Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared wi...Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy （OM）, transmission electron microscopy （TEM）, and energy dispersive spectrometry （EDS）. The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are narrowed; the precipitates, whose quantity in normalized plate is more than that in hot-rolled plate greatly, are mainly A1N, MnS, composite precipitates （Cu,Mn）S and so on. Normalizing technology with a temperature of 1120 ℃, holding for 3 min, and a two-stage cooling is a most advantaged method to obtain oriented silicon steel with sharper Goss texture and higher magnetic properties, owing to the uniform surface microstructures and the obvious inhomogeneity of microstructures along the thickness. The normalizing technology with the two-stage cooling is the optimum process, which can generate more fine precipitates dispersed over the matrix, and be beneficial for finished products to get higher magnetic properties.展开更多
The microstructure characteristics and mechanical properties of a low-silicon TRIP steel containing phosphorus and vanadium at different finish rolling temperatures were studied by laboratory hot rolling experiments. ...The microstructure characteristics and mechanical properties of a low-silicon TRIP steel containing phosphorus and vanadium at different finish rolling temperatures were studied by laboratory hot rolling experiments. Dif- ferent ratios of multiphase microstructure （ferrite, granular bainite and retained austenite） are obtained. With a decrease in finish rolling temperature, the volume fractions of ferrite and retained austenite increase. EBSD analysis re veals that most of the ferrite grains are fine, and decreasing of finish rolling temperature leads to an increase in low angle boundaries. Under the joint effects of fine grain strengthening, dislocation strengthening and precipitation strengthening, higher strength is obtained. When the finish rolling temperature is decreased to 800 ℃, the steel has excellent mechanical properties： Rp0.2 =470 MPa; Rm=960 MPa; Rp0. 2/Rm=0. 49; A50 =19.7%; n=0. 25.展开更多
Low-temperature slab-reheated grain-oriented silicon steel is characterized by a sharp {411}〈148〉 primary recrystallization texture. To date, the influence of this texture on secondary recrystallization is not clear...Low-temperature slab-reheated grain-oriented silicon steel is characterized by a sharp {411}〈148〉 primary recrystallization texture. To date, the influence of this texture on secondary recrystallization is not clear. Microtextures in primary and secondary reerystallized sheets of low-temperature reheated grain-oriented silicon steel were examined using electron backscatter diffraction. By comparing the textures and microstructures of specific primary reerystallized grains neighboring secondary grains with those of other primary grains, the influences of primary re- crystallization textures and microstructures on the orientations of secondary grains were investigated. Results show that for low-temperature reheated graiworiented silicon steel, the primary recrystallization sheet comprises { 411 } 〈148〉, {111}〈112〉, and {001}〈120〉 texture componems. During secondary recrystallization, the {111}〈112〉 primary recrystallized grains were easily consumed by abnormally grown Goss, deviated Goss, Brass, or {210}〈001〉grains ;the { 411 }〈148〉 primary recrystallized grains were more resistant to being swallowed; and the {001} 〈120 grains were the most resistant to being consumed. For a particular primary grain, the distribution of its surrounding grain boundaries determined how easily it is consumed during secondary recrystallization. Primary grains surrounded by 20°- 45° grain boundaries were consumed much earlier than those having grain boundaries above 45°, which is in accordance with high-energy grain boundary theory. In addition, special ∑9 boundaries between {411}〈148〉 and Goss grains move more slowly than ∑9 boundaries between {111 }〈112〉 and Goss grains, which is attributed to the different positions of 〈110〉 rotation axis with respect to the normals of grain boundaries.展开更多
The effects of final air cooling temperature on the microstructure and mechanical properties of hot rolled 0.2C-1.9Mn-0.5Si-0.08P TRIP steel were studied by utilizing OM, SEM, TEM and tensile tests. Experimental resul...The effects of final air cooling temperature on the microstructure and mechanical properties of hot rolled 0.2C-1.9Mn-0.5Si-0.08P TRIP steel were studied by utilizing OM, SEM, TEM and tensile tests. Experimental results showed that in the multiphase microstructure of the investigated steel when the finish rolling temperature was about 820 ℃ and the final air cooling temperature was in the range of 630-700 ℃, the grain size of most of ferrite was finer (about 4 μm) and which had higher dislocation density, the bainite packets had chaotic orientations and lath boundaries of bainite were not quite straight, the retained austenite distributed in the ferrite grain boundaries or triradius was fine and dispersive, and their grain size was about 0.4-1.9 μm. With increasing the amount of ferrite, the volume fraction of retained austenite had a slight decrease. When the final air cooling temperature was 630 ℃, the steel had excellent mechanical properties, which was characterized by combination of continuous yielding, high strength (about 796 MPa) and high elongation (22.7%) as well as low yield/strength ratio (0.58); when the final air cooling temperature increased to 700 ℃, the matrix structure was bainite packets and the comprehensive properties were deteriorated.展开更多
基金Projects(51274083,51074062)supported by the National Natural Science Foundation of China
文摘Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy （OM）, transmission electron microscopy （TEM）, and energy dispersive spectrometry （EDS）. The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are narrowed; the precipitates, whose quantity in normalized plate is more than that in hot-rolled plate greatly, are mainly A1N, MnS, composite precipitates （Cu,Mn）S and so on. Normalizing technology with a temperature of 1120 ℃, holding for 3 min, and a two-stage cooling is a most advantaged method to obtain oriented silicon steel with sharper Goss texture and higher magnetic properties, owing to the uniform surface microstructures and the obvious inhomogeneity of microstructures along the thickness. The normalizing technology with the two-stage cooling is the optimum process, which can generate more fine precipitates dispersed over the matrix, and be beneficial for finished products to get higher magnetic properties.
基金Item Sponsored by National Natural Science Foundation of China (50734001,51174059,50971039)Fundamental Research Funds for Central Universities of China (N090407001)
文摘The microstructure characteristics and mechanical properties of a low-silicon TRIP steel containing phosphorus and vanadium at different finish rolling temperatures were studied by laboratory hot rolling experiments. Dif- ferent ratios of multiphase microstructure （ferrite, granular bainite and retained austenite） are obtained. With a decrease in finish rolling temperature, the volume fractions of ferrite and retained austenite increase. EBSD analysis re veals that most of the ferrite grains are fine, and decreasing of finish rolling temperature leads to an increase in low angle boundaries. Under the joint effects of fine grain strengthening, dislocation strengthening and precipitation strengthening, higher strength is obtained. When the finish rolling temperature is decreased to 800 ℃, the steel has excellent mechanical properties： Rp0.2 =470 MPa; Rm=960 MPa; Rp0. 2/Rm=0. 49; A50 =19.7%; n=0. 25.
基金Item Sponsored by National High Technology Research and Development Program of China(2012AA03A505)
文摘Low-temperature slab-reheated grain-oriented silicon steel is characterized by a sharp {411}〈148〉 primary recrystallization texture. To date, the influence of this texture on secondary recrystallization is not clear. Microtextures in primary and secondary reerystallized sheets of low-temperature reheated grain-oriented silicon steel were examined using electron backscatter diffraction. By comparing the textures and microstructures of specific primary reerystallized grains neighboring secondary grains with those of other primary grains, the influences of primary re- crystallization textures and microstructures on the orientations of secondary grains were investigated. Results show that for low-temperature reheated graiworiented silicon steel, the primary recrystallization sheet comprises { 411 } 〈148〉, {111}〈112〉, and {001}〈120〉 texture componems. During secondary recrystallization, the {111}〈112〉 primary recrystallized grains were easily consumed by abnormally grown Goss, deviated Goss, Brass, or {210}〈001〉grains ;the { 411 }〈148〉 primary recrystallized grains were more resistant to being swallowed; and the {001} 〈120 grains were the most resistant to being consumed. For a particular primary grain, the distribution of its surrounding grain boundaries determined how easily it is consumed during secondary recrystallization. Primary grains surrounded by 20°- 45° grain boundaries were consumed much earlier than those having grain boundaries above 45°, which is in accordance with high-energy grain boundary theory. In addition, special ∑9 boundaries between {411}〈148〉 and Goss grains move more slowly than ∑9 boundaries between {111 }〈112〉 and Goss grains, which is attributed to the different positions of 〈110〉 rotation axis with respect to the normals of grain boundaries.
基金Fundamental Research Funds for the Central Universities (N090407001)National Key Project of Scientific and Technical Supporting Programs(2007BAE51B07)National Natural Science Foundation of China (50734001)
文摘The effects of final air cooling temperature on the microstructure and mechanical properties of hot rolled 0.2C-1.9Mn-0.5Si-0.08P TRIP steel were studied by utilizing OM, SEM, TEM and tensile tests. Experimental results showed that in the multiphase microstructure of the investigated steel when the finish rolling temperature was about 820 ℃ and the final air cooling temperature was in the range of 630-700 ℃, the grain size of most of ferrite was finer (about 4 μm) and which had higher dislocation density, the bainite packets had chaotic orientations and lath boundaries of bainite were not quite straight, the retained austenite distributed in the ferrite grain boundaries or triradius was fine and dispersive, and their grain size was about 0.4-1.9 μm. With increasing the amount of ferrite, the volume fraction of retained austenite had a slight decrease. When the final air cooling temperature was 630 ℃, the steel had excellent mechanical properties, which was characterized by combination of continuous yielding, high strength (about 796 MPa) and high elongation (22.7%) as well as low yield/strength ratio (0.58); when the final air cooling temperature increased to 700 ℃, the matrix structure was bainite packets and the comprehensive properties were deteriorated.
