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Microwave-assisted Micellar Extraction and Determination of Glycyrrhizic Acid and Liquiritin in Licorice Root by HPLC 被引量:4
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作者 孙晨 谢渝春 刘会洲 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2007年第4期474-477,共4页
The feasibility of emploving non-ionic surfactant (Triton X-100) as an alternative and effective solventfor the microwave-assisted extraction of glycyrrhizic acid (GA) and liquiritin (LQ) from licorice root was ... The feasibility of emploving non-ionic surfactant (Triton X-100) as an alternative and effective solventfor the microwave-assisted extraction of glycyrrhizic acid (GA) and liquiritin (LQ) from licorice root was studied.The optimal extraction parameters based on the microwave-assisted micellar extraction technique were determined.Under the optimal conditions, i.e. 5% (by volume) Triton X-100, microwave-assisted extraction for 3--5min at 373K, the percentage extraction of active ingredients reached the highest value. The preconcentration tactor for GA and L'Q (about 13.5) and the extraction efficiency for these two ingredients approached 100% showed the coupling of microwave-assisted extraction and cloud-point extraction could be employed as a new and. effective techniquefor the rapid extraction and preconcentration of pharrnacologically active ingredients from medicinal plants SUCh aslicorice root without disturbing chromatographic analysis. 展开更多
关键词 microwave-assisted micellarextraction cloud-point extraction Triton X-100 glycyrrhizic acid LIQUIRITIN
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