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Microstructure and properties of Nb,V and N alloyed low magnetic hot rolled stainless steel plate
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作者 Jing-Bo Dong Kun Li +1 位作者 Li-Xiang Gao Chang-Sheng Li 《Tungsten》 EI CSCD 2023年第4期512-521,共10页
It is a common technical difficulty to improve the strength of low magnetic stainless steel plates on the premise of ensuring ductility,corrosion resistance,and low magnetism.In this paper,the chemical composition of ... It is a common technical difficulty to improve the strength of low magnetic stainless steel plates on the premise of ensuring ductility,corrosion resistance,and low magnetism.In this paper,the chemical composition of low magnetic stainless steels with excellent paramagnetic stabilities and corrosion resistances was formulated through composition design and calculation.Through the alloying of Nb,V,and N and the controlled hot rolling process,large numbers of uniformly distributed high-temperature second phase particles were formed in the steel plate,and low magnetic stainless steel 35 mm plate with yield strength,ultimate tensile strength and elongation of 407 MPa,739 MPa and 54%respectively were obtained.The main strengthening strategies of the steel were solid solution strengthening and precipitation strengthening.The precipitation law and types of the high-temperature second phase in the steel were explored.The micro structure of the steel plate was characterized by scanning electron microscope,electron probe microanalysis,and transmission electron microscope.The magnetic properties of the steel plate were tested by a vibrating sample magnetometer.The relative magnetic permeability of the hot rolled plate was 1.0063 which met the requirement of low magnetism. 展开更多
关键词 low magnetic stainless steel Steel plate Solution strengthening Second phase Precipitation strengthening
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Experimental investigation of backward wave oscillator with low magnetic field 被引量:4
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作者 马乔生 吴勇 +3 位作者 范植开 甘延青 金晓 周传明 《Chinese Physics C》 SCIE CAS CSCD 北大核心 2008年第3期222-226,共5页
A backward wave oscillator (BWO) is introduced in the paper. On the accelerator of Sinus-700, it is experimentally investigated. Under the condition that the electron energy is 740 keV, the beam current is 7 kA and ... A backward wave oscillator (BWO) is introduced in the paper. On the accelerator of Sinus-700, it is experimentally investigated. Under the condition that the electron energy is 740 keV, the beam current is 7 kA and the guiding magnetic field is at 0.68 T, the performance of 1.15 GW microwave output power at 9.1 GHz microwave frequency with 22 ns pulse width and 22% conversion efficiency are reached. 展开更多
关键词 high power microwave BWO low magnetic field ACCELERATOR
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Low frequency acoustic properties of bilayer membrane acoustic metamaterial with magnetic oscillator 被引量:2
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作者 Nansha Gao Hong Hou Yihao Mu 《Theoretical & Applied Mechanics Letters》 CAS CSCD 2017年第4期252-257,共6页
A bilayer membrane acoustic metamaterial was proposed to overcome the influence of the mass law on traditional acoustic materials and obtain a lightweight thin-layer structure that can effectively isolate low frequenc... A bilayer membrane acoustic metamaterial was proposed to overcome the influence of the mass law on traditional acoustic materials and obtain a lightweight thin-layer structure that can effectively isolate low frequency noise. The finite element analysis(FEA) results agree well with the experimental results.It is proved that the sound transmission losses(STLs) of the proposed structures are higher than those of same surface density acoustic materials. The introduction of the magnetic mass block is different from the traditional design method, in which only a passive mass block is fixed on the membrane. The magnetic force will cause tension in the membrane, increase membrane prestress, and improve overall structural stiffness. The effects of the geometry size on the STLs are discussed in detail. The kind of method presented in this paper can provide a new means for engineering noise control. 展开更多
关键词 Bilayer membrane acoustic metamaterial low frequency sound insulation Sound transmission loss Magnet oscillator
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Modulation of absorption manner in helicon discharges by changing profile of low axial magnetic field
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作者 赵高 王宇 +3 位作者 牛晨 刘忠伟 欧阳吉庭 陈强 《Chinese Physics B》 SCIE EI CAS CSCD 2017年第10期302-309,共8页
The modulation of absorption manner in helicon discharge by changing the profile of low axial magnetic field is explored experimentally in this work. The experiments are carried out in Boswell-type antenna driven by 1... The modulation of absorption manner in helicon discharge by changing the profile of low axial magnetic field is explored experimentally in this work. The experiments are carried out in Boswell-type antenna driven by 13.56-MHz power source in 0.35-Pa argon environment. The peak of the external non-uniform magnetic field (Bex) along the axis is observed in a range from 0 Gs to 250 Gs (1 Gs=10^-4 T), where the electron density varies from 0.5×10^16 m^-3 to 9×10^16 m^-3. When Bex is located near the tube upper end sealed by a dielectric plate, or near the tube bottom end connected with a diffusion chamber, the plasmas are centralized in the tube in the former case while the strong luminance appears between the edge of the tube and the axial line in the latter case. When Bex is located in the middle of the antenna, moreover, an effective resistance (Reff) peak appears apparently with increasing magnetic field. The glow moves toward first the edge of the tube and then the two antenna legs as the magnetic field increases. The discharge in this case is caused by the absorption of Trivelpiece-Gould (TG) wave. It is suggested that Bex is located in the middle of the antenna to obtain a higher efficiency of power transfer. 展开更多
关键词 helicon discharge absorption manner low supply power low axial magnetic field
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EXTREMELY LOW FREQUENCY MAGNETIC FIELD SUSCEPTIBILITY OF VISUAL DISPLAY UNITS
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作者 傅正财 杜亚平 J.Burnett 《Journal of Shanghai Jiaotong university(Science)》 EI 2001年第2期201-205,共5页
Extremely low frequency (ELF) magnetic field susceptibility is an index of visual display unit (VDU) quality and performance. This paper provided field measured data on the susceptibility for a large variety of VDUs. ... Extremely low frequency (ELF) magnetic field susceptibility is an index of visual display unit (VDU) quality and performance. This paper provided field measured data on the susceptibility for a large variety of VDUs. A test rig was built to study the susceptibility of VDUs to magnetic fields at fundamental and third harmonic frequencies. It was found that the susceptibility level is largely dependent on refresh rate of the VDU and the orientation of the external ELF field. It was also found that the VDU susceptibility is significantly increased in the presence of harmonic frequency magnetic fields. About 30% of the tested samples have susceptibility levels higher than that stated in IEC 1000-4-8 standard. 展开更多
关键词 visual display unit extremely low frequency magnetic field electromagnetic compatibility susceptibility test
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Energetic-ion excited internal kink modes with weak magnetic shear in q0> 1 tokamak plasmas
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作者 陈文明 王晓钢 +1 位作者 王先驱 张瑞斌 《Chinese Physics B》 SCIE EI CAS CSCD 2017年第8期259-264,共6页
The energetic particle driven internal kink mode is investigated in this paper for q0〉 1 tokamak plasma with weak magnetic shear. With the effect of energetic particles, the m/n = 1/1 internal mode structure in tokam... The energetic particle driven internal kink mode is investigated in this paper for q0〉 1 tokamak plasma with weak magnetic shear. With the effect of energetic particles, the m/n = 1/1 internal mode structure in tokamak plasma does not appear as a rigid step-function when safety factor passes through q = 1 rational surface. It is found that even when the rational surface is removed, the mode may be still unstable under the low magnetic shear condition if the energetic particle drive is strong enough; with the low shear region of safety factor profile widening, the mode becomes more unstable with its growth-rate increasing. Furthermore, we find that the existence of the q = 1 rational surface does not have a significant effect on the stability of the plasma if energetic particles are present, which is very different from the scenarios of the ideal-MHD modes. 展开更多
关键词 tokamak instabilities low magnetic shear internal kink mode
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Combined Effects of 50 Hz Magnetic Field and Magnetic Nanoparticles on the Proliferation and Apoptosis of PC12 Cells 被引量:2
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作者 JIA Hong Li WANG Chao +4 位作者 LI Yue LU Yan WANG Ping Ping PAN Wei Dong SONG Tao 《Biomedical and Environmental Sciences》 SCIE CAS CSCD 2014年第2期97-105,共9页
Objective To investigate the bioeffects of extremely low frequency (ELF) magnetic field (MF) (50 Hz, 400 μT) and magnetic nanoparticles (MNPs) via cytotoxicity and apoptosis assays on PC12 cells. Methods MNPs... Objective To investigate the bioeffects of extremely low frequency (ELF) magnetic field (MF) (50 Hz, 400 μT) and magnetic nanoparticles (MNPs) via cytotoxicity and apoptosis assays on PC12 cells. Methods MNPs modified by SiO2 (MNP-SiO2) were characterized by transmission electron microscopy (TEM), dynamic light scattering and hysteresis loop measurement. PC12 cells were administrated with MNP-SiO2 with or without MF exposure for 48 h. Cytotoxicity and apoptosis were evaluated with MTI- assay and annexin V-FITC/PI staining, respectively. The morphology and uptake of MNP-SiO2 were determined by TEM. MF simulation was performed by Ansoft Maxwell based on the finite element method. Results MNP-SiO2 were identified as -20 nm (diameter) ferromagnetic particles. MNP-SiO2 reduced cell viability in a dose-dependent manner. MF also reduced cell viability with increasing concentrations of MNP-SiO2. MNP-SiO2 alone did not cause apoptosis in PC12 cells; instead, the proportion of apoptotic cells increased significantly under MF exposure and increasing doses of MNP-SiO2. MNP-SiO2 could be ingested and then cause a slight change in cell morphology. Conclusion Combined exposure of MF and MNP-SiO2 resulted in remarkable cytotoxicity and increased apoptosis in PC12 cells. The results suggested that MF exposure could strengthen the MF of MNPs, which may enhance the bioeffects of ELF MF. 展开更多
关键词 Extremely low frequency magnetic field magnetic nanoparticles CYTOTOXICITY APOPTOSIS MORPHOLOGY
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High Energy and High Coercivity Sintered NdFeB Magnets by Low Oxygen Process 被引量:5
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作者 Kaihong DING, Guozheng LIU, Zhejun LI, Jieming YAN, Yingjie TAO and Bing WU (Baotou Research Institute of Rare Earth, Baotou 014010, China) 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2000年第2期127-128,共2页
Using ball milling and single direction pressing, we can produce high performance NdFeB sintered magnets. The oxygen content of sintered magnets can be controlled under 1500xl0^-6 and the magnetic performance can be i... Using ball milling and single direction pressing, we can produce high performance NdFeB sintered magnets. The oxygen content of sintered magnets can be controlled under 1500xl0^-6 and the magnetic performance can be improved by using low oxygen processing. The high preformance NdFeB sintered magnets with Br=(1.4 ± 0.2)T, iHc>796 kA/m and (BH)max=(390± 16) kJ/m^3, have been batch produced. 展开更多
关键词 NDFEB CO High Energy and High Coercivity Sintered NdFeB Magnets by low Oxygen Process
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A low-outgassing-rate carbon fiber array cathode
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作者 李安昆 樊玉伟 +2 位作者 钱宝良 张自成 荀涛 《Chinese Physics B》 SCIE EI CAS CSCD 2018年第2期613-618,共6页
In this paper, a new carbon fiber based cathode — a low-outgassing-rate carbon fiber array cathode — is investigated experimentally, and the experimental results are compared with those of a polymer velvet cathode. ... In this paper, a new carbon fiber based cathode — a low-outgassing-rate carbon fiber array cathode — is investigated experimentally, and the experimental results are compared with those of a polymer velvet cathode. The carbon fiber array cathode is constructed by inserting bunches of carbon fibers into the cylindrical surface of the cathode. In experiment, the diode base pressure is maintained at 1×10^(-2) Pa–2×10^(-2) Pa, and the diode is driven by a compact pulsed power system which can provide a diode voltage of about 100 kV and pulse duration of about 30 ns at a repetition rate of tens of Hz.Real-time pressure data are measured by a magnetron gauge. Under the similar conditions, the experimental results show that the outgassing rate of the carbon fiber array cathode is an order smaller than that of the velvet cathode and that this carbon fiber array cathode has better shot-to-shot stability than the velvet cathode. Hence, this carbon fiber array cathode is demonstrated to be a promising cathode for the radial diode, which can be used in magnetically insulated transmission line oscillator(MILO) and relativistic magnetron(RM). 展开更多
关键词 high power microwave magnetically insulated transmission line oscillator carbon fiber array cathode low outgassing rate
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A Novel Method to Enhance the Inversion Speed and Precision of the NMR T_(2) Spectrum by the TSVD Based Linearized Bregman Iteration
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作者 Yiguo Chen Congjun Feng +4 位作者 Yonghong He Zhijun Chen Xiaowei Fan Chao Wang Xinmin Ge 《Computer Modeling in Engineering & Sciences》 SCIE EI 2023年第9期2451-2463,共13页
The low-field nuclear magnetic resonance(NMR)technique has been used to probe the pore size distribution and the fluid composition in geophysical prospecting and related fields.However,the speed and accuracy of the ex... The low-field nuclear magnetic resonance(NMR)technique has been used to probe the pore size distribution and the fluid composition in geophysical prospecting and related fields.However,the speed and accuracy of the existing numerical inversion methods are still challenging due to the ill-posed nature of the first kind Fredholm integral equation and the contamination of the noises.This paper proposes a novel inversion algorithmto accelerate the convergence and enhance the precision using empirical truncated singular value decompositions(TSVD)and the linearized Bregman iteration.The L1 penalty term is applied to construct the objective function,and then the linearized Bregman iteration is utilized to obtain fast convergence.To reduce the complexity of the computation,empirical TSVD is proposed to compress the kernel matrix and determine the appropriate truncated position.This novel inversion method is validated using numerical simulations.The results indicate that the proposed novel method is significantly efficient and can achieve quick and effective data solutions with low signal-to-noise ratios. 展开更多
关键词 low field nuclear magnetic resonance linearized bregman iteration truncated singular value decomposition numerical simulations
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Preparation and Magnetostriction of Tb_(0.22)Dy_(0.48)Ho_(0.35)Fe_2 Alloys
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作者 江民红 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第S2期198-201,共4页
Tb0.22Dy0.48Ho0.35Fe2 quaternary alloys are prepared by melting-top casting-annealing process. X-ray diffraction reveals that the alloy is single phase polycrystalline alloy with MgCu2 type cubic Laves phase structure... Tb0.22Dy0.48Ho0.35Fe2 quaternary alloys are prepared by melting-top casting-annealing process. X-ray diffraction reveals that the alloy is single phase polycrystalline alloy with MgCu2 type cubic Laves phase structure, and (511) preferred orientation occurs in its. The magnetostriction measurements are carried out at room temperature using standard strain gauge technique in magnetic fields up to 400 kA·m-1. The results show that when the magnetic field, H, is 90 kA·m-1, the magnetostriction, λ, of Tb0.22Dy0.48Ho0.35Fe2 quaternary alloys is 260×10-6, and when the H is 210 kA·m-1, the λ is 438×10-6. When the H is 400 kA·m-1, the λ is up to the saturation value, 538×10-6. As compared with TbDyFe ternary alloys, the λ of the quaternary alloy is significantly higher when the H is less than or equal to 210 kA·m-1. When the H is 120 kA·m-1, the λ of the alloy is 333×10-6, 70×10-6 more than the ternary alloy. Research results and mechanism are discussed. 展开更多
关键词 MAGNETOSTRICTION Tb0.22Dy0.48Ho0.35Fe2 Laves phase low magnetic field
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Influence of the low voltage pulsed magnetic field on the columnar-to-equiaxed transition during directional solidification of superalloy K4169 被引量:8
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作者 Kuiliang Zhang Yingju Li Yuansheng Yang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2020年第13期9-17,共9页
The low voltage pulsed magnetic field(LVPMF)disrupts the columnar dendrite growth,and the columnarto-equiaxed transition(CET)occurs during the directional solidification of superalloy K4169.Within the pulse voltage ra... The low voltage pulsed magnetic field(LVPMF)disrupts the columnar dendrite growth,and the columnarto-equiaxed transition(CET)occurs during the directional solidification of superalloy K4169.Within the pulse voltage ranging from 100Vto 200 V,a transition from columnar to equiaxed grain was observed,and the grain size decreased as the pulse voltage rised.As the pulse frequency increased,the CET occurred,and the grains were refined.However,the grains became coarse,and the solidification structure was columnar crystal again when frequency increased to 10 Hz.The LVPMF had an optimal frequency to promote CET.The LVPMF on the CET was affected by the withdrawal speed and increasing the withdrawal speed enhances the CET.The distribution of electromagnetic force and flow field in the melt under the LVPMF were modeled and simulated to reveal the CET mechanism.It is considered that the CET should be attributed to the coupling effects of magnetic vibration and melt convection induced by the LVPMF. 展开更多
关键词 CET low voltage pulsed magnetic field Simulation Directional solidification SUPERALLOY
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Effects of extremely low frequency magnetic field on anxiety level and spatial memory of adult rats 被引量:2
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作者 HE Li-hua SHI Hong-mei +3 位作者 LIUTong-tong XU Ying-chun YE Kang-ping WANG Sheng 《Chinese Medical Journal》 SCIE CAS CSCD 2011年第20期3362-3366,共5页
Background As the widespread use of electric devices in modern life, human are exposed to extremely low frequency magnetic fields (ELF MF) much more frequently than ever. Over the past decades, a substantial number ... Background As the widespread use of electric devices in modern life, human are exposed to extremely low frequency magnetic fields (ELF MF) much more frequently than ever. Over the past decades, a substantial number of epidemiological and experimental studies have demonstrated that ELF MF (50 Hz) exposure is associated with increased risk of various health effects. The present study examined the effects of chronic exposure to ELF MF on anxiety level and spatial memory of adult rats. Methods The 50-Hz ELF MF was used during the whole experimental procedures and the value of magnetic field (MF) was set to 2 mT. Adult rats were divided randomly to control, MF 1 hour and MF 4 hours group. Anxiety-related behaviors were examined in the open field test and the elevated plus maze; changes in spatial learning and memory were determined in Morris water maze aRer 4 weeks of daily exposure. Results Rats in MF 4 hours group had increased anxiety-like behaviors with unaltered locomotor activity. In the Morris water maze test, rats had reduced latency to find the hidden platform and improved long-term memory of former location of platform without changes in short-term memory and locomotor activity. Conclusion Chronic ELF MF exposure has anxiogenic effect on rats, and the promoting effects on spatial learning and long-term retention of spatial memory. 展开更多
关键词 extremely low frequency magnetic field ANXIETY spatial memory Morris water maze test open field test
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Novel compact and lightweight coaxial C-band transit-time oscillator 被引量:1
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作者 邓晓波 贺军涛 +4 位作者 令钧溥 邓秉方 宋莉莉 阳福香 徐伟力 《Chinese Physics B》 SCIE EI CAS CSCD 2020年第9期384-389,共6页
Compactness and miniaturization have become increasingly important in the development of high-power microwave devices.Based on this rising demand,a novel C-band coaxial transit-time oscillator(TTO)with a low external ... Compactness and miniaturization have become increasingly important in the development of high-power microwave devices.Based on this rising demand,a novel C-band coaxial transit-time oscillator(TTO)with a low external guiding magnetic field is proposed and analyzed.The proposed device has the following advantages:simple structure,short axial length,high power conversion efficiency,and low external guiding magnetic field,which are of great significance for developing the compact and miniaturized high-power microwave devices.The application of a shorter axial length is made possible by the use of a transit radiation mechanism.Also,loading the opening foil symmetrically to both ends of the buncher helps reduce the external magnetic field of the proposed device.Unlike traditional foils,the proposed opening foil has a circular-hole;therefore,the electron beam will not bombard the conductive foil to generate plasma.This makes it possible to realize long pulse and high repetition rate operation of the device in future experiments.Through numerical calculation and PIC particle simulation,the stability of the intense relativistic electron beam(IREB)and the saturation time of the device are improved by using the conductive foil.The voltage and current of the diode are 548 kV and 11.4 kA,respectively.Under a 0.4-T external guiding magnetic field,a C-band output microwave with a frequency of 4.27 GHz and power of 1.88 GW can be generated.The power conversion efficiency of the proposed device is about 30%. 展开更多
关键词 low guiding magnetic field foil focus simple structure short axial length
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Decoding brain responses to pixelized images in the primary visual cortex: implications for visual cortical prostheses 被引量:3
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作者 Bing-bing Guo Xiao-lin Zheng +4 位作者 Zhen-gang Lu Xing Wang Zheng-qin Yin Wen-sheng Hou Ming Meng 《Neural Regeneration Research》 SCIE CAS CSCD 2015年第10期1622-1627,共6页
Visual cortical prostheses have the potential to restore partial vision. Still limited by the low-resolution visual percepts provided by visual cortical prostheses, implant wearers can currently only "see" pixelized... Visual cortical prostheses have the potential to restore partial vision. Still limited by the low-resolution visual percepts provided by visual cortical prostheses, implant wearers can currently only "see" pixelized images, and how to obtain the specific brain responses to different pixelized images in the primary visual cortex(the implant area) is still unknown. We conducted a functional magnetic resonance imaging experiment on normal human participants to investigate the brain activation patterns in response to 18 different pixelized images. There were 100 voxels in the brain activation pattern that were selected from the primary visual cortex, and voxel size was 4 mm × 4 mm × 4 mm. Multi-voxel pattern analysis was used to test if these 18 different brain activation patterns were specific. We chose a Linear Support Vector Machine(LSVM) as the classifier in this study. The results showed that the classification accuracies of different brain activation patterns were significantly above chance level, which suggests that the classifier can successfully distinguish the brain activation patterns. Our results suggest that the specific brain activation patterns to different pixelized images can be obtained in the primary visual cortex using a 4 mm × 4 mm × 4 mm voxel size and a 100-voxel pattern. 展开更多
关键词 nerve regeneration primary visual cortex electrical stimulation visual cortical prosthesis low resolution vision pixelized image functional magnetic resonance imaging voxel size neural regeneration brain activation pattern
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Insights into spin polarization regulated exciton dissociation and charge separation of C_(3)N_(4)for efficient hydrogen evolution and simultaneous benzylamine oxidation 被引量:1
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作者 Gen Li Xiaomei Sun +4 位作者 Peng Chen Meiyang Song Tianxiang Zhao Fei Liu Shuang-Feng Yin 《Nano Research》 SCIE EI CSCD 2023年第7期8845-8852,共8页
The employment of spin polarization under an external magnetic field holds great potential for the improvements of photocatalytic performance.However,owing to the huge difference in dielectric properties between ferro... The employment of spin polarization under an external magnetic field holds great potential for the improvements of photocatalytic performance.However,owing to the huge difference in dielectric properties between ferromagnetic oxide and polymers,the photogenerated excitons with spin states are often limited to the ferromagnetic oxide wells,which leads to unsatisfactory activity.In this paper,a single-atom Co-doped C_(3)N_(4)photocatalyst is successfully synthesized for photocatalytic water splitting and simultaneous oxidation of benzylamine.Under a tiny external magnetic field(24.5 mT),the hydrogen production rate could reach at 3979.0μmol·g^(-1)·h^(-1),which is about 340 times that of C_(3)N_(4).Experimental results and theoretical calculations indicate that the interaction of Co d and N p orbital changes the symmetry center of C_(3)N_(4),resulting in an increase in dielectric constant and spin polarization.Moreover,magnetic fields further promote parallel electron spin,and the increased number of charges with the parallel spin-down state is likely to dissociate under the action of an external magnetic field.On the other hand,the Co-N bond provides a huge built-in electric field and active site for strengthening the charge transfer and surface reaction.This work not only deepens the understanding of spin polarization,but also enriches methods to accelerate electron-hole separation. 展开更多
关键词 low magnetic field C_(3)N_(4) spin polarization photocatalytic hydrogen evolution benzylamine oxidation
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Development of the relativistic backward wave oscillator with a permanent magnet 被引量:4
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作者 马乔生 刘忠 +1 位作者 李正红 金晓 《Chinese Physics C》 SCIE CAS CSCD 2012年第8期753-755,共3页
Firstly, an X-band relativistic backward wave oscillator with a low guiding magnetic field is simulated, whose output microwave power is 520 MW. Then, an experiment is carried out on an accelerator to investigate a re... Firstly, an X-band relativistic backward wave oscillator with a low guiding magnetic field is simulated, whose output microwave power is 520 MW. Then, an experiment is carried out on an accelerator to investigate a relativistic backward wave oscillator with a permanent magnetic field whose strength is 0.46 T. When the energy of the electron is 630 keV and the current of the electron beam is 6.7 kA, a 15 ns width pulsed microwave with 510 MW output power at 8.0 GHz microwave frequency is achieved. 展开更多
关键词 permanent magnet relativistic backward wave oscillator low magnetic field
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Simultaneous Determination of Oil and Water in Soybean by LF-NMR Relaxometry and Chemometrics 被引量:2
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作者 WU Jing LI Yanru GAO Xingsheng 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2016年第5期731-735,共5页
A fast, non-destructive and eco-friendly method was developed to simultaneously determine the oil and water contents of soybean based on low field nuclear magnetic resonance(LF-NMR) relaxometry combined with chemome... A fast, non-destructive and eco-friendly method was developed to simultaneously determine the oil and water contents of soybean based on low field nuclear magnetic resonance(LF-NMR) relaxometry combined with chemometrics, such as partial least squares regression(PLSR). The Carr-Purcell-Meiboom-Gill(CPMG) magnetiza- tion decay data of ten soybean samples were acquired by LF-NMR and directly applied to the PLSR analysis. Cali- bration models were established via PLSR with full cross-validation based on the reference values obtained by the Soxhlet extraction method for measuring oil and oven-drying method for measuring water. The results indicate that the calibration models are satisfactory for both oil and water determinations; the root mean squared errors of cross-validation(RMSECV) for oil and water are 0.2285% and 0.0178%, respectively. Furthermore, the oil and water contents in unknown soybean samples were predicted by the PLSR models and the results were compared with the reference values. The relative errors of the predicted oil and water contents were in ranges of 1.25%---4.96% and 0.44%--2.49%, respectively. These results demonstrate that the combination of LF-NMR relaxometry with chemo- metrics shows great potential for the simultaneous determination of contents of oil and water in soybean with high accuracy. 展开更多
关键词 low field nuclear magnetic resonance(LF-NMR) SOYBEAN Oil content Water content Partial leastsquares regression(PLSR)
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Pore size distribution of high volatile bituminous coal of the southern Junggar Basin: a full-scale characterization applying multiple methods 被引量:1
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作者 Wanchun ZHAO Xin LI +1 位作者 Tingting WANG Xuehai FU 《Frontiers of Earth Science》 SCIE CSCD 2021年第2期237-255,共19页
Studying on the pore size distribution of coal is vital for determining reasonable coalbed methane development strategies.The coalbed methane project is in progress in the southern Junggar Basin of northwestern China,... Studying on the pore size distribution of coal is vital for determining reasonable coalbed methane development strategies.The coalbed methane project is in progress in the southern Junggar Basin of northwestern China,where high volatile bituminous coal is reserved.In this study,with the purpose of accurately characterizing the full-scale pore size distribution of the high volatile bituminous coal of the southern Junggar Basin,two grouped coal samples were applied for mercury intrusion porosimetry,low-temperature nitrogen adsorption,low-field nuclear magnetic resonance,rate-controlled mercury penetration,scanning electron microscopy,and nano-CT measurements.A comprehensive pore size distribution was proposed by combining the corrected mercury intrusion porosimetry data and low-temperature nitrogen adsorption data.The relationship between transverse relaxation time(T2,ms)and the pore diameter was determined by comparing the T2 spectrum with the comprehensive pore size distribution.The macro-pore and throat size distributions derived from nano-CT and rate-controlled mercury penetration were distinguishingly analyzed.The results showed that:1)comprehensive pore size distribution analysis can be regarded as an accurate method to characterize the pore size distribution of high volatile bituminous coal;2)for the high volatile bituminous coal of the southern Junggar Basin,the meso-pore volume was the greatest,followed by the transition pore volume or macro-pore volume,and the micro-pore volume was the lowest;3)the relationship between T2 and the pore diameter varied for different samples,even for samples with close maturities;4)the throat size distribution derived from nano-CT was close to that derived from rate-controlled mercury penetration,while the macro-pore size distributions derived from those two methods were very different.This work can deepen the knowledge of the pore size distribution characterization techniques of coal and provide new insight for accurate pore size distribution characterization of high volatile bituminous coal. 展开更多
关键词 pore size distribution coalbed methane high volatile bituminous coal low field nuclear magnetic resonance the southern Junggar Basin
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