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3-甲基-4-乙氧甲酰-2-环己烯酮合成方法的改进 被引量:5
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作者 胡炳成 吕春绪 刘祖亮 《应用化学》 CAS CSCD 北大核心 2003年第10期1012-1014,共3页
The method for synthesis of the title compound has been improved, with product yield being increased to 58%. The following measures have been adopted: using 1,8-diazabicyclo\undec-7-ene(DBU) as catalyst instead of pip... The method for synthesis of the title compound has been improved, with product yield being increased to 58%. The following measures have been adopted: using 1,8-diazabicyclo\undec-7-ene(DBU) as catalyst instead of piperidine; adding benzene in the reaction mixture to favor azeotropic dehydration. The optimum molar ratio of DBU/ethylacetoacetate/solid paraformaldehyde was 4∶20∶11. 展开更多
关键词 甲基乙氧羰基环己烯酮 二氮杂双环十一烯 多聚甲醛 合成
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