost-effective method to fabricate superhydrophobic coating by introducing in-situ functionalized nano-SiO2 into side-amino modified hydroxy-terminated polydimethylsiloxane (SA-HTPDMS) curing system. With the characterization using water contact angle (WCA) tester, Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), atomic force microscopy (AFM) and simultaneous thermal analysis, the as-prepared coating displayed a tremendous WCA of 154.8±1°, sliding angle (SA) about 3.5° and stable self-cleaning property range from -10 to 80 ℃. It was also found that the synergistic effect of surface micro-nano hierarchical structure and chemical hydrophobicity, stability from matrix had made contributions to the superhydrophobicity and excellent heat resistance up to 300 ℃. 展开更多
关键词 NANO-SIO2 amino-modified polysiloxane THERMAL-STABILITY SUPERHYDROPHOBIC
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The Thermal Decomposition Kinetics of Polysiloxane /Polymethylacrylate IPNs Materials 被引量:2
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作者 黄志雄 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2006年第2期47-49,共3页
Polydimethylsiloxane/ polymethylacrylate ( PDMS/ PMA ) interpenetratrating polymer networks (IPNs) was fabricated by simultaneous synthesis and characterized by thermogravimetry ( TG ). The kinetics of the therm... Polydimethylsiloxane/ polymethylacrylate ( PDMS/ PMA ) interpenetratrating polymer networks (IPNs) was fabricated by simultaneous synthesis and characterized by thermogravimetry ( TG ). The kinetics of the thermal decomposition of polysiloxane/ polymethylacrylate IPNs in N2 and air was studied at different heating rates. It was observed that there were two decomposition peaks both in N2 and air, which showed that thermal decomposition process obeyed two-step pyrolysis mechanism and accorded with the two compositions of IPN. Kinetic parameters were determined during simultaneous integration of the Doyle equation and the IPN/ s kinetics equation was one-order equation in N2 and Air. The decomposition activation energy in N2 and air were 147. 405 kJ· monl^-1 and 192.656 kJ·monl^-1 respectively. 展开更多
关键词 polysiloxane polymethylacrylate IPNS thermogravimetery KINETICS
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NOVEL SULPHONATED POLYSILOXANE POLYUREA-URETHANE IONOMERS 被引量:2
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作者 陈雷 余学海 杨昌正 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 1996年第4期295-303,共9页
A series of novel polysiloxane polyurea-urethane blockcopolymers based on methylene bis(p-phenylisocyanate (MDI), sodium-s-1,2-dihydroxy propyl sulphonate (SDPS) and aminopropyl-terminated polydimethylsiloxane (ATPS) ... A series of novel polysiloxane polyurea-urethane blockcopolymers based on methylene bis(p-phenylisocyanate (MDI), sodium-s-1,2-dihydroxy propyl sulphonate (SDPS) and aminopropyl-terminated polydimethylsiloxane (ATPS) was synthesized with varying length of soft segments and neutralizing cation. The effect of the chemical composition and the cation on the morphology and mechanical properties of the samples were studied. It was found that the SDPS chain extender based samples have definite chemical structure (-MDI-SDPS-MDI-ATPS-). As the length of the soft segment increases, an improvement of phase separation was observed. In addition, when SO3Na was translated into SO3H or the sulphonic acid groups were neutralized with different charge cations (Na+, Zn2+ and Al3+), the morphology and mechanical properties changed greatly. 展开更多
关键词 polysiloxane POLYUREA POLYURETHANE IONOMERS
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A novel ionic liquids grafted polysiloxane for capillary gas chromatography 被引量:2
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作者 Qing Quan Wei Mei Ling Qi Ruo Nong Fu 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第9期1111-1114,共4页
A new ionic liquids grafted polysiloxane used as stationary phase for capillary gas chromatography (CGC) is described. The stationary phase of 1-vinyl-3-hexylimidazolium hexafluorophosphate anchored to polysiloxane ... A new ionic liquids grafted polysiloxane used as stationary phase for capillary gas chromatography (CGC) is described. The stationary phase of 1-vinyl-3-hexylimidazolium hexafluorophosphate anchored to polysiloxane (PMHS-[VHIm][PF6]) was synthe- sized, characterized and coated onto capillary columns by static coating. The results show that the present stationary phase exhibits a very good chromatographic resolution and selectivity for Grob test mixture and alcohols with baseline resolution and symmetry peaks. The present work suggests that novel stationary phase has a great potential for further development and application. 2009 Mei Ling Qi. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved. 展开更多
关键词 Ionic liquids polysiloxane Stationary phase Gas chromatography
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Synthesis and Characterization of Sidechain Liquid Cryastalline Polysiloxanes Containting Either Cholesteryl or Cyanobiphenyl Mesogenic Groups 被引量:2
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作者 Xu Guangwei Huang Ronghua Zhang Xianliang 《Wuhan University Journal of Natural Sciences》 CAS 1997年第1期77-83,共7页
A series of side chain liquid crystalline polysiloxanes containing either cholesteryl or cyanobiphenyl mesogenic groups were synthesized by the hydrosilylation reaction of a polysiloxane containing Si H group with a v... A series of side chain liquid crystalline polysiloxanes containing either cholesteryl or cyanobiphenyl mesogenic groups were synthesized by the hydrosilylation reaction of a polysiloxane containing Si H group with a vinyl terminated compound containing the mesogenic group. Their chemical structures were confirmed by IR, 1H NMR, and elemental analysis, Their phase behaviors were investigated by differential scanning calorimetry, optical polarizing microscope, and X ray diffraction techniques. The results show that all these polysiloxanes except PⅤ display smectic or nematic mesonorphism or both. The dependence of phase transition temperature on the rigidity of mesogenic unit. the length of spacer group, and the flexibility of Si(CH 3) 2O chain is also described. 展开更多
关键词 polysiloxane liquid crystal phase behavior mesogenic groups
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SIDE CHAIN LIQUID CRYSTALLINE POLYSILOXANES CONTAINING CROWN ETHER AND BENZYL ETHER MOIETIES 被引量:2
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作者 戴荣继 傅若农 佟斌 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 1998年第1期18-24,共7页
Two kinds of side chain liquid crystalline polysiloxanes containing crown ether and benzyl ether were synthesized and characterized by optical polarization microscopy. Both the monomeric liquid crystals and polymeric ... Two kinds of side chain liquid crystalline polysiloxanes containing crown ether and benzyl ether were synthesized and characterized by optical polarization microscopy. Both the monomeric liquid crystals and polymeric liquid crystals show smectic phases. 展开更多
关键词 liquid crystalline polysiloxane side chain crown ether benzyl ether mesogens
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MODIFICATION OF EPOXY RESINS WITH PHENOLIC HYDROXYL-TERMINATED POLYSILOXANE 被引量:1
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作者 侯庆普 黄英 余云照 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 1995年第3期235-243,共9页
Phenolic hydroxyl-terminated polysiloxanes were incorporated into epoxy resins to reduce the internal stress owing to the mismatch in coefficient of thermal expansion (CTE). Polysiloxane-epoxy resin block copolymers w... Phenolic hydroxyl-terminated polysiloxanes were incorporated into epoxy resins to reduce the internal stress owing to the mismatch in coefficient of thermal expansion (CTE). Polysiloxane-epoxy resin block copolymers were made by a pre-reaction step prior to the curing. In the cured resin, the domain size of the polysiloxane phase depended on the structure of the phenolic hydroxyl-terminated polysiloxane. It was found that the modulus of the cured resin depended largely on the level of the modifier, while the CTE was affected greatly by the structure of the polysiloxane. By means of incorporating a few percent of methylphenylsiloxane unit into the polydimethylsiloxane chain, or by introducing; more compatible end-capping groups, the compounds of more effective low stress modifiers were synthesized. 展开更多
关键词 EPOXY RESIN polysiloxane INTERNAL STRESS
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Syntheses and Characterization of New Chiral Side-Chain Liquid Crystalline Polysiloxanes 被引量:1
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作者 Tang Hongding Xu Guangwei Zhang Xianliang 《Wuhan University Journal of Natural Sciences》 EI CAS 1998年第2期253-254,共2页
A new serial chiral side-chain liquid crystal polysiloxanes containing L-Tyr structures were synthesized at room temperature. Both of them exhibited Sc phase at room temperature.
关键词 polysiloxaneS liquid crystal L-TYROSINE
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Template Polymerization Based on Stober Method:an Improved Method for Fabrication of Hollow Polysiloxane Spheres 被引量:1
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作者 Hui Gang WANG Ping CHEN Xiao Ming ZHENG 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第5期637-640,共4页
A modified Stober method has been developed which permits the controlled growth of spherical hollow spheres with diameters between 197 and 208 nanometers by consecutively cocondensed methyltrimethoxysilane and dimethy... A modified Stober method has been developed which permits the controlled growth of spherical hollow spheres with diameters between 197 and 208 nanometers by consecutively cocondensed methyltrimethoxysilane and dimethyldimethoxysilane monomers onto microemulsion of polydimethylsiloxane and subsequently removing the templated polydimethylsiloxane by exposure to solvents. Ammonia was used as a morphological catalyst. The morphology of the polymer spheres was demonstrated by transmission electron micrographs (TEM) and atomic force microscopy (AFM). 展开更多
关键词 Stober method hollow polysiloxane spheres template polymerization.
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Polysiloxane with Pendant Benzo Crown Ether via a Spacer of Undecyloxymethyl as Stationary Phase for Capillary Chromatography 被引量:1
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作者 LU Xue-ran ZHANG Li-feng +2 位作者 ZHOU Xi-chun WU Cai-ying and CHEN Yuan-yin(Department of Chemistry, Wuhan University, Wuhan, 430072) 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1994年第2期163-166,共4页
PolysiloxanewithPendantBenzoCrownEtherviaaSpacerofUndecyloxymethylasStationaryPhaseforCapillaryChromatograph... PolysiloxanewithPendantBenzoCrownEtherviaaSpacerofUndecyloxymethylasStationaryPhaseforCapillaryChromatographyLUXue-ran;ZHANGL... 展开更多
关键词 polysiloxane Undecyloxy methyl spacer Crown ether
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Silica-supported Polysiloxanes with Dithiacrown Ether Groups and Their Platinum Complexes 被引量:1
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作者 CHEN Yuan-yin, LU Xue-ran and SONG Xiao-ping(Department of Chemistry, Wuhan University, Wuhan, 430072) 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1992年第4期439-444,共6页
The present paper represents the syntheses of polypropyloxymethyldithia 15-crown-5 and 18-crown-6 supported on silica and their platinum complexes. The platinum complexes are effective catalysts for the hydrosilylatio... The present paper represents the syntheses of polypropyloxymethyldithia 15-crown-5 and 18-crown-6 supported on silica and their platinum complexes. The platinum complexes are effective catalysts for the hydrosilylation of olefins with triethoxysilane. The influences of temperature, amount of platinum complexes used and the nature of olefins used on the catalytic activity of the complexes are also investigated in this paper. 展开更多
关键词 Functionalized polysiloxane Thiacrown ether Platinum complex Hydrosilyla-tion catalyst
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SYNTHESIS AND CHARACTERIZATION OF A NOVEL REACTIVE LADDER-LIKE POLYSILSESQUIOXANE WITH LATERAL BROMOPHENYL GROUPS 被引量:1
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作者 张榕本 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2004年第5期445-451,共7页
A novel soluble, reactive ladder-like polysilsesquioxane (L) with lateral bromophenyl groups was synthesized successfully by stepwise coupling polymerization (SCP) method including preaminolysis, hydrolysis and polyco... A novel soluble, reactive ladder-like polysilsesquioxane (L) with lateral bromophenyl groups was synthesized successfully by stepwise coupling polymerization (SCP) method including preaminolysis, hydrolysis and polycondensation steps. The monomer 3-trichlorosilylpropoxy-4-bromobenzene (M) was first prepared via hydrosilylation reaction catalyzed by dicyclopentadienylplatinum dichloride (Cp2PtCl2). The title polymer (L) was characterized by 1H-NMR, 29Si-NMR, FTIR, X-ray diffraction (XRD), DSC and vapor pressure osmometry (VPO). The experimental results indicate that the polymer (L) possesses a typical ladder-like structure. 展开更多
关键词 ladder-like POLYSILSESQUIOXANE Stepwise coupling polymerization HYDROSILYLATION
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Superhydrophobic and mechanically robust polysiloxane composite coatings containing modified silica nanoparticles and PS-grafted halloysite nanotubes 被引量:1
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作者 Jie Wang Ling Zhang Chunzhong Li 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2022年第12期56-65,共10页
Excellent mechanical properties are the prerequisite for the application of superhydrophobic polymer coatings.However,significantly improving the mechanical properties without affecting other properties such as hydrop... Excellent mechanical properties are the prerequisite for the application of superhydrophobic polymer coatings.However,significantly improving the mechanical properties without affecting other properties such as hydrophobicity is a huge challenge.In this study,a superhydrophobic coating with excellent mechanical properties was prepared by spraying a mixture of polysiloxane resins based on three siloxane monomers,hexadecyltrimethoxysilane(HDTMS) modified nano-SiO_(2)particles(SiO_(2)-HDTMS) and polystyrene-grafted halloysite nanotubes(HNTs-PS).SiO_(2)-HDTMS dispersed homogeneously in polysiloxane coatings and the water contact angle of corresponding coating exceeding 150°,achieving superhydrophobicity.The SiO_(2)-HDTMS/HNTs-PS/polysiloxane composite coatings showed excellent abrasion resistance with the water coating contact angle remaining above 150°after 90 abrasion cycles,indicating that HNTs-PS can significantly improve the mechanical properties of the coating without affecting the hydrophobic properties of the coating.The achieved coating also exhibited excellent antifouling and acid and alkali corrosion resistance.This work provides a convenient and ecologically friendly method to prepare superhydrophobic polysiloxane composite coating with excellent mechanical properties,which is promising in the application of anti-fouling,anti-corrosion,and oil-water separation etc. 展开更多
关键词 polysiloxane Superhydrophobic coating Mechanical properties
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