The cast structure of a K465 nickel-based superalloy with different temperatures of melt superheating treatment was studied. It is shown that melt superheating treatment plays a significant role in the grain size and ...The cast structure of a K465 nickel-based superalloy with different temperatures of melt superheating treatment was studied. It is shown that melt superheating treatment plays a significant role in the grain size and carbide morphology. With increasing melt superheating temperature (below 2023 K),the grain size increases obviously and the carbide morphology is changed from a blocky to a script-like shape. However,when the melt superheating temperature is between 2023 K and 2123 K,the grain size decreases gradually,and the morphology of the MC carbide changes back to the blocky appearance. The content of W is also influenced by melt superheating treatment.展开更多
The influence of melt superheating treatment on the solid/liquid (S/L) interface morphology of directionally solidified Ni-based superalloy DZ125 is investigated to elucidate the relationship between melt characteri...The influence of melt superheating treatment on the solid/liquid (S/L) interface morphology of directionally solidified Ni-based superalloy DZ125 is investigated to elucidate the relationship between melt characteristic and S/L interface stability. The results indicate that the interface morphology is not only related to the withdrawal velocity (R) but also to the melt superheating temperature (Ts) when the thermal gradient of solidification interface remains constant for different Ts with appropriate superheating treatment regulation. The interface morphology changes from cell to plane at R of 1.1 μm/s when Ts increases from 1500°C to 1650°C, and maintains plane with further elevated Ts of 1750°C. However, the interface morphology changes from coarse dendrite to cell and then to cellular dendrite at R of 2.25 μm/s when Ts increases from 1500°C to 1650°C and then to 1750°C. It is proved that the solidification onset temperature and the solidification interval undergo the nonlinear variation when Ts increases from 1500°C to 1680°C, and the turning point is 1650°C at which the solidification onset temperature and the solidification interval are all minimum. This indicates that the melt superheating treatment enhances the solidification interface stability and has important effect on the solidification characteristics.展开更多
Melt-spun Nd7Fe90B3 ribbons were prepared under different melt treatment conditions,i.e.,the melt temperature was varied prior to ejection onto the quenching wheel.The microstructure characteristics,crystallization be...Melt-spun Nd7Fe90B3 ribbons were prepared under different melt treatment conditions,i.e.,the melt temperature was varied prior to ejection onto the quenching wheel.The microstructure characteristics,crystallization behavior,and subsequent magnetic properties of α-Fe/Nd2Fe14B-based exchange-spring magnets were investigated using X-ray diffraction,differential scanning calorimeter,transmission electron microscopy,and vibrating sample magnetometer.It was shown that melt spinning at different quenching temperat...展开更多
文摘The cast structure of a K465 nickel-based superalloy with different temperatures of melt superheating treatment was studied. It is shown that melt superheating treatment plays a significant role in the grain size and carbide morphology. With increasing melt superheating temperature (below 2023 K),the grain size increases obviously and the carbide morphology is changed from a blocky to a script-like shape. However,when the melt superheating temperature is between 2023 K and 2123 K,the grain size decreases gradually,and the morphology of the MC carbide changes back to the blocky appearance. The content of W is also influenced by melt superheating treatment.
基金supports from the National Natural Science Foundation of China (Grant No. 50931004)the National Basic Research Program of China (Grant Nos. 2011CB610406 and 2010CB631202)the National High Technology Research and Development Program (Grant No. 2007AA03Z552)
文摘The influence of melt superheating treatment on the solid/liquid (S/L) interface morphology of directionally solidified Ni-based superalloy DZ125 is investigated to elucidate the relationship between melt characteristic and S/L interface stability. The results indicate that the interface morphology is not only related to the withdrawal velocity (R) but also to the melt superheating temperature (Ts) when the thermal gradient of solidification interface remains constant for different Ts with appropriate superheating treatment regulation. The interface morphology changes from cell to plane at R of 1.1 μm/s when Ts increases from 1500°C to 1650°C, and maintains plane with further elevated Ts of 1750°C. However, the interface morphology changes from coarse dendrite to cell and then to cellular dendrite at R of 2.25 μm/s when Ts increases from 1500°C to 1650°C and then to 1750°C. It is proved that the solidification onset temperature and the solidification interval undergo the nonlinear variation when Ts increases from 1500°C to 1680°C, and the turning point is 1650°C at which the solidification onset temperature and the solidification interval are all minimum. This indicates that the melt superheating treatment enhances the solidification interface stability and has important effect on the solidification characteristics.
基金supported by the Science and Technology Foundation of Shenzhen,China (200605)
文摘Melt-spun Nd7Fe90B3 ribbons were prepared under different melt treatment conditions,i.e.,the melt temperature was varied prior to ejection onto the quenching wheel.The microstructure characteristics,crystallization behavior,and subsequent magnetic properties of α-Fe/Nd2Fe14B-based exchange-spring magnets were investigated using X-ray diffraction,differential scanning calorimeter,transmission electron microscopy,and vibrating sample magnetometer.It was shown that melt spinning at different quenching temperat...