Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range...Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range of experimental techniques, such as X-ray diffraction, scanning electronic microscopy, and infrared spectroscopy. It was revealed that the structures of the produced zeolites were dependent on the molar ratios of the reactants and hydrothermal reaction conditions, so the synthesis conditions were optimized to obtain pure zeolite NaA. Adsorption of nitrogen and carbon dioxide on the prepared zeolite NaA was also measured and analyzed. The results showed that zeolite NaA could be prepared with reasonable purity, it had physicochemical properties comparable with zeolite NaA made from other methods, and it had excellent gas adsorption properties, thus demonstrating that zeolite NaA could be prepared from nickel laterite residue.展开更多
The dissolution behavior of nickel during the oxygen chloride leaching of the copper residue was investigated.Technological variables of the leaching,including oxygen flow rate,concentrations of chloride and sulfuric...The dissolution behavior of nickel during the oxygen chloride leaching of the copper residue was investigated.Technological variables of the leaching,including oxygen flow rate,concentrations of chloride and sulfuric acid,and temperature,were discussed.展开更多
An austenitic stainless steel 1Cr18Ni9Ti and a solid solution-strengthened Ni-base superalloy GH30 were shock processed using a Q-switched pulsed Nd-glass laser. Microstructure, hardness and residual stress of the las...An austenitic stainless steel 1Cr18Ni9Ti and a solid solution-strengthened Ni-base superalloy GH30 were shock processed using a Q-switched pulsed Nd-glass laser. Microstructure, hardness and residual stress of the laser shock processed surface were investigated as functions of laser processing parameters. Results show that high density of dislocations and fine deformation twins are produced in the laser shock processed surface layers in both the austenitic stainless steel and the nickel-base superalloy. Extensive strain-induced martensite was also observed in the laser shock processed zone of the austenitic steel. The hardness of the laser shock processed surface was significantly enhanced and compressive stress as high as 400 MPa was produced in the laser shock processed surface.展开更多
X-ray diffraction was utilized to measure the residual stress of 45 mm UNS N08810 plates after post-weld heat treatment at temperatures of 680℃ and 900℃, which showed reductions of 86.9% and 71.6% in the residual st...X-ray diffraction was utilized to measure the residual stress of 45 mm UNS N08810 plates after post-weld heat treatment at temperatures of 680℃ and 900℃, which showed reductions of 86.9% and 71.6% in the residual stress, respectively. This indicates that post-weld heat treatment can play a significant role in reducing residual stress, while no significant effects on tensile stress and micro-hardness of the welding joint were observed after treatment.展开更多
基金financially supported by the Fundamental Research Funds for the Central Universities of China (No. N120302006)the China Postdoctoral Science Foundation(No. 2013M530939)the Key Programs on Social Development of Liaoning Province, China (No. 2012201011)
文摘Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range of experimental techniques, such as X-ray diffraction, scanning electronic microscopy, and infrared spectroscopy. It was revealed that the structures of the produced zeolites were dependent on the molar ratios of the reactants and hydrothermal reaction conditions, so the synthesis conditions were optimized to obtain pure zeolite NaA. Adsorption of nitrogen and carbon dioxide on the prepared zeolite NaA was also measured and analyzed. The results showed that zeolite NaA could be prepared with reasonable purity, it had physicochemical properties comparable with zeolite NaA made from other methods, and it had excellent gas adsorption properties, thus demonstrating that zeolite NaA could be prepared from nickel laterite residue.
文摘The dissolution behavior of nickel during the oxygen chloride leaching of the copper residue was investigated.Technological variables of the leaching,including oxygen flow rate,concentrations of chloride and sulfuric acid,and temperature,were discussed.
文摘An austenitic stainless steel 1Cr18Ni9Ti and a solid solution-strengthened Ni-base superalloy GH30 were shock processed using a Q-switched pulsed Nd-glass laser. Microstructure, hardness and residual stress of the laser shock processed surface were investigated as functions of laser processing parameters. Results show that high density of dislocations and fine deformation twins are produced in the laser shock processed surface layers in both the austenitic stainless steel and the nickel-base superalloy. Extensive strain-induced martensite was also observed in the laser shock processed zone of the austenitic steel. The hardness of the laser shock processed surface was significantly enhanced and compressive stress as high as 400 MPa was produced in the laser shock processed surface.
文摘X-ray diffraction was utilized to measure the residual stress of 45 mm UNS N08810 plates after post-weld heat treatment at temperatures of 680℃ and 900℃, which showed reductions of 86.9% and 71.6% in the residual stress, respectively. This indicates that post-weld heat treatment can play a significant role in reducing residual stress, while no significant effects on tensile stress and micro-hardness of the welding joint were observed after treatment.
