This study aims to investigate mechanical properties and failure mechanisms of layered rock with rough joint surfaces under direct shear loading.Cubic layered samples with dimensions of 100 mm×100 mm×100 mm ...This study aims to investigate mechanical properties and failure mechanisms of layered rock with rough joint surfaces under direct shear loading.Cubic layered samples with dimensions of 100 mm×100 mm×100 mm were casted using rock-like materials,with anisotropic angle(α)and joint roughness coefficient(JRC)ranging from 15°to 75°and 2-20,respectively.The direct shear tests were conducted under the application of initial normal stress(σ_(n)) ranging from 1-4 MPa.The test results indicate significant differences in mechanical properties,acoustic emission(AE)responses,maximum principal strain fields,and ultimate failure modes of layered samples under different test conditions.The peak stress increases with the increasingαand achieves a maximum value atα=60°or 75°.As σ_(n) increases,the peak stress shows an increasing trend,with correlation coefficients R² ranging from 0.918 to 0.995 for the linear least squares fitting.As JRC increases from 2-4 to 18-20,the cohesion increases by 86.32%whenα=15°,while the cohesion decreases by 27.93%whenα=75°.The differences in roughness characteristics of shear failure surface induced byαresult in anisotropic post-peak AE responses,which is characterized by active AE signals whenαis small and quiet AE signals for a largeα.For a given JRC=6-8 andσ_(n)=1 MPa,asαincreases,the accumulative AE counts increase by 224.31%(αincreased from 15°to 60°),and then decrease by 14.68%(αincreased from 60°to 75°).The shear failure surface is formed along the weak interlayer whenα=15°and penetrates the layered matrix whenα=60°.Whenα=15°,as σ_(n) increases,the adjacent weak interlayer induces a change in the direction of tensile cracks propagation,resulting in a stepped pattern of cracks distribution.The increase in JRC intensifies roughness characteristics of shear failure surface for a smallα,however,it is not pronounced for a largeα.The findings will contribute to a better understanding of the mechanical responses and failure mechanisms of the layered rocks subjected to shear loads.展开更多
The difference in microstructure leads to the diversity of shale mechanical properties and bedding fractures distribution patterns.In this paper,the microstructure and mechanical properties of Longmaxi marine shale an...The difference in microstructure leads to the diversity of shale mechanical properties and bedding fractures distribution patterns.In this paper,the microstructure and mechanical properties of Longmaxi marine shale and Qingshankou continental shale were studied by X-ray diffractometer(XRD),field emission scanning electron microscope(FE-SEM)with mineral analysis system,and nanoindentation.Additionally,the typical bedding layers area was properly stratified using Focused Ion Beam(FIB),and the effects of microstructure and mechanical properties on the distribution patterns of bedding fractures were analyzed.The results show that the Longmaxi marine shale sample contains more clay mineral grains,while the Qingshankou continental shale sample contains more hard brittle mineral grains such as feldspar.For Longmaxi marine shale sample,hard brittle minerals with grain sizes larger than 20μm is18.24%and those with grain sizes smaller than 20μm is 16.22%.For Qingshankou continental shale sample,hard brittle minerals with grain sizes larger than 20μm is 40.7%and those with grain sizes smaller than 20μm is 11.82%.In comparison to the Qingshankou continental shale sample,the Longmaxi marine shale sample has a lower modulus,hardness,and heterogeneity.Laminated shales are formed by alternating coarse-grained and fine-grained layers during deposition.The average single-layer thickness of Longmaxi marine shale sample is greater than Qingshankou continental shale sample.The two types of shale have similar bedding fractures distribution patterns and fractures tend to occur in the transition zone from coarse-grained to fine-grained deposition.The orientation of the fracture is usually parallel to the bedding plane and detour occurs in the presence of hard brittle grains.The fracture distribution density of the Longmaxi marine shale sample is lower than that of the Qingshankou continental shale sample due to the strong heterogeneity of the Qingshankou continental shale.The current research provides guidelines for the effective development of shale reservoirs in various sedimentary environments.展开更多
A high-zinc composite,12vol%SiC/Al-13.3 Zn-3.27 Mg-1.07Cu(wt%),with an ultra-high-strength of 781 MPa was success-fully fabricated through a powder metallurgy method,followed by an extrusion process.The effects of sol...A high-zinc composite,12vol%SiC/Al-13.3 Zn-3.27 Mg-1.07Cu(wt%),with an ultra-high-strength of 781 MPa was success-fully fabricated through a powder metallurgy method,followed by an extrusion process.The effects of solid-solution and aging heat treat-ments on the microstructure and mechanical properties of the composite were extensively investigated.Compared with a single-stage sol-id-solution treatment,a two-stage solid-solution treatment(470℃/1 h+480℃/1 h)exhibited a more effective solid-solution strengthen-ing owing to the higher degree of solid-solution and a more uniform microstructure.According to the aging hardness curves of the com-posite,the optimized aging parameter(100℃/22 h)was determined.Reducing the aging temperature and time resulted in finer and more uniform nanoscale precipitates but only yielded a marginal increase in tensile strength.The fractography analysis revealed that intergranu-lar cracking and interface debonding were the main fracture mechanisms in the ultra-high-strength SiC/Al-Zn-Mg-Cu composites.Weak regions,such as the SiC/Al interface containing numerous compounds and the precipitate-free zones at the high-angle grain boundaries,were identified as significant factors limiting the strength enhancement of the composite.Interfacial compounds,including MgO,MgZn2,and Cu5Zn8,reduced the interfacial bonding strength,leading to interfacial debonding.展开更多
The far-field microdynamic disturbance caused by the excavation of deep mineral resources and underground engineering can induce surrounding rock damage in high-stress conditions and even lead to disasters.However,the...The far-field microdynamic disturbance caused by the excavation of deep mineral resources and underground engineering can induce surrounding rock damage in high-stress conditions and even lead to disasters.However,the mechanical properties and damage/fracture evolution mechanisms of deep rock induced by microdynamic disturbance under three-dimensional stress states are unclear.Therefore,a true triaxial multilevel disturbance test method is proposed,which can completely simulate natural geostress,excavation stress redistribution(such as stress unloading,concentration and rotation),and subsequently the microdynamic disturbance triggering damaged rock failure.Based on a dynamic true triaxial test platform,true triaxial microdynamic disturbance tests under different frequency and amplitudes were carried out on monzogabbro.The results show that increasing amplitude or decreasing frequency diminishes the failure strength of monzogabbro.Deformation modulus gradually decreases during disturbance failure.As frequency and amplitude increase,the degradation rate of deformation modulus decreases slightly,disturbance dissipated energy increases significantly,and disturbance deformation anisotropy strengthens obviously.A damage model has been proposed to quantitatively characterize the disturbance-induced damage evolution at different frequency and amplitude under true triaxial stress.Before disturbance failure,the micro-tensile crack mechanism is dominant,and the micro-shear crack mechanism increases significantly at failure.With the increase of amplitude and frequency,the micro-shear crack mechanism increases.When approaching disturbance failure,the acoustic emission fractal dimension changes from a stable value to local large oscillation,and finally increases sharply to a high value at failure.Finally,the disturbance-induced failure mechanism of surrounding rock in deep engineering is clearly elucidated.展开更多
In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.S...In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.Such defects are identified as crucial contributors to the failure and instability of the surrounding rock,subsequently impacting the engineering stability.The study aimed to investigate the impact of fracture geometry and confining pressure on the deformation,failure characteristics,and strength of specimens using sand powder 3D printing technology and conventional triaxial compression tests.The results indicate that the number of fractures present considerably influences the peak strength,axial peak strain and elastic modulus of the specimens.Confining pressure is an important factor affecting the failure pattern of the specimen,under which the specimen is more prone to shear failure,but the initiation,expansion and penetration processes of secondary cracks in different fracture specimens are different.This study confirmed the feasibility of using sand powder 3D printing specimens as soft rock analogs for triaxial compression research.The insights from this research are deemed essential for a deeper understanding of the mechanical behavior of fractured surrounding rocks when under triaxial stress state.展开更多
In this paper,the effect of the Si content on microstructure evolution,mechanical properties,and fracture behavior of the Al-xSi/AZ91D bimetallic composites prepared by compound casting was investigated systematically...In this paper,the effect of the Si content on microstructure evolution,mechanical properties,and fracture behavior of the Al-xSi/AZ91D bimetallic composites prepared by compound casting was investigated systematically.The obtained results showed that all the Al-xSi/AZ91D bimetallic composites had a metallurgical reaction layer(MRL),whose thickness increased with increasing Si content for the hypoeutectic Al-Si/AZ91D composites,while the hypereutectic Al-Si/AZ91D composites were opposite.The MRL included eutectic layer(E layer),intermetallic compound layer(IMC layer)and transition region layer(T layer).In the IMC layer,the hypereutectic Al-Si/AZ91D composites contained some Si solid solution and flocculent Mg_(2)Si+Al-Mg IMCs phases not presented in the hypoeutectic Al-Si/AZ91D composites.Besides,increasing Si content,the thickness proportion of the T layer increased,forming an inconsistent preferred orientation of the MRL.The shear strengths of the Al-xSi/AZ91D bimetallic composites enhanced with increasing Si content,and the Al-15Si/AZ91D composite obtained a maximum shear strength of 58.6 MPa,which was 73.4% higher than the Al-6Si/AZ91D composite.The fractures of the Al-xSi/AZ91D bimetallic composites transformed from the T layer into the E layer with the increase of the Si content.The improvement of the shear strength of the Al-xSi/AZ91D bimetallic composites was attributed to the synergistic action of the Mg_(2)Si particle reinforcement,the reduction of oxidizing inclusions and the ratio of Al-Mg IMCs as well as the orientation change of the MRL.展开更多
Fracture propagation in shale under in situ conditions is a critical but poorly understood mechanical process in hydraulic fracturing for deep shale gas reservoirs. To address this, hydraulic fracturing experiments we...Fracture propagation in shale under in situ conditions is a critical but poorly understood mechanical process in hydraulic fracturing for deep shale gas reservoirs. To address this, hydraulic fracturing experiments were conducted on hollow double-wing crack specimens of the Longmaxi shale under conditions simulating the ground surface(confining pressure σ_(cp)=0, room temperature(Tr)) and at depths of 1600 m(σ_(cp)=40 MPa, Ti=70 ℃) and 3300 m(σ_(cp)=80 MPa, high temperature Ti=110 ℃) in the study area.High in situ stress was found to significantly increase fracture toughness through constrained microcracking and particle frictional bridging mechanisms. Increasing the temperature enhances rather than weakens the fracture resistance because it increases the grain debonding length, which dissipates more plastic energy and enlarges grains to close microdefects and generate compressive stress to inhibit microcracking. Interestingly, the fracture toughness anisotropy in the shale was found to be nearly constant across burial depths, despite reported variations with increasing confining pressure. Heated water was not found to be as important as the in situ environment in influencing shale fracture. These findings emphasize the need to test the fracture toughness of deep shales under coupled in situ stress and temperature conditions rather than focusing on either in situ stress or temperature alone.展开更多
The effect of W element on the microstructure evolution and mechanical properties of Al_(1.25)CoCrFeNi3 eutectic high-entropy alloy and Al_(1.25)CoCrFeNi_(3-x)W_(x)(x=0,0.05,0.1,0.3,and 0.5;atomic ratio)high-entropy a...The effect of W element on the microstructure evolution and mechanical properties of Al_(1.25)CoCrFeNi3 eutectic high-entropy alloy and Al_(1.25)CoCrFeNi_(3-x)W_(x)(x=0,0.05,0.1,0.3,and 0.5;atomic ratio)high-entropy alloys(HEAs)were explored.Results show that the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs are composed of face-centered cubic and body-centered cubic(BCC)phases.As W content increases,the microstructure changes from eutectic to dendritic.The addition of W lowers the nucleation barrier of the BCC phase,decreases the valence electron concentration of the HEAs,and replaces Al in the BCC phase,thus facilitating the nucleation of the BCC phase.Tensile results show that the addition of W greatly improves the mechanical properties,and solid-solution,heterogeneous-interface,and second-phase strengthening are the main strengthening mechanisms.The yield strength,tensile strength,and elongation of the Al_(1.25)CoCrFeNi2.95W0.05 HEA are 601.44 MPa,1132.26 MPa,and 15.94%,respectively,realizing a balance between strength and plasti-city.The fracture mode of the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs is ductile–brittle mixed fracture,and the crack propagates and initiates in the BCC phase.The eutectic lamellar structure impedes crack propagation and maintains plasticity.展开更多
In order to study and analyze the stability of engineering rock mass under non-uniform triaxial stress and obtain the evolution mechanism of the whole process of fracture,a series of conventional triaxial compression ...In order to study and analyze the stability of engineering rock mass under non-uniform triaxial stress and obtain the evolution mechanism of the whole process of fracture,a series of conventional triaxial compression tests and three-dimensional numerical simulation tests were carried out on hollow granite specimens with different diameters.The bearing capacity of hollow cylindrical specimen is analyzed based on elasticity.The results show that:1)Under low confining pressure,the tensile strain near the hole of the hollow cylindrical specimen is obvious,and the specimen deformation near the hole is significant.At the initial stage of loading,the compressive stress and compressive strain of the specimen are widely distributed.With the progress of loading,the number of microelements subjected to tensile strain gradually increases,and even spreads throughout the specimen;2)Under conventional triaxial compression,the cracking position of hollow cylinder specimens is concentrated in the upper and lower parts,and the final fracture mode is generally compressive shear failure.The final fracture mode of complete specimen is generally tensile fracture.Under high confining pressure,the tensile cracks of the sample are concentrated in the upper and lower parts and are not connected,while the cracks of the upper and lower parts of the intact sample will expand and connect to form a fracture surface;3)In addition,the tensile crack widths of intact and hollow cylindrical specimens under low confining pressure are larger than those under high confining pressure.展开更多
Sandstone is the fundamental material in various engineering and construction projects.However,the mechanical integrity of sandstone can be compromised by initial unloading damage resulting from activities such as eng...Sandstone is the fundamental material in various engineering and construction projects.However,the mechanical integrity of sandstone can be compromised by initial unloading damage resulting from activities such as engineering excavations.Furthermore,this degradation is further exacerbated under periodic dry-wet environmental conditions.This study investigated the effects of dry-wet cycles and unloading on the mechanical properties of jointed fine sandstone using uniaxial and triaxial compression tests.These tests were performed on rock samples subjected to varying unloading degrees and different numbers of dry-wet cycles.The results demonstrate that with an increase in the unloading degree from 0%to 70%,there is a corresponding decrease in peak stress ranging from 10%to 33%.Additionally,the cohesion exhibits a reduction of approximately 20%to 25%,while the internal friction angle experiences a decline of about 3.5%to 6%.These findings emphasize a significant unloading effect.Moreover,the degree of peak stress degradation in unloading jointed fine sandstone diminishes with an increase in confining pressure,suggesting that confining pressure mitigates the deterioration caused by dry-wet cycles.Additionally,as the number of dry-wet cycles increases,there is a notable decline in the mechanical properties of the sandstone,evidencing significant dry-wet degradation.Utilizing the Drucker Prager criterion,this study establishes a strength criterion and fracture criterion,denoted as σ_(1)(m,n) and K_(T)^(Ⅱ)(m, n), to quantify the combined impacts of dry-wet cycles and unloading on jointed fine sandstone,which provides a comprehensive understanding of its mechanical behavior under such conditions.展开更多
Liquid nitrogen has shown excellent performances as a good fracturing medium in the extraction of unconventional natural gas,and its application in coalbed methane extraction is currently a research hotspot.This study...Liquid nitrogen has shown excellent performances as a good fracturing medium in the extraction of unconventional natural gas,and its application in coalbed methane extraction is currently a research hotspot.This study focuses on the acoustic emission properties of coal specimens treated utilizing liquid nitrogen with varying initial temperatures in a three-point bending environment.Through examination of the load-displacement curves of the considered coal samples,their mechanical properties are also revealed for different initial temperatures and cycling frequencies.The findings demonstrate a gradual decline in the maximum load capacity of coal rock as the temperature rises.Similarly,when subjected to the same temperature,an escalation in the cycling frequency leads to a reduction in the peak load of coal rock.This suggests that both temperature and cycling frequency exert a notable impact on the fracturing efficacy of liquid nitrogen.Freeze-thaw cycling treatments and exposure to high-temperature conditions can activate preexisting damage in the coal rock,and,accordingly,influence its mechanical properties.In particular,throughout the progressive loading of coal rock samples,the failure mechanisms are predominantly characterized by the occurrence of tensile cracks,succeeded by the development,spread,and fracture of shear fissures.展开更多
Based on the actual data collected from the tight sandstone development zone, correlation analysis using theSpearman method was conducted to determine the main factors influencing the gas production rate of tightsands...Based on the actual data collected from the tight sandstone development zone, correlation analysis using theSpearman method was conducted to determine the main factors influencing the gas production rate of tightsandstone fracturing. An integrated model combining geological engineering and numerical simulation of fracturepropagation and production was completed. Based on data analysis, the hydraulic fracture parameters wereoptimized to develop a differentiated fracturing treatment adjustment plan. The results indicate that the influenceof geological and engineering factors in the X1 and X2 development zones in the study area differs significantly.Therefore, it is challenging to adopt a uniform development strategy to achieve rapid production increase. Thedata analysis reveals that the variation in gas production rate is primarily affected by the reservoir thickness andpermeability parameters as geological factors. On the other hand, the amount of treatment fluid and proppantaddition significantly impact the gas production rate as engineering factors. Among these factors, the influence ofgeological factors is more pronounced in block X1. Therefore, the main focus should be on further optimizing thefracturing interval and adjusting the geological development well location. Given the existing well location, thereis limited potential for further optimizing fracture parameters to increase production. For block X2, the fracturingparameters should be optimized. Data screening was conducted to identify outliers in the entire dataset, and adata-driven fracturing parameter optimization method was employed to determine the basic adjustment directionfor reservoir stimulation in the target block. This approach provides insights into the influence of geological,stimulation, and completion parameters on gas production rate. Consequently, the subsequent fracturing parameteroptimization design can significantly reduce the modeling and simulation workload and guide field operations toimprove and optimize hydraulic fracturing efficiency.展开更多
The microscopic characteristics and mechanical properties of rocks change after the action of acid on deep shale,which affects the fracturing effect.Accordingly,we designed and conducted indoor experiments related to ...The microscopic characteristics and mechanical properties of rocks change after the action of acid on deep shale,which affects the fracturing effect.Accordingly,we designed and conducted indoor experiments related to the changes in macro and microscopic characteristics after the interaction of acid with the shale of Wujiaping Formation,based on which the characteristic law of fracture volume modification after acid fracturing was studied using numerical simulation.The results demonstrate that the pores and fractures are enlarged and the structure is significantly loosened after the acid immersion.And a 15%concentration of hydrochloric acid can effectively dissolve shale.Furthermore,the degree of acid-etching reaction is highly variable because of the different carbonate content,which reveals the strong inhomogeneity of the shale system in the Wujiaping Group reservoir section.After the acid interacted with the shale rock samples,the triaxial compressive strength,elastic modulus,and Poisson’s ratio of shale decreased.Moreover,the evaluation of the effect after acid fracturing simulated by fracturing software revealed that the smaller the value of elastic modulus in shale-based reservoirs,the more favorable the fracture volume modification.This discovery not only provides a theoretical basis for the expansion and extension patterns of acid-fracturing in carbonaceous shale formations but also offers research methods and theoretical insights for the fundamental exploration of other deep-seated oil and gas resources.展开更多
Under the policy background and advocacy of carbon capture,utilization,and storage(CCUS),CO_(2)-EOR has become a promising direction in the shale oil reservoir industry.The multi-scale pore structure distribution and ...Under the policy background and advocacy of carbon capture,utilization,and storage(CCUS),CO_(2)-EOR has become a promising direction in the shale oil reservoir industry.The multi-scale pore structure distribution and fracture structure lead to complex multiphase flow,comprehensively considering multiple mechanisms is crucial for development and CO_(2) storage in fractured shale reservoirs.In this paper,a multi-mechanism coupled model is developed by MATLAB.Compared to the traditional Eclipse300 and MATLAB Reservoir Simulation Toolbox(MRST),this model considers the impact of pore structure on fluid phase behavior by the modified Peng—Robinson equation of state(PR-EOS),and the effect simultaneously radiate to Maxwell—Stefan(M—S)diffusion,stress sensitivity,the nano-confinement(NC)effect.Moreover,a modified embedded discrete fracture model(EDFM)is used to model the complex fractures,which optimizes connection types and half-transmissibility calculation approaches between non-neighboring connections(NNCs).The full implicit equation adopts the finite volume method(FVM)and Newton—Raphson iteration for discretization and solution.The model verification with the Eclipse300 and MRST is satisfactory.The results show that the interaction between the mechanisms significantly affects the production performance and storage characteristics.The effect of molecular diffusion may be overestimated in oil-dominated(liquid-dominated)shale reservoirs.The well spacing and injection gas rate are the most crucial factors affecting the production by sensitivity analysis.Moreover,the potential gas invasion risk is mentioned.This model provides a reliable theoretical basis for CO_(2)-EOR and sequestration in shale oil reservoirs.展开更多
Reef limestone is a biogenic sedimentary rock widely distributed in coral reef areas, acting as an important foundation for coast construction. Due to its special biogenic origin, reef limestone is different from conv...Reef limestone is a biogenic sedimentary rock widely distributed in coral reef areas, acting as an important foundation for coast construction. Due to its special biogenic origin, reef limestone is different from conventional rocks both in terms of rock structure and mechanical properties. In this study, mesoscale uniaxial compression experiments with five different loading directions were conducted on two kinds of reef limestones from the Maldives Islands and the South China Sea, respectively. The real-time high-resolution videos and images of failure processes were recorded simultaneously to investigate the fracture evolution and fracture surface roughness of reef limestones. It demonstrated that the reef limestones belonged to extremely soft to soft rocks, and their uniaxial compressive strength (UCS) values fluctuated with high discreteness. The mesoscale mechanical properties of reef limestones were highly anisotropic and mainly controlled by pore structure. The occurrence of dissolution pores in reef limestone tended to intensify mechanical anisotropy. With the integration of the fracture initiation and propagation features of reef limestones, it is supposed that the intrinsic mechanism of anisotropy was probably attributed to the differences in coral growth direction and dissolution. Furthermore, the quantified fracture surface roughness was revealed to have a good consistency with density and UCS for the reef limestones from the South China Sea. The findings are helpful for providing theoretical and experimental references for engineering construction in coral reef areas.展开更多
Magnesium alloys,a novel functional material for the fabrication of fracturing tools,are being paid more and more attentions recently due to their relatively high mechanical properties and fast dissolubility ability a...Magnesium alloys,a novel functional material for the fabrication of fracturing tools,are being paid more and more attentions recently due to their relatively high mechanical properties and fast dissolubility ability after fracturing.In this study,the novel extruded Mg-10Gd-3Y-0.3Zr-xNi alloys will be reported and their microstructure,mechanical and corrosion behaviors will be also studied.The results show that Ni contents influence phase precipitation behaviors.With adding 0.2 wt%Ni,a large amount of Zr_(7)Ni_(10)phases will be precipitated insidesα-Mg matrix,directly leading to degradation of strength and large corrosion rate.With further increasing Ni contents,the precipitation phases can be changed from Mg_(5)RE to 18R-LPSO structure,resulting in higher mechanical properties and faster corrosion rate.Moreover,adding Ni element also change the texture orientation by influencing the precipitation behavior of the alloys.The alloys invented in this paper have attained the highest compressive and tensile properties among all the reported dissoluble magnesium alloys.This work is beneficial in understanding the role of Ni in the magnesium alloys and provides more materials alternatives for the fabrication of dissoluble fracturing tools.展开更多
In this work,as-cast Mg-Ni-Y alloys were proposed to develop a feasible material for fracturing balls,and their mechanical performance and corrosion behavior were systematically investigated.Long period stacking order...In this work,as-cast Mg-Ni-Y alloys were proposed to develop a feasible material for fracturing balls,and their mechanical performance and corrosion behavior were systematically investigated.Long period stacking order(LPSO)phase was firstly introduced to improve both the mechanical properties and degradation rate of magnesium alloys.With the increase of LPSO phase,the compressive strength was improved significantly,while the elongation of the alloys decreased owing to the relatively brittle nature of LPSO phase.Due to the higher corrosion potential of LPSO phase,the LPSO phase can accelerate the corrosion process by providing more micro-couples.However,the LPSO phase would serve as the corrosion barrier between the corrosion medium and the matrix when the contents of LPSO phase are too high in Mg92.5Ni3Y4.5 and Mg87.5Ni5Y7.5 alloys.As-cast Mg97.5Ni1Y1.5 alloy with satisfactory mechanical properties and rapid degradation rate was successfully developed,exhibiting a high degradation rate of 6675 mm/a(93℃)in 3 wt.%KCl solution and a favorable ultimate compressive strength of 410 MPa.The degradation rate of Mg97.5Ni1Y1.5 alloy is 2-5 times of the current commercial magnesium alloy fracturing materials.展开更多
The premise of hydraulic fracturing is to have an accurate and detailed understanding of the rock mechanical properties and fracture propagation law of shale reservoirs. In this paper,a comprehensive evaluation of the...The premise of hydraulic fracturing is to have an accurate and detailed understanding of the rock mechanical properties and fracture propagation law of shale reservoirs. In this paper,a comprehensive evaluation of the mechanical properties of the shale oil reservoir in the south of Songliao Basin is carried out. Based on the experiments and the in-situ stress analysis, the fracture propagation law of three types of shale reservoirs is obtained,and the suggestions for fracturing are put forward. The results have shown that the fracture propagation of pure shale and low mature reservoir is easy to open along the bedding plane under compression loading,which is greatly influenced by the bedding. Sand-bearing shale is slightly better,the fractures of which are not easy to open along the bedding plane. The mechanical experimental results show that all the samples have the characteristics of low compressive strength,low Young’s modulus and strong anisotropy,indicating that the shale oil reservoir is certain plastic,which is related to its high clay mineral content and controlled by the bedding development. Compared with pure shale and low mature shale,the sandbearing shale has less clay content and less developed bedding,which maybe the main reason for its slightly better brittleness. Overall,the expansion of hydraulic fracture is controlled by in-situ stress and bedding. Because of the development of bedding,it is easy to form horizontal fractures. Thus it is not suitable for horizontal well fracturing.Because of the high content of clay minerals,the applicability of conventional slick hydraulic fracturing fluid is poor. It is suggested to use vertical well or directional well to carry out volume fracturing. In this way,the effect of bedding can be effectively used to open and connect the bedding and form a larger fracture network.展开更多
The influence of rock mechanical properties on the electromagnetic radiation(EMR)mechanism of rock fracturing is an important research topic in solid mechanics and earthquake prediction.In this study,an EMR model of r...The influence of rock mechanical properties on the electromagnetic radiation(EMR)mechanism of rock fracturing is an important research topic in solid mechanics and earthquake prediction.In this study,an EMR model of rock fracturing considering the fracture factor,elastic modulus,Poisson’s ratio,radiation distance and crack length is derived based on the Hertz oscillator array assumption.An experimental system,including an electromagnetic shielding module,an EMR signal induction and transmission module,a signal recording module and a loading module,is developed to understand the EMR characteristics of four different rocks.The validity of the EMR theoretical model is verified and the relationships between the rock cracking morphology and the EMR waveform,amplitude and frequency are revealed.It is found that rock mechanical properties have obvious influences on the EMR waveform,amplitude and frequency during rock fracturing.This study provides a better understanding on the EMR mechanism of rock fracturing and can help to improve the accuracy of rock disaster prediction based on EMR.展开更多
Based on the elastoplastic model of cement sheath considering the influence of three-dimensional principal stress and the stress field model of interface crack,a mechanical performance design method of cement sheath i...Based on the elastoplastic model of cement sheath considering the influence of three-dimensional principal stress and the stress field model of interface crack,a mechanical performance design method of cement sheath is established to meet the wellbore sealing requirements during fracturing.This method takes the failure types of the cement sheath,such as tensile failure,plastic yield,interface crack propagation along interface and zigzag propagation into account.Meanwhile,the elasticity modulus and Poisson's ratio quantitative design charts of cement sheath are constructed based on this method,and the safety and risk areas of wellbores are defined,which quantify the yield strength and tensile strength indexes of cement sheath.The results show that decreasing elasticity modulus,increasing yield strength and Poisson's ratio of cement sheath can avoid plastic deformation of cement sheath;increasing the tensile strength of cement sheath can prevent its tensile failure;increasing elasticity modulus and Poisson's ratio of cement sheath is good for shortening the length of the interface crack,but will increase the risk of interface cracks zigzagging into cement sheath.The model calculation and case verification has proved that the method in this paper can give accurate calculation results and is convenient for field application.展开更多
基金financial support from the National Natural Science Foundation of China(Nos.52174092,51904290,52004272,52104125,42372328,and U23B2091)Natural Science Foundation of Jiangsu Province,China(Nos.BK20220157 and BK20240209)+3 种基金the Fundamental Research Funds for the Central Universities,China(No.2022YCPY0202)Xuzhou Science and Technology Project,China(Nos.KC21033 and KC22005)Yunlong Lake Laboratory of Deep Underground Science and Engineering Project,China(No.104023002)the Graduate Innovation Program of China University of Mining and Technology(No.2023WLTCRCZL052)。
文摘This study aims to investigate mechanical properties and failure mechanisms of layered rock with rough joint surfaces under direct shear loading.Cubic layered samples with dimensions of 100 mm×100 mm×100 mm were casted using rock-like materials,with anisotropic angle(α)and joint roughness coefficient(JRC)ranging from 15°to 75°and 2-20,respectively.The direct shear tests were conducted under the application of initial normal stress(σ_(n)) ranging from 1-4 MPa.The test results indicate significant differences in mechanical properties,acoustic emission(AE)responses,maximum principal strain fields,and ultimate failure modes of layered samples under different test conditions.The peak stress increases with the increasingαand achieves a maximum value atα=60°or 75°.As σ_(n) increases,the peak stress shows an increasing trend,with correlation coefficients R² ranging from 0.918 to 0.995 for the linear least squares fitting.As JRC increases from 2-4 to 18-20,the cohesion increases by 86.32%whenα=15°,while the cohesion decreases by 27.93%whenα=75°.The differences in roughness characteristics of shear failure surface induced byαresult in anisotropic post-peak AE responses,which is characterized by active AE signals whenαis small and quiet AE signals for a largeα.For a given JRC=6-8 andσ_(n)=1 MPa,asαincreases,the accumulative AE counts increase by 224.31%(αincreased from 15°to 60°),and then decrease by 14.68%(αincreased from 60°to 75°).The shear failure surface is formed along the weak interlayer whenα=15°and penetrates the layered matrix whenα=60°.Whenα=15°,as σ_(n) increases,the adjacent weak interlayer induces a change in the direction of tensile cracks propagation,resulting in a stepped pattern of cracks distribution.The increase in JRC intensifies roughness characteristics of shear failure surface for a smallα,however,it is not pronounced for a largeα.The findings will contribute to a better understanding of the mechanical responses and failure mechanisms of the layered rocks subjected to shear loads.
基金financially supported by the National Natural Science Foundation of China(Grant Nos.52074315&U19B6003)。
文摘The difference in microstructure leads to the diversity of shale mechanical properties and bedding fractures distribution patterns.In this paper,the microstructure and mechanical properties of Longmaxi marine shale and Qingshankou continental shale were studied by X-ray diffractometer(XRD),field emission scanning electron microscope(FE-SEM)with mineral analysis system,and nanoindentation.Additionally,the typical bedding layers area was properly stratified using Focused Ion Beam(FIB),and the effects of microstructure and mechanical properties on the distribution patterns of bedding fractures were analyzed.The results show that the Longmaxi marine shale sample contains more clay mineral grains,while the Qingshankou continental shale sample contains more hard brittle mineral grains such as feldspar.For Longmaxi marine shale sample,hard brittle minerals with grain sizes larger than 20μm is18.24%and those with grain sizes smaller than 20μm is 16.22%.For Qingshankou continental shale sample,hard brittle minerals with grain sizes larger than 20μm is 40.7%and those with grain sizes smaller than 20μm is 11.82%.In comparison to the Qingshankou continental shale sample,the Longmaxi marine shale sample has a lower modulus,hardness,and heterogeneity.Laminated shales are formed by alternating coarse-grained and fine-grained layers during deposition.The average single-layer thickness of Longmaxi marine shale sample is greater than Qingshankou continental shale sample.The two types of shale have similar bedding fractures distribution patterns and fractures tend to occur in the transition zone from coarse-grained to fine-grained deposition.The orientation of the fracture is usually parallel to the bedding plane and detour occurs in the presence of hard brittle grains.The fracture distribution density of the Longmaxi marine shale sample is lower than that of the Qingshankou continental shale sample due to the strong heterogeneity of the Qingshankou continental shale.The current research provides guidelines for the effective development of shale reservoirs in various sedimentary environments.
基金supported by the National Key Research and Development Program of China(No.2022YFB3707405)the Guangdong Basic and Applied Basic Research Foundation,China(No.2021A1515110525)+1 种基金the National Natural Science Foundation of China(Nos.U22A20114 and 52301200)the Liaoning Revitalization Talents Program,China(No.XLYC2007009)。
文摘A high-zinc composite,12vol%SiC/Al-13.3 Zn-3.27 Mg-1.07Cu(wt%),with an ultra-high-strength of 781 MPa was success-fully fabricated through a powder metallurgy method,followed by an extrusion process.The effects of solid-solution and aging heat treat-ments on the microstructure and mechanical properties of the composite were extensively investigated.Compared with a single-stage sol-id-solution treatment,a two-stage solid-solution treatment(470℃/1 h+480℃/1 h)exhibited a more effective solid-solution strengthen-ing owing to the higher degree of solid-solution and a more uniform microstructure.According to the aging hardness curves of the com-posite,the optimized aging parameter(100℃/22 h)was determined.Reducing the aging temperature and time resulted in finer and more uniform nanoscale precipitates but only yielded a marginal increase in tensile strength.The fractography analysis revealed that intergranu-lar cracking and interface debonding were the main fracture mechanisms in the ultra-high-strength SiC/Al-Zn-Mg-Cu composites.Weak regions,such as the SiC/Al interface containing numerous compounds and the precipitate-free zones at the high-angle grain boundaries,were identified as significant factors limiting the strength enhancement of the composite.Interfacial compounds,including MgO,MgZn2,and Cu5Zn8,reduced the interfacial bonding strength,leading to interfacial debonding.
基金the financial support from the National Natural Science Foundation of China(No.52109119)the Guangxi Natural Science Foundation(No.2021GXNSFBA075030)+2 种基金the Guangxi Science and Technology Project(No.Guike AD20325002)the Chinese Postdoctoral Science Fund Project(No.2022M723408)the Open Research Fund of State Key Laboratory of Simulation and Regulation of Water Cycle in River Basin(China Institute of Water Resources and Hydropower Research)(No.IWHR-SKL-202202)。
文摘The far-field microdynamic disturbance caused by the excavation of deep mineral resources and underground engineering can induce surrounding rock damage in high-stress conditions and even lead to disasters.However,the mechanical properties and damage/fracture evolution mechanisms of deep rock induced by microdynamic disturbance under three-dimensional stress states are unclear.Therefore,a true triaxial multilevel disturbance test method is proposed,which can completely simulate natural geostress,excavation stress redistribution(such as stress unloading,concentration and rotation),and subsequently the microdynamic disturbance triggering damaged rock failure.Based on a dynamic true triaxial test platform,true triaxial microdynamic disturbance tests under different frequency and amplitudes were carried out on monzogabbro.The results show that increasing amplitude or decreasing frequency diminishes the failure strength of monzogabbro.Deformation modulus gradually decreases during disturbance failure.As frequency and amplitude increase,the degradation rate of deformation modulus decreases slightly,disturbance dissipated energy increases significantly,and disturbance deformation anisotropy strengthens obviously.A damage model has been proposed to quantitatively characterize the disturbance-induced damage evolution at different frequency and amplitude under true triaxial stress.Before disturbance failure,the micro-tensile crack mechanism is dominant,and the micro-shear crack mechanism increases significantly at failure.With the increase of amplitude and frequency,the micro-shear crack mechanism increases.When approaching disturbance failure,the acoustic emission fractal dimension changes from a stable value to local large oscillation,and finally increases sharply to a high value at failure.Finally,the disturbance-induced failure mechanism of surrounding rock in deep engineering is clearly elucidated.
基金Project(2021YFC2900600)supported by the Young Scientist Project of National Key Research and Development Program of ChinaProject(52074166)supported by the National Natural Science Foundation of China+1 种基金Projects(ZR2021YQ38,ZR2020QE121)supported by the Natural Science Foundation of Shandong Province,ChinaProject(2022KJ101)supported by the Science and Technology Support Plan for Youth Innovation of Colleges and Universities in Shandong Province,China。
文摘In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.Such defects are identified as crucial contributors to the failure and instability of the surrounding rock,subsequently impacting the engineering stability.The study aimed to investigate the impact of fracture geometry and confining pressure on the deformation,failure characteristics,and strength of specimens using sand powder 3D printing technology and conventional triaxial compression tests.The results indicate that the number of fractures present considerably influences the peak strength,axial peak strain and elastic modulus of the specimens.Confining pressure is an important factor affecting the failure pattern of the specimen,under which the specimen is more prone to shear failure,but the initiation,expansion and penetration processes of secondary cracks in different fracture specimens are different.This study confirmed the feasibility of using sand powder 3D printing specimens as soft rock analogs for triaxial compression research.The insights from this research are deemed essential for a deeper understanding of the mechanical behavior of fractured surrounding rocks when under triaxial stress state.
基金the supports provided by the National Natural Science Foundation of China(Nos.52075198 and 52271102)the China Postdoctoral Science Foundation(No.2021M691112)+1 种基金the State Key Lab of Advanced Metals and Materials(No.2021-ZD07)the Analytical and Testing Center,HUST。
文摘In this paper,the effect of the Si content on microstructure evolution,mechanical properties,and fracture behavior of the Al-xSi/AZ91D bimetallic composites prepared by compound casting was investigated systematically.The obtained results showed that all the Al-xSi/AZ91D bimetallic composites had a metallurgical reaction layer(MRL),whose thickness increased with increasing Si content for the hypoeutectic Al-Si/AZ91D composites,while the hypereutectic Al-Si/AZ91D composites were opposite.The MRL included eutectic layer(E layer),intermetallic compound layer(IMC layer)and transition region layer(T layer).In the IMC layer,the hypereutectic Al-Si/AZ91D composites contained some Si solid solution and flocculent Mg_(2)Si+Al-Mg IMCs phases not presented in the hypoeutectic Al-Si/AZ91D composites.Besides,increasing Si content,the thickness proportion of the T layer increased,forming an inconsistent preferred orientation of the MRL.The shear strengths of the Al-xSi/AZ91D bimetallic composites enhanced with increasing Si content,and the Al-15Si/AZ91D composite obtained a maximum shear strength of 58.6 MPa,which was 73.4% higher than the Al-6Si/AZ91D composite.The fractures of the Al-xSi/AZ91D bimetallic composites transformed from the T layer into the E layer with the increase of the Si content.The improvement of the shear strength of the Al-xSi/AZ91D bimetallic composites was attributed to the synergistic action of the Mg_(2)Si particle reinforcement,the reduction of oxidizing inclusions and the ratio of Al-Mg IMCs as well as the orientation change of the MRL.
基金supported by the National Natural Science Foundation of China(No.12172240).
文摘Fracture propagation in shale under in situ conditions is a critical but poorly understood mechanical process in hydraulic fracturing for deep shale gas reservoirs. To address this, hydraulic fracturing experiments were conducted on hollow double-wing crack specimens of the Longmaxi shale under conditions simulating the ground surface(confining pressure σ_(cp)=0, room temperature(Tr)) and at depths of 1600 m(σ_(cp)=40 MPa, Ti=70 ℃) and 3300 m(σ_(cp)=80 MPa, high temperature Ti=110 ℃) in the study area.High in situ stress was found to significantly increase fracture toughness through constrained microcracking and particle frictional bridging mechanisms. Increasing the temperature enhances rather than weakens the fracture resistance because it increases the grain debonding length, which dissipates more plastic energy and enlarges grains to close microdefects and generate compressive stress to inhibit microcracking. Interestingly, the fracture toughness anisotropy in the shale was found to be nearly constant across burial depths, despite reported variations with increasing confining pressure. Heated water was not found to be as important as the in situ environment in influencing shale fracture. These findings emphasize the need to test the fracture toughness of deep shales under coupled in situ stress and temperature conditions rather than focusing on either in situ stress or temperature alone.
基金supported by the National Natural Science Foundation of China(No.51825401)the China Postdoctoral Science Foundation(No.2023TO0099)the Interdisciplinary Research Foundation of Harbin Institute of Technology.
文摘The effect of W element on the microstructure evolution and mechanical properties of Al_(1.25)CoCrFeNi3 eutectic high-entropy alloy and Al_(1.25)CoCrFeNi_(3-x)W_(x)(x=0,0.05,0.1,0.3,and 0.5;atomic ratio)high-entropy alloys(HEAs)were explored.Results show that the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs are composed of face-centered cubic and body-centered cubic(BCC)phases.As W content increases,the microstructure changes from eutectic to dendritic.The addition of W lowers the nucleation barrier of the BCC phase,decreases the valence electron concentration of the HEAs,and replaces Al in the BCC phase,thus facilitating the nucleation of the BCC phase.Tensile results show that the addition of W greatly improves the mechanical properties,and solid-solution,heterogeneous-interface,and second-phase strengthening are the main strengthening mechanisms.The yield strength,tensile strength,and elongation of the Al_(1.25)CoCrFeNi2.95W0.05 HEA are 601.44 MPa,1132.26 MPa,and 15.94%,respectively,realizing a balance between strength and plasti-city.The fracture mode of the Al_(1.25)CoCrFeNi_(3-x)W_(x) HEAs is ductile–brittle mixed fracture,and the crack propagates and initiates in the BCC phase.The eutectic lamellar structure impedes crack propagation and maintains plasticity.
基金Projects(52074116,51804113)supported by the National Natural Science Foundation of China。
文摘In order to study and analyze the stability of engineering rock mass under non-uniform triaxial stress and obtain the evolution mechanism of the whole process of fracture,a series of conventional triaxial compression tests and three-dimensional numerical simulation tests were carried out on hollow granite specimens with different diameters.The bearing capacity of hollow cylindrical specimen is analyzed based on elasticity.The results show that:1)Under low confining pressure,the tensile strain near the hole of the hollow cylindrical specimen is obvious,and the specimen deformation near the hole is significant.At the initial stage of loading,the compressive stress and compressive strain of the specimen are widely distributed.With the progress of loading,the number of microelements subjected to tensile strain gradually increases,and even spreads throughout the specimen;2)Under conventional triaxial compression,the cracking position of hollow cylinder specimens is concentrated in the upper and lower parts,and the final fracture mode is generally compressive shear failure.The final fracture mode of complete specimen is generally tensile fracture.Under high confining pressure,the tensile cracks of the sample are concentrated in the upper and lower parts and are not connected,while the cracks of the upper and lower parts of the intact sample will expand and connect to form a fracture surface;3)In addition,the tensile crack widths of intact and hollow cylindrical specimens under low confining pressure are larger than those under high confining pressure.
基金financially supported by the National Natural Science Foundation of China(42177166).
文摘Sandstone is the fundamental material in various engineering and construction projects.However,the mechanical integrity of sandstone can be compromised by initial unloading damage resulting from activities such as engineering excavations.Furthermore,this degradation is further exacerbated under periodic dry-wet environmental conditions.This study investigated the effects of dry-wet cycles and unloading on the mechanical properties of jointed fine sandstone using uniaxial and triaxial compression tests.These tests were performed on rock samples subjected to varying unloading degrees and different numbers of dry-wet cycles.The results demonstrate that with an increase in the unloading degree from 0%to 70%,there is a corresponding decrease in peak stress ranging from 10%to 33%.Additionally,the cohesion exhibits a reduction of approximately 20%to 25%,while the internal friction angle experiences a decline of about 3.5%to 6%.These findings emphasize a significant unloading effect.Moreover,the degree of peak stress degradation in unloading jointed fine sandstone diminishes with an increase in confining pressure,suggesting that confining pressure mitigates the deterioration caused by dry-wet cycles.Additionally,as the number of dry-wet cycles increases,there is a notable decline in the mechanical properties of the sandstone,evidencing significant dry-wet degradation.Utilizing the Drucker Prager criterion,this study establishes a strength criterion and fracture criterion,denoted as σ_(1)(m,n) and K_(T)^(Ⅱ)(m, n), to quantify the combined impacts of dry-wet cycles and unloading on jointed fine sandstone,which provides a comprehensive understanding of its mechanical behavior under such conditions.
基金the National Natural Science Foundation(52004285)Fundamental Research Funds for the Central Universities from China University of Mining and Technology-Beijing(JCCXXNY06)the Open Fund of State Key Laboratory Cultivation Base for Gas Geology and Gas Control(Henan Polytechnic University)(WS2021A03).
文摘Liquid nitrogen has shown excellent performances as a good fracturing medium in the extraction of unconventional natural gas,and its application in coalbed methane extraction is currently a research hotspot.This study focuses on the acoustic emission properties of coal specimens treated utilizing liquid nitrogen with varying initial temperatures in a three-point bending environment.Through examination of the load-displacement curves of the considered coal samples,their mechanical properties are also revealed for different initial temperatures and cycling frequencies.The findings demonstrate a gradual decline in the maximum load capacity of coal rock as the temperature rises.Similarly,when subjected to the same temperature,an escalation in the cycling frequency leads to a reduction in the peak load of coal rock.This suggests that both temperature and cycling frequency exert a notable impact on the fracturing efficacy of liquid nitrogen.Freeze-thaw cycling treatments and exposure to high-temperature conditions can activate preexisting damage in the coal rock,and,accordingly,influence its mechanical properties.In particular,throughout the progressive loading of coal rock samples,the failure mechanisms are predominantly characterized by the occurrence of tensile cracks,succeeded by the development,spread,and fracture of shear fissures.
基金Research and Application of Key Technologies for Tight Gas Production Improvement and Rehabilitation of Linxing Shenfu(YXKY-ZL-01-2021)。
文摘Based on the actual data collected from the tight sandstone development zone, correlation analysis using theSpearman method was conducted to determine the main factors influencing the gas production rate of tightsandstone fracturing. An integrated model combining geological engineering and numerical simulation of fracturepropagation and production was completed. Based on data analysis, the hydraulic fracture parameters wereoptimized to develop a differentiated fracturing treatment adjustment plan. The results indicate that the influenceof geological and engineering factors in the X1 and X2 development zones in the study area differs significantly.Therefore, it is challenging to adopt a uniform development strategy to achieve rapid production increase. Thedata analysis reveals that the variation in gas production rate is primarily affected by the reservoir thickness andpermeability parameters as geological factors. On the other hand, the amount of treatment fluid and proppantaddition significantly impact the gas production rate as engineering factors. Among these factors, the influence ofgeological factors is more pronounced in block X1. Therefore, the main focus should be on further optimizing thefracturing interval and adjusting the geological development well location. Given the existing well location, thereis limited potential for further optimizing fracture parameters to increase production. For block X2, the fracturingparameters should be optimized. Data screening was conducted to identify outliers in the entire dataset, and adata-driven fracturing parameter optimization method was employed to determine the basic adjustment directionfor reservoir stimulation in the target block. This approach provides insights into the influence of geological,stimulation, and completion parameters on gas production rate. Consequently, the subsequent fracturing parameteroptimization design can significantly reduce the modeling and simulation workload and guide field operations toimprove and optimize hydraulic fracturing efficiency.
基金This study is supported by a Scientific Research Project of Sinopec(Program No.P21087-2)the Open Fund of Key Laboratory of Marine Oil&Gas Reservoirs Production,Sinopec(Grant No.33550000-22-FW2099-0004).
文摘The microscopic characteristics and mechanical properties of rocks change after the action of acid on deep shale,which affects the fracturing effect.Accordingly,we designed and conducted indoor experiments related to the changes in macro and microscopic characteristics after the interaction of acid with the shale of Wujiaping Formation,based on which the characteristic law of fracture volume modification after acid fracturing was studied using numerical simulation.The results demonstrate that the pores and fractures are enlarged and the structure is significantly loosened after the acid immersion.And a 15%concentration of hydrochloric acid can effectively dissolve shale.Furthermore,the degree of acid-etching reaction is highly variable because of the different carbonate content,which reveals the strong inhomogeneity of the shale system in the Wujiaping Group reservoir section.After the acid interacted with the shale rock samples,the triaxial compressive strength,elastic modulus,and Poisson’s ratio of shale decreased.Moreover,the evaluation of the effect after acid fracturing simulated by fracturing software revealed that the smaller the value of elastic modulus in shale-based reservoirs,the more favorable the fracture volume modification.This discovery not only provides a theoretical basis for the expansion and extension patterns of acid-fracturing in carbonaceous shale formations but also offers research methods and theoretical insights for the fundamental exploration of other deep-seated oil and gas resources.
基金supported by the National Natural Science Foundation of China(No.52174038 and No.52004307)China Petroleum Science and Technology Project-Major Project-Research on Tight Oil-Shale Oil Reservoir Engineering Methods and Key Technologies in Ordos Basin(No.ZLZX2020-02-04)Science Foundation of China University of Petroleum,Beijing(No.2462018YJRC015)。
文摘Under the policy background and advocacy of carbon capture,utilization,and storage(CCUS),CO_(2)-EOR has become a promising direction in the shale oil reservoir industry.The multi-scale pore structure distribution and fracture structure lead to complex multiphase flow,comprehensively considering multiple mechanisms is crucial for development and CO_(2) storage in fractured shale reservoirs.In this paper,a multi-mechanism coupled model is developed by MATLAB.Compared to the traditional Eclipse300 and MATLAB Reservoir Simulation Toolbox(MRST),this model considers the impact of pore structure on fluid phase behavior by the modified Peng—Robinson equation of state(PR-EOS),and the effect simultaneously radiate to Maxwell—Stefan(M—S)diffusion,stress sensitivity,the nano-confinement(NC)effect.Moreover,a modified embedded discrete fracture model(EDFM)is used to model the complex fractures,which optimizes connection types and half-transmissibility calculation approaches between non-neighboring connections(NNCs).The full implicit equation adopts the finite volume method(FVM)and Newton—Raphson iteration for discretization and solution.The model verification with the Eclipse300 and MRST is satisfactory.The results show that the interaction between the mechanisms significantly affects the production performance and storage characteristics.The effect of molecular diffusion may be overestimated in oil-dominated(liquid-dominated)shale reservoirs.The well spacing and injection gas rate are the most crucial factors affecting the production by sensitivity analysis.Moreover,the potential gas invasion risk is mentioned.This model provides a reliable theoretical basis for CO_(2)-EOR and sequestration in shale oil reservoirs.
基金supported by the National Natural Science Foundation of China(Grant Nos.41977248 and 42207219)the Key Research Program of the Institute of Geology and Geophysics,Chinese Academy of Sciences(CAS)(Grant No.IGGCAS-201903).
文摘Reef limestone is a biogenic sedimentary rock widely distributed in coral reef areas, acting as an important foundation for coast construction. Due to its special biogenic origin, reef limestone is different from conventional rocks both in terms of rock structure and mechanical properties. In this study, mesoscale uniaxial compression experiments with five different loading directions were conducted on two kinds of reef limestones from the Maldives Islands and the South China Sea, respectively. The real-time high-resolution videos and images of failure processes were recorded simultaneously to investigate the fracture evolution and fracture surface roughness of reef limestones. It demonstrated that the reef limestones belonged to extremely soft to soft rocks, and their uniaxial compressive strength (UCS) values fluctuated with high discreteness. The mesoscale mechanical properties of reef limestones were highly anisotropic and mainly controlled by pore structure. The occurrence of dissolution pores in reef limestone tended to intensify mechanical anisotropy. With the integration of the fracture initiation and propagation features of reef limestones, it is supposed that the intrinsic mechanism of anisotropy was probably attributed to the differences in coral growth direction and dissolution. Furthermore, the quantified fracture surface roughness was revealed to have a good consistency with density and UCS for the reef limestones from the South China Sea. The findings are helpful for providing theoretical and experimental references for engineering construction in coral reef areas.
基金The National Natural Science Foundation of China(Nos.51671017,51971020)the Major State Research and Development Program of China(No.2016YFB0300801)+4 种基金Beijing Municipal Natural Science Foundation(No.2202033)Beijing Laboratory of Metallic Materials and Processing for Modern Transportationthe fund of the State Key Laboratory of Solidification Processing in NWPU(No.SKLSP201835)the Fundamental Research Funds for the Central Universities(No.FRF-IC-19–010,FRF-IC-19–015)the Opening Research Fund of State Key Laboratory for Advanced Metals and Materials(2018-Z04)。
文摘Magnesium alloys,a novel functional material for the fabrication of fracturing tools,are being paid more and more attentions recently due to their relatively high mechanical properties and fast dissolubility ability after fracturing.In this study,the novel extruded Mg-10Gd-3Y-0.3Zr-xNi alloys will be reported and their microstructure,mechanical and corrosion behaviors will be also studied.The results show that Ni contents influence phase precipitation behaviors.With adding 0.2 wt%Ni,a large amount of Zr_(7)Ni_(10)phases will be precipitated insidesα-Mg matrix,directly leading to degradation of strength and large corrosion rate.With further increasing Ni contents,the precipitation phases can be changed from Mg_(5)RE to 18R-LPSO structure,resulting in higher mechanical properties and faster corrosion rate.Moreover,adding Ni element also change the texture orientation by influencing the precipitation behavior of the alloys.The alloys invented in this paper have attained the highest compressive and tensile properties among all the reported dissoluble magnesium alloys.This work is beneficial in understanding the role of Ni in the magnesium alloys and provides more materials alternatives for the fabrication of dissoluble fracturing tools.
基金This work is financially supported by the National Key Research and Development Program of China(Grant No.2016YFB0301100)the Chongqing Foundation and Advanced Research Project(Grant No.cstc2019jcyj-zdxmX0010)+1 种基金the Natural Science Foundation Commission of China(Grant No.51571044 and 51874062)Fundamental Research Funds for the Central Universities(Grant No.2018CDGFCL0005 and 2019CDXYCL0031).
文摘In this work,as-cast Mg-Ni-Y alloys were proposed to develop a feasible material for fracturing balls,and their mechanical performance and corrosion behavior were systematically investigated.Long period stacking order(LPSO)phase was firstly introduced to improve both the mechanical properties and degradation rate of magnesium alloys.With the increase of LPSO phase,the compressive strength was improved significantly,while the elongation of the alloys decreased owing to the relatively brittle nature of LPSO phase.Due to the higher corrosion potential of LPSO phase,the LPSO phase can accelerate the corrosion process by providing more micro-couples.However,the LPSO phase would serve as the corrosion barrier between the corrosion medium and the matrix when the contents of LPSO phase are too high in Mg92.5Ni3Y4.5 and Mg87.5Ni5Y7.5 alloys.As-cast Mg97.5Ni1Y1.5 alloy with satisfactory mechanical properties and rapid degradation rate was successfully developed,exhibiting a high degradation rate of 6675 mm/a(93℃)in 3 wt.%KCl solution and a favorable ultimate compressive strength of 410 MPa.The degradation rate of Mg97.5Ni1Y1.5 alloy is 2-5 times of the current commercial magnesium alloy fracturing materials.
基金sponsored by the National Science and Technology Major Project(2017ZX05039-004)。
文摘The premise of hydraulic fracturing is to have an accurate and detailed understanding of the rock mechanical properties and fracture propagation law of shale reservoirs. In this paper,a comprehensive evaluation of the mechanical properties of the shale oil reservoir in the south of Songliao Basin is carried out. Based on the experiments and the in-situ stress analysis, the fracture propagation law of three types of shale reservoirs is obtained,and the suggestions for fracturing are put forward. The results have shown that the fracture propagation of pure shale and low mature reservoir is easy to open along the bedding plane under compression loading,which is greatly influenced by the bedding. Sand-bearing shale is slightly better,the fractures of which are not easy to open along the bedding plane. The mechanical experimental results show that all the samples have the characteristics of low compressive strength,low Young’s modulus and strong anisotropy,indicating that the shale oil reservoir is certain plastic,which is related to its high clay mineral content and controlled by the bedding development. Compared with pure shale and low mature shale,the sandbearing shale has less clay content and less developed bedding,which maybe the main reason for its slightly better brittleness. Overall,the expansion of hydraulic fracture is controlled by in-situ stress and bedding. Because of the development of bedding,it is easy to form horizontal fractures. Thus it is not suitable for horizontal well fracturing.Because of the high content of clay minerals,the applicability of conventional slick hydraulic fracturing fluid is poor. It is suggested to use vertical well or directional well to carry out volume fracturing. In this way,the effect of bedding can be effectively used to open and connect the bedding and form a larger fracture network.
基金supported by the National Natural Science Foundation of China(Grant Nos.51979146 and 11272178)。
文摘The influence of rock mechanical properties on the electromagnetic radiation(EMR)mechanism of rock fracturing is an important research topic in solid mechanics and earthquake prediction.In this study,an EMR model of rock fracturing considering the fracture factor,elastic modulus,Poisson’s ratio,radiation distance and crack length is derived based on the Hertz oscillator array assumption.An experimental system,including an electromagnetic shielding module,an EMR signal induction and transmission module,a signal recording module and a loading module,is developed to understand the EMR characteristics of four different rocks.The validity of the EMR theoretical model is verified and the relationships between the rock cracking morphology and the EMR waveform,amplitude and frequency are revealed.It is found that rock mechanical properties have obvious influences on the EMR waveform,amplitude and frequency during rock fracturing.This study provides a better understanding on the EMR mechanism of rock fracturing and can help to improve the accuracy of rock disaster prediction based on EMR.
基金Supported by Science and Technology Cooperation Project of the CNPC-SWPU Innovation Alliance(2020CX040000)Sichuan Science and Technology Program(2020JDTD0019)+1 种基金National Natural Science Foundation of China(52004231)Research Project of Dagang Oilfield(NO.DGYT-2018-JS-244).
文摘Based on the elastoplastic model of cement sheath considering the influence of three-dimensional principal stress and the stress field model of interface crack,a mechanical performance design method of cement sheath is established to meet the wellbore sealing requirements during fracturing.This method takes the failure types of the cement sheath,such as tensile failure,plastic yield,interface crack propagation along interface and zigzag propagation into account.Meanwhile,the elasticity modulus and Poisson's ratio quantitative design charts of cement sheath are constructed based on this method,and the safety and risk areas of wellbores are defined,which quantify the yield strength and tensile strength indexes of cement sheath.The results show that decreasing elasticity modulus,increasing yield strength and Poisson's ratio of cement sheath can avoid plastic deformation of cement sheath;increasing the tensile strength of cement sheath can prevent its tensile failure;increasing elasticity modulus and Poisson's ratio of cement sheath is good for shortening the length of the interface crack,but will increase the risk of interface cracks zigzagging into cement sheath.The model calculation and case verification has proved that the method in this paper can give accurate calculation results and is convenient for field application.