In-situ Characterization of Non-aqueous Nano-dispersion Systems by Freeze-etching TEM and Comparative Study with Laser Scattering Method

In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium.

Analysis of random laser scattering pulse signals with lognormal distribution

The statistical distribution of natural phenomena is of great significance in studying the laws of nature. In order to study the statistical characteristics of a random pulse signal, a random process model is proposed theoretically for better studying of the random law of measured results. Moreover, a simple random pulse signal generation and testing system is designed for studying the counting distributions of three typical objects including particles suspended in the air, standard particles, and background noise. Both normal and lognormal distribution fittings are used for analyzing the experimental results and testified by chi-square distribution fit test and correlation coefficient for comparison. In addition, the statistical laws of three typical objects and the relations between them are discussed in detail. The relation is also the non-integral dimension fractal relation of statistical distributions of different random laser scattering pulse signal groups.

Characterization of a microsecond pulsed non-equilibrium atmospheric pressure Ar plasma using laser scattering and optical emission spectroscopy

A non-equilibrium atmospheric pressure argon(Ar)plasma excited by microsecond pulse is studied experimentally by laser scattering and optical emission spectroscopy(OES),and theoretically by collisional-radiative(CR)model.More specifically,the electron temperature and electron density of plasma are obtained directly by the laser Thomson scattering,the gas temperature is measured by laser Raman scattering,the optical emissions of excited Ar states of plasma are measured by OES.The laser scattering results show that the electron temperature is about 1 eV which is similar to that excited by 60 Hz AC power,but the gas temperature is as low as 300 K compared to about 700 K excited by 60 Hz AC power.It is shown that the microsecond pulsed power supply,rather than nanosecond ones,is short enough to reduce the gas temperature of atmospheric pressure plasma to near room temperature.The electron temperature and electron density are also obtained by CR model based on OES,and find that the intensities of the optical emission intensity lines of 727.41,811.73,841.08,842.83,852.44 and 912.86 nm of Ar can be used to characterize the behavior of electron density and electron temperature,it is very useful to quickly estimate the activity of the atmospheric pressure Ar plasma in many applications.

Planar laser scattering visualization of streamwise vortex pairs in a Mach 6 flow

A series of cross-sectional flow fields of Counterrotating Vortex Pairs(CVPs) generated by a large-scale ramp vortex generator is observed using an ice-cluster-based Planar Laser Scattering(PLS) method in a shock tunnel with a nominal flow Mach number of 6. Combined with a numerical simulation, two streamwise CVPs with opposite rotating directions are identified in the wake flow of the vortex generator with an absence of a boundary layer, namely, a Primary CVP(PCVP) and a Secondary CVP(SCVP). The wake flow is divided into two stages with different features of the PCVP and SCVP. In Stage Ⅰ, the PCVP and SCVP gradually mature, and the flow is relatively stable. In Stage Ⅱ, the PCVP and SCVP depart from each other, and the flow becomes unstable. The profiles of the transverse velocity in the spanwise symmetry plane induced by the PCVP and SCVP do not obey the scaling law of CVPs immersed in the boundary layer. A new scaling law is proposed, in which the transverse distances between adjacent saddle points in the cross-sectional flow field are used as the characteristic lengths for the PCVP and SCVP. After this new scaling procedure, the profiles of transverse velocity induced by the PCVP and SCVP at different streamwise locations collapse well. Moreover, the PLS images show that the mixing between the CVPs and the outside high-momentum flow becomes evident at approximately 5.5 times the height of the vortex generator, which is earlier than that immersed in the boundary layer. These findings enrich the knowledge of CVPs in the hypersonic regime, especially in the absence of the boundary layer.

Measurement of electron density and electron temperature of a cascaded arc plasma using laser Thomson scattering compared to an optical emission spectroscopic approach

As advanced linear plasma sources, cascaded arc plasma devices have been used to generate steady plasma with high electron density, high particle flux and low electron temperature. To measure electron density and electron temperature of the plasma device accurately, a laser Thomson scattering（LTS） system, which is generally recognized as the most precise plasma diagnostic method, has been established in our lab in Dalian University of Technology. The electron density has been measured successfully in the region of 4.5？×10^19m^-3 to7.1？×10^20m^-3 and electron temperature in the region of 0.18 eV to 0.58 eV. For comparison,an optical emission spectroscopy（OES） system was established as well. The results showed that the electron excitation temperature（configuration temperature） measured by OES is significantly higher than the electron temperature（kinetic electron temperature） measured by LTS by up to 40% in the given discharge conditions. The results indicate that the cascaded arc plasma is recombining plasma and it is not in local thermodynamic equilibrium（LTE）. This leads to significant error using OES when characterizing the electron temperature in a non-LTE plasma.

High energy and high brightness laser compton backscattering gamma-ray source at IHEP

Based on the LINAC of BEPCII, a high-polarized, high bightness, energy-tunable, monoenergetic laser compton backscattering (LCS)gamma-ray source is under construction at IHEP. The gamma-ray energy range is from 1 MeV to 111 MeV. It is a powerful and hopeful researchplatform to reveal the underlying physics of the nuclear, the basic particles and the vacuum or to check the exist basic physical models, quantumelectrodynamic (QED) theories. In the platform, a 1.064 mm Nd:YAG laser system and a 10.6 mm CO_(2) laser system are employed. All the triggersignals to the laser system and the electron control system are from the only reference clock at the very beginning of the LINAC to make sure thetemporal synchronization. Two optical transition radiation (OTR) targets and two charged-couple devices (CCD) are used to monitor and to alignthe electron beam and the laser beam. With the LCS gamma-ray source, it is proposed to experimentally check the gamma-ray calibrations, thephoton-nuclear physics, nuclear astrophysics and some basic QED phenomena.

HT-7 Multipoint Nd Laser Thomson Scattering Apparatus

A compact, low cost, multipoint Thomson scattering diagnostic system for HT-7 superconducting tokamak has been in operation since 1999. Its capability of measuring electron temperatures is in the range of 200 eV to 2 keV at a density of a few times IO12 cm-3, with a spatial resolution of 2.4 cm for 5 spatial points and a temporal resolution of 1 ms-1 s for 8 time points. The main components of the diagnostic system include a 20-25 J Nd: glass laser with 35 ns pulse width (8 pulses per burst), a KDP frequency-doubling unit, spherical mirrors of multipass input optical system, a wide-angle collection objective, a bandpass glass filter for reducing the stray light to zero a f/2.5 polychromator, a fiberglass collimator, a photomultiplier's box with electronic preamplifier, high gain and high signal/noise ratio, CAMAC data acquisition and so on. The multipass optical system has been successful at increasing the quantity of scattered photons by passing the probing laser beam 10 times through the plasma under investigation. The HT7 Thomson scattering diagnostic has provided successfully the information on two-dimensional electron temperature in the plasma of HT-7 tokamak with LHCD and IBW.

Relation between Debye series and generalized Lorentz-Mie theory of laser beam scattering by multilayer cylinder

With the recursive relations of Bessel function and applying inductive approach, the consistency between the scattering coefficient formula of Debye series and that of the generalized Lorentz-Mie theory （GLMT） in the scattering of a multilayer cylinder illuminated by a laser beam is proved in detail. As an application example, rainbow phenomenon in the scattering of a two-layer cylinder is discussed by the Debye series components. It can be concluded that the radius and the refractive index of a two-layer cylinder have an effect on the twin-primary rainbow, and the high-order Debye series components which are associated with the high-order rainbows are more complex than those of a homogeneous cylinder.

Multipulse Nd:YAG Laser Thomson Scattering Diagnostics on HT-7 Tokamak

A multipulse Nd：YAG （Neodym-yttrium aluminium garnet） laser Thomson scattering diagnostic system developed was recently applied on HT-7 tokamak to obtain more accurate electron temperatures. A CAMAC-based real-time computer system for laser control, data acquisition, analysis and calibration was investigated in detail. Furthermore, the reliability and accuracy of this diagnostic system were demonstrated by comparing the results with those of a soft-X ray diagnostic system.

The Stimulated Brillouin Scattering of a Strong Laser in Partially Stripped Plasmas

The effects of the nonlinear polarization in a partially stripped plasma on stimulated Brillouin scattering (SBS) process of a strong laser are discussed. A set of nonlineax mode coupling equations and the linear growth rate of SBS instability is derived, respectively. When the intensity of an incident laser Io > 10^(17) W/cm^2, the third order susceptibility X(3) will reduce the above mentioned linear growth rate enormously. If taking the maximum value of the second order susceptibility X(2), the growth rate may be decreased observably when Io > 10_^(14)W/cm2. Furthermore, the nonlinear susceptibility can affect the nonlinear evolution of SBS much extensively.

Commissioning of laser electron gamma beamline SLEGS at SSRF

The Shanghai Laser Electron Gamma Source(SLEGS)is a powerful gamma source that provides MeV gamma-ray beams for nuclear science and technology.It was developed as one of the 16 beamline stations in the Phase Ⅱ Project of the Shanghai Synchrotron Radiation Facility.The slant-scattering mode is for the first time systematically employed in laser Compton scattering at SLEGS to produce energy-tunable quasi-monoenergetic gamma-ray beams.The SLEGS officially completed its commissioning from July to December 2021.Gamma rays in the energy range of 0.25-21.7 MeV with a flux of 2.1×10^(4)-1.2×10^(7) photons/s and an energy spread of 2-15% were produced during the test.This paper reports the results from commissioning the SLEGS beamline.

LIGHT-SCATTERING STUDY OF POLYELECTROLYTE HOLLOW CAPSULES

Silver halide (AgX) microcrystal was used as template to synthesize hollow polyelectrolyte capsules. These hollow capsules were characterized by laser light scattering (LLS) used to measure the size of the capsules in solution. The ratio of hydrodynamic radius (R h ) from dynamic LLS to the radius of gyration (Rg) from static LLS is almost unity, revealing that the entities are hollow in solution. The results suggest that the LLS method can be regarded as a good complement to the confocal laser scanning microscopy (CLSM) method for the characterization of small hollow capsules, and it possesses the advantage of not needing fluorescence labeling.

Data Processing and Acquisition System for the HT-7 Multipulse Thomson Scattering Diagnostic

This article describes the data processing and acquisition system for the HT-7 mul-tipulse Thomson scattering diagnostic. An eight-pulse laser is used in the Thomson scattering system to obtain electron temperature profiles at eight different times throughout an entire plasma discharge. The major components of the diagnostic system consist of a multipulse Nd-glass laser, a photodetector's subsystem, a calibration set and a CAMAC data processing and acquisition system. The data processing software along with LeCroy 2250L will perform the data acquisition. In order to simplify the operation and extend the capability of its compatibility with other math softwares, the processing software has been improved by the authors. The new software based on the VC++ easily utilizes some math softwares to calculate the electron temperature. The new software is simpler and more operational than the old one.

Present Status of the Nd:YAG Thomson Scattering System Development for Time Evolution Measurement of Plasma Profile on Heliotron J

A new high repetition rate Nd：YAG Thomson scattering system is developed for the Heliotron J helical device. A main purpose of installing the new system is the temporal evolution measurement of a plasma profile for improved confinement physics such as the edge transport barrier （H-mode） or the internal transport barrier of the helical plasma. The system has 25 spatial points with -10 mm resolution. Two high repetition Nd：YAG lasers （〉 550 m J@ 50 Hz） realize the measurement of the time evolution of the plasma profile with ~10 ms time intervals. Scattered light is collected by a large concave mirror （D----800 mm, f/2.25） with a solid angle of -100 mstr and transferred to interference filter polychromators by optical fiber bundles in a staircase form. The signal is amplified by newly designed fast preamplifiers with DC and AC output, which reduces the low frequency background noise. The signals are digitized with a multi-event QDC, fast gated integrators. The data acquisition is performed by a VME-based system operated by the CINOS.

Doppler shift of a laser pulse beam scattered by a rotating cone and cylinder

Based on laser radar equations, a Doppler shift model of a laser pulse beam scattered by a rotating arbitrary convex target is reported in this paper. The boundary relations between an incident pulse beam and the detected area elements are analyzed by geometric methods. The Doppler shift characteristics of the rotating cone and cylinder are discussed and the difference between the laser pulse beam and the plane wave scattered from the same rotating target is compared accordingly. Numerical simulations show that the Doppler shift is tightly relevant to their dimensions, speeds, and so on. In the same incidence conditions, the pulse beam and plane wave have difference peak values and the same Doppler shift bandwidth. If the waist radius of the pulse beam is larger, the peak value is higher, and the Doppler shifts are proportional to the speed of the rotating target. By virtue of our theoretical model, we probe into the scattered characteristics of the Doppler shifts of a laser pulse beam, which would benefit target identification in national defense.

Methods for Detection of Subsurface Damage:A Review

Subsurface damage is easily induced in machining of hard and brittle materials because of their particular mechani?cal and physical properties. It is detrimental to the strength,performance and lifetime of a machined part. To manu?facture a high quality part,it is necessary to detect and remove the machining induced subsurface damage by the subsequent processes. However,subsurface damage is often covered with a smearing layer generated in a machining process,it is rather di cult to directly observe and detect by optical microscopy. An e cient detection of subsur?face damage directly leads to quality improvement and time saving for machining of hard and brittle materials. This paper presents a review of the methods for detection of subsurface damage,both destructive and non?destructive. Although more reliable,destructive methods are typically time?consuming and confined to local damage infor?mation. Non?destructive methods usually su er from uncertainty factors,but may provide global information on subsurface damage distribution. These methods are promising because they can provide a capacity of rapid scan and detection of subsurface damage in spatial distribution.

Supersonic boundary layer transition induced by self-sustaining dual jets

To promote high-speed boundary layer transition,this paper proposes an active self-sustaining dual jets(SDJ)actuator utilizing the energy of supersonic mainflow.Employing the nanoparticle-based planar laser scattering(NPLS),supersonic flat-plate boundary layer transition induced by SDJ is experimentally investigated in an Ma-2.95 low-turbulence wind tunnel.Streamwise and spanwise NPLS images are obtained to analyze fine flow structures of the whole transition process.The results reveal the transition control mechanisms that on the one hand,the jet-induced shear layer produces unstable Kelvin–Helmholtz instabilities in the wake flow,on the other hand,the jets also generates an adverse pressure gradient in the boundary layer and induce unstable streak structures,which gradually break down into turbulence downstream.The paper provides a new method for transition control of high-speed boundary layer,and have prospect both in theory and engineering application.

On variation of surface topography and robust product performance

The customer's demands for higher quality,faster delivery times and reduction of cost,give evidence for the need to develop new technologies or enhance existing technologies combined with research activities.The automotive industry's capability to develop new products in a shorter time is constantly improved.Tool and die creation is a major part of the product creation for many industrial products and in particular for the automotive industry.The higher product requirements on reduced weight,better safety,and lower emissions have meant that a larger number of automotive body parts must be made in advanced high strength steels.Improved functionality of surface textures and engineered tailor made component surfaces is one enabling technology for industry to increase compete ability by improved component function and reduced friction losses.However,material properties'variation,un-evenly spread wear,unknown manufacturing process variations,the“human factor”,faulty metrology procedures…All factors interact to increase the problems of utilizing surface texturing on the micro metre level as a competitive tool for industry.Large variation of the micro topography created by industrial machining processes tends to reduce the impact of the usage of improved engineered surfaces on critical components.A proposal of a strategy for metrology using"intelligent"sampling techniques comprising of regionalization of the functional area and designed sampling patterns is presented.To efficiently make use of efficient sampling,an example of a recently developed optical scattering light in-line metrology of high precision surfaces is discussed as a tool to enable efficient control of machine tools in general.Future steps discussed include developing of control loops for implementation in CNC controllers to efficiently make use of the"smart"surface texture characterisation data from the developed in-line surface texture sensors.

Speckle intensity images of target based on Monte Carlo method

Speckle intensity in the detector plane is deduced in the free-space optical system and imaging system based on Van Cittert-Zemike theorem. The speckle intensity images of plane target and conical target are obtained by using the Monte Carlo method and measured experimentally. The results show that when the range extent of target is smaller, the speckle size along the same direction become longer, and the speckle size increase with increasing incident light wavelengths. The speckle size increases and the speckle intensity images of target is closer to the actual object when the aperture scale augments. These findings are useful to access the target information by speckle in laser radar systems.

Study on Molecular Chain Morphology of Konjac Glucomannan

The long-range structure of konjac glucomannan(KGM)is studied by using laser light scatter(LLS), gel permeation chromatography(GPC)and method of viscosidity. The weight-average molecular weight(Mw), root-mean-square ratio of gyration[(S2)1/2], second viral coefficient(A2)and multi-dispersion coefficient(Mw/Mn)are 1.04×106, 105. 0±0. 9 nm,(-1. 59±0.28)×10-3 mol ml g-2 and 1.015±0.003, respectively. Mark-Houwink equation is established as [η] = 5. 96×10-2Mw0.73 and the molecular chain parameters are as follows: ML=982. 82 nm-1, Lp = 27. 93 nm, d = 0. 74 nm, h = 0. 26 nm, L = l 054.11 nm. Further more molecular chain morphology of KGM is studied by using atom force microscope(AFM)and transmission electronic microscope(TEM), and the result shows that the KGM molecular is an extending semi-flexible linear chain without branch. Therefore, the image of molecular chain morphology confirms the deduction drawn by Mark-Houwink equation and molecular chain parameters.