In recent years, a new kind of drilling fluid system with unique structure micro-foam has been developed. Compared with other drilling fluid systems, it possesses many advantages. And it has been successfully applied ...In recent years, a new kind of drilling fluid system with unique structure micro-foam has been developed. Compared with other drilling fluid systems, it possesses many advantages. And it has been successfully applied in hundreds of wells to drill depleted reservoirs in the world wide. The geological structure is very complex in Haita area, it is difficult to achieve the requirement of increasing drilling rate by conventional drilling methods, even can’t make footage. The micro-foam drilling fluid can apply to Haita area, and solve the drilling problems commendably, which is comprehended by studying the structure and plugging, prevent caving, speed mechanism of the micro-foam drilling fluid. Field practice indicates that micro-foam drilling fluid technology can resolve the drilling problem effectively in Haita basin. It has the extremely vital significance to improve drilling speed, discover and protect reservoir stratum, decrease the risk of circulation loss and save the drilling cost.展开更多
Emulsifier-free poly(methyl methacrylate-styrene) [P(MMA-St)] nanospheres with an average particle size of 100 nm were synthesized in an isopropyl alcoholwater medium by a solvothermal method. Then, through radica...Emulsifier-free poly(methyl methacrylate-styrene) [P(MMA-St)] nanospheres with an average particle size of 100 nm were synthesized in an isopropyl alcoholwater medium by a solvothermal method. Then, through radical graft copolymerization of thermo-sensitive mono- mer N-isopropylacrylamide (NIPAm) and hydrophilic monomer acrylic acid (AA) onto the surface of P(MMA- St) nanospheres at 80 ℃, a series of thermo-sensitive polymer nanospheres, named SD-SEAL with different lower critical solution temperatures (LCST), were prepared by adjusting the mole ratio of NIPAm to AA. The products were characterized by Fourier transform infrared spectroscopy, transmission electron microscopy, thermogravimetric analysis, particle size distribution, and specific surface area analysis. The temperature-sensitive behavior was studied by light transmittance tests, while the sealing performance was investigated by pressure transmission tests with Lungmachi Formation shales. The experimental results showed that the synthesized nanoparticles are sensitive to temperature and had apparent LCST values which increased with an increase in hydrophilic monomer AA. When the temperature was higher than its LCST value, SD- SEAL played a dual role of physical plugging and chemical inhibition, slowed down pressure transmission, and reduced shale permeability remarkably. The plugged layer of shale was changed to being hydrophobic, which greatly improved the shale stability展开更多
Modeling of the roughness in micro-nano scale and its influence have not been fully investigated, however the roughness will cause amplitude and phase errors of the radiating slot, and decrease the precision and effic...Modeling of the roughness in micro-nano scale and its influence have not been fully investigated, however the roughness will cause amplitude and phase errors of the radiating slot, and decrease the precision and efficiency of the SWA in Ku-band. Firstly, the roughness is simulated using the electromechanical coupled(EC) model. The relationship between roughness and the antenna's radiation properties is obtained. For verification, an antenna proto- type is manufactured and tested, and the simulation method is introduced. According to the prototype, a contrasting experiment dealing with the flatness of the radiating plane is conducted to test the simulation method. The advantage of the EC model is validated by comparisons of the EC model and two classical roughness models (sine wave and fractal function), which shows that the EC model gives a more accurate description model for roughness, the maxi- mum error is 13%. The existence of roughness strongly broadens the beamwidth and raises the side-lobe level of SWA, which is 1.2 times greater than the ideal antenna. In addition, effect of the EC model's evaluation indices is investigated, the most affected scale of the roughness is found, which is 1/10 of the working wavelength. The proposed research provides the instruction for antenna designing and manufacturing.展开更多
文摘In recent years, a new kind of drilling fluid system with unique structure micro-foam has been developed. Compared with other drilling fluid systems, it possesses many advantages. And it has been successfully applied in hundreds of wells to drill depleted reservoirs in the world wide. The geological structure is very complex in Haita area, it is difficult to achieve the requirement of increasing drilling rate by conventional drilling methods, even can’t make footage. The micro-foam drilling fluid can apply to Haita area, and solve the drilling problems commendably, which is comprehended by studying the structure and plugging, prevent caving, speed mechanism of the micro-foam drilling fluid. Field practice indicates that micro-foam drilling fluid technology can resolve the drilling problem effectively in Haita basin. It has the extremely vital significance to improve drilling speed, discover and protect reservoir stratum, decrease the risk of circulation loss and save the drilling cost.
基金financial support from the National Science Foundation of China (Nos. 51374233, 51474235)the Postdoctoral Innovative Project Foundation of Shandong Province (No. 201602027)+2 种基金the Qingdao Postdoctoral Applied Research Project (No. 2015242)the Fundamental Research Funds for the Central Universities (No. 15CX06021A)the Graduate Student Innovation Project from China University of Petroleum (East China) (No. YCX2015011)
文摘Emulsifier-free poly(methyl methacrylate-styrene) [P(MMA-St)] nanospheres with an average particle size of 100 nm were synthesized in an isopropyl alcoholwater medium by a solvothermal method. Then, through radical graft copolymerization of thermo-sensitive mono- mer N-isopropylacrylamide (NIPAm) and hydrophilic monomer acrylic acid (AA) onto the surface of P(MMA- St) nanospheres at 80 ℃, a series of thermo-sensitive polymer nanospheres, named SD-SEAL with different lower critical solution temperatures (LCST), were prepared by adjusting the mole ratio of NIPAm to AA. The products were characterized by Fourier transform infrared spectroscopy, transmission electron microscopy, thermogravimetric analysis, particle size distribution, and specific surface area analysis. The temperature-sensitive behavior was studied by light transmittance tests, while the sealing performance was investigated by pressure transmission tests with Lungmachi Formation shales. The experimental results showed that the synthesized nanoparticles are sensitive to temperature and had apparent LCST values which increased with an increase in hydrophilic monomer AA. When the temperature was higher than its LCST value, SD- SEAL played a dual role of physical plugging and chemical inhibition, slowed down pressure transmission, and reduced shale permeability remarkably. The plugged layer of shale was changed to being hydrophobic, which greatly improved the shale stability
基金Supported by National Natural Science Foundation of China(Grant Nos.51305322,51405364,51475348)
文摘Modeling of the roughness in micro-nano scale and its influence have not been fully investigated, however the roughness will cause amplitude and phase errors of the radiating slot, and decrease the precision and efficiency of the SWA in Ku-band. Firstly, the roughness is simulated using the electromechanical coupled(EC) model. The relationship between roughness and the antenna's radiation properties is obtained. For verification, an antenna proto- type is manufactured and tested, and the simulation method is introduced. According to the prototype, a contrasting experiment dealing with the flatness of the radiating plane is conducted to test the simulation method. The advantage of the EC model is validated by comparisons of the EC model and two classical roughness models (sine wave and fractal function), which shows that the EC model gives a more accurate description model for roughness, the maxi- mum error is 13%. The existence of roughness strongly broadens the beamwidth and raises the side-lobe level of SWA, which is 1.2 times greater than the ideal antenna. In addition, effect of the EC model's evaluation indices is investigated, the most affected scale of the roughness is found, which is 1/10 of the working wavelength. The proposed research provides the instruction for antenna designing and manufacturing.