Additive manufacturing(AM)is an emerging customized three-dimensional(3D)functional product fabrication technology.It provides a higher degree of design freedom,reduces manufacturing steps,cost and production cycles.H...Additive manufacturing(AM)is an emerging customized three-dimensional(3D)functional product fabrication technology.It provides a higher degree of design freedom,reduces manufacturing steps,cost and production cycles.However,existing metallic component 3D printing techniques are mainly for the manufacture of single material components.With the increasing commercial applications of AM technologies,the need for 3D printing of more than one type of dissimilar materials in a single component increases.Therefore,investigations on multi-material AM(MMAM)emerge over the past decade.Lasers are currently widely used for the AM of metallic components where high temperatures are involved.Here we report the progress and trend in laser-based macro-and micro-scale AM of multiple metallic components.The methods covered in this paper include laser powder bed fusion,laser powder directed energy deposition,and laser-induced forward transfer for MMAM applications.The principles and process/material characteristics are described.Potential applications and challenges are discussed.Finally,future research directions and prospects are proposed.展开更多
Metal mold micron scale precision casting technology was developed successfully,and three-dimension complicated microgear castings in micron scale were produced.Evolvement regularity of microgear castings were observe...Metal mold micron scale precision casting technology was developed successfully,and three-dimension complicated microgear castings in micron scale were produced.Evolvement regularity of microgear castings were observed by optical microscope and scanning electron microscope.Compared with conventional casting,microcasting is characterized by typical nonequilibrium solidification,for example,its grain size can be refined significantly,eutectic structure is transformed from lamellar morphology to rod eutectic,and the ratio of primary phase is increased.This kind of microstructure can promote mechanical properties of microcasting.展开更多
In this paper,we report the study of the process of fabricating a multi-layermetal micro-structure using UV-LIGA overlay technology,includingmask fabrication,substrate treatment,and UV-LIGA overlay processes.To solve ...In this paper,we report the study of the process of fabricating a multi-layermetal micro-structure using UV-LIGA overlay technology,includingmask fabrication,substrate treatment,and UV-LIGA overlay processes.To solve the process problems in the masking procedure,the swelling problemof the first layer of SU-8 thick photoresist was studied experimentally.The 5μmline-width compensation and closed 20μmand 30μmisolation strips were designed and fabricated around the micro-structure pattern.The pore problemin the Ni micro-electroforming layer was analyzed and the electroforming parameters were improved.The pH value of the electroforming solution should be controlled between 3.8 and 4.4 and the current density should be below 3 A/dm^2.To solve the problems of high inner stress and incomplete development of the micro-cylinder hole array with a diameter of 30μm,the lithography process was optimized.The pre-baking temperature was increased via gradient heating and rose every 5℃ from 65℃ to 85℃ and then remained at 85℃ for 50 min–1 h.In addition,the full contact exposure was used.Finally,a multi-layer metal micro-structure with high precision and good quality of microelectroforming layer was fabricated using UV-LIGA overlay technology.展开更多
Effects of the volume fraction and the size of crystallized alumina silicate short fibers as well as heat treatment processes on micro-yield strength(MYS) of Al2O3-SiO2(sf)/Al-Si metal matrix composite(MMC) that was f...Effects of the volume fraction and the size of crystallized alumina silicate short fibers as well as heat treatment processes on micro-yield strength(MYS) of Al2O3-SiO2(sf)/Al-Si metal matrix composite(MMC) that was fabricated by squeezing cast, were investigated by using continuous loading method on an Instron 5569 tester with a special extensometer with an accuracy of 10?7. The results show that MYS of MMC decreases with the increase of volume fraction and length of the alumina silicate short fibers in the metal matrix composite, respectively. MYS of quenched Al2O3-SiO2(sf)/Al-Si MMC is the lowest, MYS of the MMC through peak-aging treatment is higher than that through other heat treatment methods. And before the peak-aging, MYS of MMC aging treated gradually increases with the increase of the aging time. Aging treatment after solution treatment is a preferred way that enhances micro and macro-yield strength of Al2O3-SiO2(sf)/Al-Si MMC.展开更多
The coagulation time and position of micro-sized non-metallic inclusions in molten metal during ultrasonic separation process were investigated, and the motion course of micro-sized non-metallic inclusions in an ultra...The coagulation time and position of micro-sized non-metallic inclusions in molten metal during ultrasonic separation process were investigated, and the motion course of micro-sized non-metallic inclusions in an ultrasonic standing wave field was numerically simulated. The results of theoretical analysis and numerical simulation show that the movement of inclusions depends on the balance between the acoustic radiation force, effective buoyancy force and viscous drag force. It is presented that micro-sized inclusions, agglomerated at antinode-planes may be removed further with horizon tal ultrasound.``展开更多
The microstructure in the weld metals for HQ130 + QJ63 high strength steels,which are welded by Ar-CO_2 gas shielded metal arc welding,was analyzed by means of microscope and scan electron microscope(SEM).The relative...The microstructure in the weld metals for HQ130 + QJ63 high strength steels,which are welded by Ar-CO_2 gas shielded metal arc welding,was analyzed by means of microscope and scan electron microscope(SEM).The relative content of different microstructure was evaluated with XQF-2000 micro-image analyzer.The effect of acicular ferrite content on the impact toughness was also studied.The test results indicated that the main microstructure in the weld metals of HQ130 + QJ63 high strength steels is acicular ferrite and a few pro-eutectic ferrite on the boundary of original austenite grain.Near the fusion zone there are columnar grains whose direction coefficient(X) is 3.22,but the microstructure in the center of the weld metal is isometric grain,whose direction coefficient X = 1.In order to avoid welding crack and improve welding technology the weld heat input should be strictly controlled in 10-16 kJ/cm.Thus,the main microstructure in the weld metals is fine acicular ferrite and the content of pro-eutectic ferrite is limited.The impact toughness in the weld metals of HQ130+ QJ63 steels can be ensured and can meet the requirements for application in engineering and machinery.展开更多
Multifunctional photodetectors boost the development of traditional optical communication technology and emerging artificial intelligence fields, such as robotics and autonomous driving. However, the current implement...Multifunctional photodetectors boost the development of traditional optical communication technology and emerging artificial intelligence fields, such as robotics and autonomous driving. However, the current implementation of multifunctional detectors is based on the physical combination of optical lenses, gratings, and multiple photodetectors, the large size and its complex structure hinder the miniaturization, lightweight, and integration of devices. In contrast, perovskite materials have achieved remarkable progress in the field of multifunctional photodetectors due to their diverse crystal structures, simple morphology manipulation, and excellent optoelectronic properties. In this review, we first overview the crystal structures and morphology manipulation techniques of perovskite materials and then summarize the working mechanism and performance parameters of multifunctional photodetectors. Furthermore, the fabrication strategies of multifunctional perovskite photodetectors and their advancements are highlighted, including polarized light detection, spectral detection, angle-sensing detection, and selfpowered detection. Finally, the existing problems of multifunctional detectors and the perspectives of their future development are presented.展开更多
Metal nano layer coating for increasing the sensitivity of spectroscopic measurements is proposed and experimentally demonstrated in this paper. The metal nano layer will attract the micro-poisons from any measured aq...Metal nano layer coating for increasing the sensitivity of spectroscopic measurements is proposed and experimentally demonstrated in this paper. The metal nano layer will attract the micro-poisons from any measured aqueous sample increasing the concentration of the micro-poison in the vicinity of the surface and significantly improves the sensitivity of the spectroscopic measurement. The demonstration was carried out using Fourier Transform Infra-Red (FTIR) operating in the MIR 400 cm-1 - 4000 cm-1 and 5 nm Gold layer which was grown on silicon oxide substrate. In the experimental demonstration Malathion organophosphate pesticide was used as micro-poison. The spectroscopic measurement proves that Malathion was attracted to the metal nano layer. Furthermore, the absorption lines of Malathion were detected and recognized. This proof of principle can be applied to any Internal Reflection Elements (IRE) and it can be used to purify any aqueous solutions and atmosphere from micro-poisons which will be attracted to the metal Nano layer.展开更多
The metal cutting process is accompanied by complex stress field,strain field,temperature field.The comprehensive effects of process parameters on chip morphology,cutting force,tool wear and residual stress are comple...The metal cutting process is accompanied by complex stress field,strain field,temperature field.The comprehensive effects of process parameters on chip morphology,cutting force,tool wear and residual stress are complex and inter-connected.Finite element method(FEM)is considered as an effective method to predict process variables and reveal microscopic physical phenomena in the cutting process.Therefore,the finite element(FE)simulation is used to research the conventional and micro scale cutting process,and the differences in the establishment of process variable FE simulation models are distinguished,thereby improving the accuracy of FE simulation.The reliability and effectiveness of FE simulation model largely depend on the accuracy of the simulation method,constitutive model,friction model,damage model in describing mesh element,the dynamic mechanical behavior of materials,the tool-chip-workpiece contact process and the chip formation mechanism.In this paper,the FE models of conventional and micro process variables are comprehensively and up-to-date reviewed for different materials and machining methods.The purpose is to establish a FE model that is more in line with the real cutting conditions,and to provide the possibility for optimizing the cutting process variables.The development direction of FE simulation of metal cutting process is discussed,which provides guidance for future cutting process modeling.展开更多
文摘Additive manufacturing(AM)is an emerging customized three-dimensional(3D)functional product fabrication technology.It provides a higher degree of design freedom,reduces manufacturing steps,cost and production cycles.However,existing metallic component 3D printing techniques are mainly for the manufacture of single material components.With the increasing commercial applications of AM technologies,the need for 3D printing of more than one type of dissimilar materials in a single component increases.Therefore,investigations on multi-material AM(MMAM)emerge over the past decade.Lasers are currently widely used for the AM of metallic components where high temperatures are involved.Here we report the progress and trend in laser-based macro-and micro-scale AM of multiple metallic components.The methods covered in this paper include laser powder bed fusion,laser powder directed energy deposition,and laser-induced forward transfer for MMAM applications.The principles and process/material characteristics are described.Potential applications and challenges are discussed.Finally,future research directions and prospects are proposed.
基金Project(50475028)supported by the National Natural Science Foundation of China
文摘Metal mold micron scale precision casting technology was developed successfully,and three-dimension complicated microgear castings in micron scale were produced.Evolvement regularity of microgear castings were observed by optical microscope and scanning electron microscope.Compared with conventional casting,microcasting is characterized by typical nonequilibrium solidification,for example,its grain size can be refined significantly,eutectic structure is transformed from lamellar morphology to rod eutectic,and the ratio of primary phase is increased.This kind of microstructure can promote mechanical properties of microcasting.
文摘In this paper,we report the study of the process of fabricating a multi-layermetal micro-structure using UV-LIGA overlay technology,includingmask fabrication,substrate treatment,and UV-LIGA overlay processes.To solve the process problems in the masking procedure,the swelling problemof the first layer of SU-8 thick photoresist was studied experimentally.The 5μmline-width compensation and closed 20μmand 30μmisolation strips were designed and fabricated around the micro-structure pattern.The pore problemin the Ni micro-electroforming layer was analyzed and the electroforming parameters were improved.The pH value of the electroforming solution should be controlled between 3.8 and 4.4 and the current density should be below 3 A/dm^2.To solve the problems of high inner stress and incomplete development of the micro-cylinder hole array with a diameter of 30μm,the lithography process was optimized.The pre-baking temperature was increased via gradient heating and rose every 5℃ from 65℃ to 85℃ and then remained at 85℃ for 50 min–1 h.In addition,the full contact exposure was used.Finally,a multi-layer metal micro-structure with high precision and good quality of microelectroforming layer was fabricated using UV-LIGA overlay technology.
基金Project(19972021)supported by the National Natural Science Foundation of China
文摘Effects of the volume fraction and the size of crystallized alumina silicate short fibers as well as heat treatment processes on micro-yield strength(MYS) of Al2O3-SiO2(sf)/Al-Si metal matrix composite(MMC) that was fabricated by squeezing cast, were investigated by using continuous loading method on an Instron 5569 tester with a special extensometer with an accuracy of 10?7. The results show that MYS of MMC decreases with the increase of volume fraction and length of the alumina silicate short fibers in the metal matrix composite, respectively. MYS of quenched Al2O3-SiO2(sf)/Al-Si MMC is the lowest, MYS of the MMC through peak-aging treatment is higher than that through other heat treatment methods. And before the peak-aging, MYS of MMC aging treated gradually increases with the increase of the aging time. Aging treatment after solution treatment is a preferred way that enhances micro and macro-yield strength of Al2O3-SiO2(sf)/Al-Si MMC.
文摘The coagulation time and position of micro-sized non-metallic inclusions in molten metal during ultrasonic separation process were investigated, and the motion course of micro-sized non-metallic inclusions in an ultrasonic standing wave field was numerically simulated. The results of theoretical analysis and numerical simulation show that the movement of inclusions depends on the balance between the acoustic radiation force, effective buoyancy force and viscous drag force. It is presented that micro-sized inclusions, agglomerated at antinode-planes may be removed further with horizon tal ultrasound.``
基金supported by the visting scholar foundation of the National Key Laboratory of the Advanced Welding Production Technology,Harbin Institute of Technology,P.R.China
文摘The microstructure in the weld metals for HQ130 + QJ63 high strength steels,which are welded by Ar-CO_2 gas shielded metal arc welding,was analyzed by means of microscope and scan electron microscope(SEM).The relative content of different microstructure was evaluated with XQF-2000 micro-image analyzer.The effect of acicular ferrite content on the impact toughness was also studied.The test results indicated that the main microstructure in the weld metals of HQ130 + QJ63 high strength steels is acicular ferrite and a few pro-eutectic ferrite on the boundary of original austenite grain.Near the fusion zone there are columnar grains whose direction coefficient(X) is 3.22,but the microstructure in the center of the weld metal is isometric grain,whose direction coefficient X = 1.In order to avoid welding crack and improve welding technology the weld heat input should be strictly controlled in 10-16 kJ/cm.Thus,the main microstructure in the weld metals is fine acicular ferrite and the content of pro-eutectic ferrite is limited.The impact toughness in the weld metals of HQ130+ QJ63 steels can be ensured and can meet the requirements for application in engineering and machinery.
基金supported financially by the National Key R&D Program of China (Nos. 2018YFA0208501 and 2018YFA0703200)the National Natural Science Foundation of China (NSFC, Nos. 52103236, 91963212, 21875260)Beijing National Laboratory for Molecular Sciences (No. BNLMSCXXM-202005)。
文摘Multifunctional photodetectors boost the development of traditional optical communication technology and emerging artificial intelligence fields, such as robotics and autonomous driving. However, the current implementation of multifunctional detectors is based on the physical combination of optical lenses, gratings, and multiple photodetectors, the large size and its complex structure hinder the miniaturization, lightweight, and integration of devices. In contrast, perovskite materials have achieved remarkable progress in the field of multifunctional photodetectors due to their diverse crystal structures, simple morphology manipulation, and excellent optoelectronic properties. In this review, we first overview the crystal structures and morphology manipulation techniques of perovskite materials and then summarize the working mechanism and performance parameters of multifunctional photodetectors. Furthermore, the fabrication strategies of multifunctional perovskite photodetectors and their advancements are highlighted, including polarized light detection, spectral detection, angle-sensing detection, and selfpowered detection. Finally, the existing problems of multifunctional detectors and the perspectives of their future development are presented.
文摘Metal nano layer coating for increasing the sensitivity of spectroscopic measurements is proposed and experimentally demonstrated in this paper. The metal nano layer will attract the micro-poisons from any measured aqueous sample increasing the concentration of the micro-poison in the vicinity of the surface and significantly improves the sensitivity of the spectroscopic measurement. The demonstration was carried out using Fourier Transform Infra-Red (FTIR) operating in the MIR 400 cm-1 - 4000 cm-1 and 5 nm Gold layer which was grown on silicon oxide substrate. In the experimental demonstration Malathion organophosphate pesticide was used as micro-poison. The spectroscopic measurement proves that Malathion was attracted to the metal nano layer. Furthermore, the absorption lines of Malathion were detected and recognized. This proof of principle can be applied to any Internal Reflection Elements (IRE) and it can be used to purify any aqueous solutions and atmosphere from micro-poisons which will be attracted to the metal Nano layer.
基金supported by the National Natural Science Foundation of China(No.52175393)。
文摘The metal cutting process is accompanied by complex stress field,strain field,temperature field.The comprehensive effects of process parameters on chip morphology,cutting force,tool wear and residual stress are complex and inter-connected.Finite element method(FEM)is considered as an effective method to predict process variables and reveal microscopic physical phenomena in the cutting process.Therefore,the finite element(FE)simulation is used to research the conventional and micro scale cutting process,and the differences in the establishment of process variable FE simulation models are distinguished,thereby improving the accuracy of FE simulation.The reliability and effectiveness of FE simulation model largely depend on the accuracy of the simulation method,constitutive model,friction model,damage model in describing mesh element,the dynamic mechanical behavior of materials,the tool-chip-workpiece contact process and the chip formation mechanism.In this paper,the FE models of conventional and micro process variables are comprehensively and up-to-date reviewed for different materials and machining methods.The purpose is to establish a FE model that is more in line with the real cutting conditions,and to provide the possibility for optimizing the cutting process variables.The development direction of FE simulation of metal cutting process is discussed,which provides guidance for future cutting process modeling.