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High Precision Thermal Ionization Mass Spectrometric Dating of Corals and Its Application to Paleo-Environmental Study
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作者 王兆荣 张兆峰 +1 位作者 彭子成 马志邦 《Chinese Journal Of Geochemistry》 EI CAS 2001年第2期138-143,共6页
Global change has become a hot spot in Quaternary geology, and high\|precision, high\|sensitivity dating is also an urgent problem which needs to be solved. This paper presents some achievements in U\|series dating of... Global change has become a hot spot in Quaternary geology, and high\|precision, high\|sensitivity dating is also an urgent problem which needs to be solved. This paper presents some achievements in U\|series dating of marine corals by thermal ionization mass spectrometry (TIMS) and its application to the study of paleo\|environments. Recently, coral samples were determined for their ages on a MAT\|262 mass spectrometer and satisfactory results have been obtained. 展开更多
关键词 光谱分析 珊瑚 古环境 全球变化
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High-precision U-series dating of Holocene corals from South China Sea by thermal ionization mass spectrometry(TIMS) 被引量:5
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作者 Zhibang Ma Ming Xia +4 位作者 Chenghui Zhang Zicheng Pen Zhaorong Wang Weidong Sun Zhisheng An 《Chinese Science Bulletin》 SCIE EI CAS 1999年第10期937-941,共5页
Using the isotopic diluting and thermal ionization mass spectrometric (TIMS) technique, the U-series dating procedure was established on the basis of measurement of national standard GBW04412. With this highly precise... Using the isotopic diluting and thermal ionization mass spectrometric (TIMS) technique, the U-series dating procedure was established on the basis of measurement of national standard GBW04412. With this highly precise technique the Holocene corals from the South China Sea were dated. Comparison between this method and α-spectrometry was made. The results show that a thriving period of corals in the South China Sea appeared at 6 800—5 800 a BP, during which the paleosea level was the higher than at present in the Holecene. 展开更多
关键词 HOLOCENE corals REEFS mass spectrometric u-series dating South China Sea.
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Precise timing of lacustrine gypsum in Luobubo,Xinjiang using the thermal ionization mass spectrometry U-series method 被引量:10
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作者 PENG Zicheng LIU Weiguo +2 位作者 ZHANG Pengxi ZHANG Zhaofeng ZHOU Jie 《Chinese Science Bulletin》 SCIE EI CAS 2001年第18期1538-1541,共4页
Dating techniques including gypsum dissolution in water, iron hydroxide co-precipitation with uranium and thorium and mass spectrometric determination have been investigated in this note. The ages of the gypsum sample... Dating techniques including gypsum dissolution in water, iron hydroxide co-precipitation with uranium and thorium and mass spectrometric determination have been investigated in this note. The ages of the gypsum samples in a CK core from Luobubo lacustrine sediments are in the range of (12.85±0.21) kaBP (4 m distance from the top core) to (153.2 ± 7.2) kaBP (49 m distance from the top core) with the relative errors of ( 1.6%-±4.7%. It indicates that the sedimental environment of the CK core was situated in the middle-late Pleistocene and Holocene periods, corresponding to 1-6 stages of oxygen isotopes in the abyssal sediments and included much information from last inter-glacial to Holocene warm periods. 展开更多
关键词 thermal ionization mass spectrometry (TIMS) u-series dating GYPSUM mineral water DISSOLUTION environmental information.
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High-Resolution Dating of Stalagmites and Reconstruction of Paleo-Environments
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作者 王兆荣 袁道先 +3 位作者 林玉石 张美良 周杰 刘卫国 《Chinese Journal Of Geochemistry》 EI CAS 2001年第3期282-288,共7页
The discovery of abrupt paleo\|climate change events and the prediction of environmental changes in the future time have raised an urgent request for high\|resolution paleo\|environmental records. This paper reviews t... The discovery of abrupt paleo\|climate change events and the prediction of environmental changes in the future time have raised an urgent request for high\|resolution paleo\|environmental records. This paper reviews the progress made in chronology and paleo\|environment of stalagmites from karst caves in China and presents some of the results of TIMS\|U\|series dating of stalagmites composed of secondary carbonates, taken from the Dongge, Longquan and Yamen karst caves in Libo County and the Qixing karst cave in Duyun, Guizhou Province, on a MAT\|262 mass spectrometer. 展开更多
关键词 精度 TIMS-U测定 光谱分析 贵州 古气候 古环境 石笋
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无氧铜样品盘异常热本底对激光^(40)Ar/^(39)Ar定年的影响
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作者 师文贝 韩志宇 +1 位作者 杨列坤 王非 《岩矿测试》 CAS CSCD 北大核心 2023年第4期737-747,共11页
激光^(40)Ar/^(39)Ar定年方法中扣除的本底是样品测试过程中的系统冷本底。在满足激光加热样品时样品盘升温幅度有限和样品盘已完全脱气两个条件的情况下,这一处理方式的有效性才能得到保证。本文利用具有不同大气暴露史的无氧铜样品盘... 激光^(40)Ar/^(39)Ar定年方法中扣除的本底是样品测试过程中的系统冷本底。在满足激光加热样品时样品盘升温幅度有限和样品盘已完全脱气两个条件的情况下,这一处理方式的有效性才能得到保证。本文利用具有不同大气暴露史的无氧铜样品盘结合透长石标准样品YBCs,使用相同的脱气及测试流程,对比分析了不同样品盘的冷、热本底以及放置于不同样品盘时YBCs的大气氩含量。分析结果表明,放置于暴露大气14个月的样品盘内时,YBCs透长石大气氩含量高达约34.4%,使用预先激光去气的样品盘此值可降低至约2%;暴露大气约10个月的样品盘,激光加热其两个样品孔时,^(40)Ar脱气量可达约1.6×10−14~3.1×10−14mol;暴露时长约为26个月的样品盘,^(40)Ar含量升高至约0.8×10^(−13)~2.0×10^(−13)mol;它们均远高于系统冷本底3.8×10^(−16)~6.2×10^(−16)mol。两个样品盘热本底^(40)Ar/36Ar值约为310,高于大气氩比值。因此,对于暴露大气时间较长的样品盘,约150℃去气四天的流程不足以使其完全脱气。激光加热样品时会导致样品盘局部升温,脱气不完全的样品盘会释放出大量热本底。模拟以及标准样品测试均显示了这种情况会影响辐照参数J值以及年龄的计算。激光微量年轻样品^(40)Ar/^(39)Ar定年过程中,建议装样后对无氧铜样品盘进行300~400℃至少5h的预脱气,以保证测试数据质量。实验室不具备预脱气条件时,持续使用同一样品盘也可以有效地降低异常热本底对测试结果的影响。 展开更多
关键词 激光^(40)Ar/^(39)Ar定年 无氧铜样品盘 热本底 脱气 质谱分析
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热电离质谱铀系定年测定过程中需考虑的因素 被引量:4
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作者 张兆峰 彭子成 +2 位作者 贺剑峰 蔡演军 刘桂建 《质谱学报》 EI CAS CSCD 2001年第3期1-7,共7页
岩溶石笋、海洋珊瑚、湖泊沉积物等信息载体可以用热电离质谱 (TIMS)铀系技术定年。在对大量上述信息载体进行定年的基础上 ,作者认为很多因素值得考虑。本文多方面分析了热电离质谱测定过程中需考虑的因素 ,并对这些因素的确认或解决... 岩溶石笋、海洋珊瑚、湖泊沉积物等信息载体可以用热电离质谱 (TIMS)铀系技术定年。在对大量上述信息载体进行定年的基础上 ,作者认为很多因素值得考虑。本文多方面分析了热电离质谱测定过程中需考虑的因素 ,并对这些因素的确认或解决提供对策 ,以期能够提高样品年龄数据的真实可靠性 ,为正确认识过去全球环境变化规律 。 展开更多
关键词 热电离质谱 铀系 测定 定年技术 年代学 第四纪 同位素比值 同位素
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^(40)K-^(40)Ca法的初步研究
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作者 王俊新 彭子成 +2 位作者 刘桂建 房明惠 桂和荣 《核技术》 CAS CSCD 北大核心 2003年第3期197-201,共5页
报道了样品中钾、钙化学分离和纯化,以及质谱测定流程的建立。测试了国家球团矿标样W7220和W7107、国家40K-40Ar法标准矿物黑云母(ZBH-25)和角闪石(ZBJ)的钾钙含量,以及国际二级钙标样Tachiti和国家钾含量标样的钙和钾同位素比值。实测... 报道了样品中钾、钙化学分离和纯化,以及质谱测定流程的建立。测试了国家球团矿标样W7220和W7107、国家40K-40Ar法标准矿物黑云母(ZBH-25)和角闪石(ZBJ)的钾钙含量,以及国际二级钙标样Tachiti和国家钾含量标样的钙和钾同位素比值。实测结果与相应的标称值在误差范围内一致。在此基础上,用实验所得的两组黑云母和角闪石的(40Ca/42Ca) 和 (40K/42Ca)数据,构筑了40K-40Ca法等时线年龄为(133.532.1)Ma, 此与标称值年龄132.7Ma在误差范围内一致。而所得的初始值(40Ca/42Ca)i为151.4160.003, 相应的xCa 值为+26.5,示踪了该矿物组合的原岩具有陆源性质,为固体地球化学的研究提出了新的判据。 展开更多
关键词 质谱 钙40 钾40 放射性同位素 地质年代学 同位素定年 示踪法 地球化学 矿物
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