Assessing efficacy of standard impregnation techniques on die-cast aluminum alloys using X-ray micro-CT

Utilizing lightweight Al alloys in various industrial applications requires achieving precise pressure tightness and leak requirements.Vacuum pressure impregnation(VPI)with thermosetting polymers is commonly used to address leakage defects in die-cast Al alloys.In this study,the efficacy of the VPI technique in sealing alloy parts was investigated using a combination of nondestructive micro X-ray computed tomography(micro XCT)and a standard leak test.The results demonstrate that the commonly used water leak test is insufficient for determining the sealing performance.Instead,micro XCT shows distinct advantages by enabling more comprehensive analysis.It reveals the presence of a low atomic number impregnates sealant within casting defects,which has low grey contrast and allows for visualizing primary leakage paths in 3D.The effective atomic number of impregnated resin is 6.75 and that of Al alloy is 13.69 by dual-energy X-ray CT.This research findings will contribute to enhancing the standard VPI process parameters and the properties of impregnating sealants to improve quality assurance for impregnation in industrial metals.

MICRO TEST1自动血沉仪性能评价及生物参考区间的建立

目的探讨MICRO TEST1自动红细胞沉降率(下称血沉)仪检测血沉的可靠性及建立该方法健康成人生物参考区间。方法随机抽取门诊患者90例,分别应用MICRO TEST1自动血沉仪和1993年国际血液学标准化委员会(ICSH)推荐的血沉测定标准方法(即魏氏法)同时检测血沉,对数据进行统计学分析与比较;应用MICRO TEST1自动血沉仪对男性321例、女性311例健康体检者测定血沉,统计该方法生物参考区间。结果MICRO TEST1自动血沉仪测定结果与魏氏法比较差异无统计学意义(P>0.05),两种方法的相关性良好(r=0.974;Y=1.015x-0.354);该方法生物参考区间第95%百分位数点:男为16.0mm/h、女为22.0mm/h,两组差异有统计学意义。结论MICROTEST1自动血沉仪是一种检测血沉快速、准确、可靠的新方法,但必须与参考方法或标准方法进行严格比对,同时应建立方法的生物参考区间。

ISOLATION DESIGN AND SIMULATIONAL EXPERIMENT OF NANOMETER MICRO MOVEMENT TEST-BED

The relation of mass, stiffness and rate of damping is obtained by using the mechanical analysis of the obstructive vibration system of two dimensions for the design of the obstructive vibration system of more freedom and the micro vibration test bed. The result of stimulational experiment indicates that the isolation of vibration of this system is satisfactory. The design method of vibration can be used as the reference to ultra precision machine tool, super micro orientation machanism and so on.

Vibration test of micro machined gyroscope based on high speed photography and SURF

Based on three kinds of dynamic test of MEMS, a dynamic system for the vibration test of micro machined gyroscope based on high speed photography is introduced. Firstly, the architecture of the system hardware is introduced. Secondly, the image tracking performance is compared by the test using the template matching algorithm, the mean shift algorithm and the SURF algorithm. The vibration curve shows that high speed photograph combined with SURF algorithm is faster, more ac- curate, and more suitable for the vibration test of micro machined gyroscope. After the frequency a- nalysis and related interpolation, more characteristics of micro gyroscope can be obtained.

Mechanical Characterization of Electroplated Ni Films by Micro-tensile Testing

Mechanical properties of structural materials are particularly important for design, performance realization and reliability analysis of microelectromechanical systems （MEMS）. Furthermore, accurate database of mechanical properties at the micro scale can provide indispensable reference for establishing MEMS standard. Electroplated nickel film is one of the most favored structural materials used in MEMS, thus its mechanical properties has been studied for many years. However, the measured values show large scatter in Yotmg＇s modulus of nickel film. Young＇s modulus and yield stress of electroplated nickel film are measured by using a micro-tensile testing instrument. The tensile load applied on the specimen is measured by a load cell with accuracy 0.25 mN directly, without additional friction. Through measuring the axial stiffness coefficient of the tensile instnunent in situ, the tensile strain of the specimen is obtained by using two-serial spring model. The electroplated nickel films were fabricated from sulfarnate baths, and the gauge section is 500μm long and 10μm wide nominally, and thickness range between 25 μm and 50μm. The obtained Young＇s modulus from tensile testing is 83＋6 GPa for nickel specimens electroplated at current density of 20 mA/cm2 and it increases to 124＋5 GPa as current density is decreased to 10 mA/cm2. The phenomena are interpreted in terms of porosity of microstructure. The higher current density produced rnicrostucture with low density and high volume fraction of pores, and the microstructure of high porosity corresponds to a lower modulus. The measured values of Young＇s modulus are consistent with those of calculated from the exponential empirical formula between Young＇s modulus and porosity. The micro-tensile testing instrument can also be used for mechanical measurement of other MEMS films.

Elastic modulus of claystone evaluated by nano-/micro-indentation tests and meso-compression tests

Toarcian claystone such as that of the Callovo-Oxfordian is a qualified multiphase material. The claystone samples tested in this study are composed of four main mineral phases: silicates(clay minerals, quartz,feldspars, micas)(z86%), sulphides(pyrite)(z3%), carbonates(calcite, dolomite)(z10%) and organic kerogen(z1%). Three sets of measurements of the modulus of deformability were compared as determined in(i) nanoindentation tests with a constant indentation depth of 2 mm,(ii) micro-indentation tests with a constant indentation depth of 20 mm, and(iii) meso-compression tests with a constant displacement of 200 mm. These three experimental methods have already been validated in earlier studies. The main objective of this study is to demonstrate the influence of the scaling effect on the modulus of deformability of the material. Different frequency distributions of the modulus of deformability were obtained at the different sample scales:(i) in nano-indentation tests, the distribution was spread between 15 GPa and 90 GPa and contained one peak at34 GPa and another at 51 GPa;(ii) in the micro-indentation tests, the distribution was spread between 25 GPa and 60 GPa and displayed peaks at 26 GPa and 37 GPa; and(iii) in the meso-compression tests, a narrow frequency distribution was obtained, ranging from 25 GPa to 50 GPa and with a maximum at around 35 GPa.

Salt spray corrosion test of micro-plasma oxidation ceramic coatings on Ti alloy

Ceramic coatings were prepared on Ti-6Al-4V alloy in NaAlO2 solution by micro-plasma oxidation （MPO）. The salt spray tests of the coated samples and the substrates were carded out in a salt spray test machine. The phase composition and surface morphology of the coatings were investigated by XRD and SEAM. Severe corrosion occurred on the substrate surface, while there were no obvious corrosion phenomena on the coated samples. The coatings were composed of Al2TiO5 and a little α-Al2O3 and mille TiO2, and the salt spray test did not change the composition of the coatings. The weight loss rate of the coatings decreased with increasing MPO time because of the increase in density and thickness of the coatings. The surface morphology of the coatings was influenced by salt spray corrosion test. Among the coated samples, the coating prepared for 2 h has the best corrosion resistance under salt spray test.

Comparison of mechanical properties in welded joint for CO_2 arc welding by using the micro－shear test and impact test

A micro shear testing method which can suit to measure the mechanical properties of heterogeneous materials is introduced, and the properties in each zone of welded joint for CO2 arc welding can be evaluated by using this method in this paper. Moreover, these results are compared with those results of Charpy V-notch impact test and their correlation is discussed.

Measurement of Ca^(2+) Flow in Cochlear Cells Using Non-Invasive Micro-Test Technique

Objective To test Calcium ion(Ca2+) flow at the head and end of outer hair cells(OHCs) in resting state and in response to Nimodipine treatment.Methods Non-invasive micro-test techniques were used to study Ca2+ in isolated OHCs in adult guinea pigs.Results Four types of Ca2+ transport were identified in OHCs on basilar membrane tissue fragments:influx at the head of with efflux at the bottom(type 1):efflux at the head of OHCs with influx at the bottom(type 2);influx at the both head and bottom(type 3);and efflux at the both head and bottom(type 4).However,only type 1 and type 3 of Ca2+ ion transport were detected in the cochlea.We propose that Ca2+ ion transport exists in adult guinea pig cochlear OHCs in resting state and is variable.Ca2 + flow in OHC can be inhibited by Nimodipine in resting state.

Micro-Doppler effect testing technique for attitude of projectile in space flight

To measure projectile attitude in space flight, based on continuous wave （CW） radar, a new micro-Doppler effect testing technique is developed in this paper. It also establishes radar testing model for attitude of flying projectile and resolve micro-Doppler effect of projectile motion attitude. By distinguishing and geting attitude parameters such as micro-motion period, this technique can in- tuitively estimate the flight stability of projectile, and the validity of this technique is proved accord- ing to flight tests.

Experimental Tests on a Pre-Heated Combustion Chamber for Ultra Micro Gas Turbine Device: Air/Fuel Ratio Evaluation

Current portable power generators are mainly based on internal combustion engine since they present higher values of efficiency comparing to other engines;the main reason why internal combustion engine is not convenient for micro power generation (5 - 30 kW) is because of their heaviness. Micro and ultra micro gas turbine devices, based on a micro compressor and a micro turbine installed on the same shaft, are more suitable for this scope for several reasons. Micro turbine systems have many advantages over reciprocating engine generators, such as higher power density (with respect to size and weight), extremely low emissions and few, or just one, moving part. Those designed with foil bearings and air-cooling operate without oil, coolants or other hazardous materials. Micro turbines also have the advantage of having the majority of their waste heat contained in their relatively high temperature exhaust. Micro turbines offer several potential advantages compared to other technologies for small-scale power generation, including: a small number of moving parts, compact size, lightweight, greater efficiency, lower emissions, lower electricity costs, and opportunities to utilize waste fuels. The object of this study is the experimental tests on a stand-alone gas turbine device with a pre-heated combustion chamber (CC), to validate the fuel consumption reduction, compared to an actual and commercial device, used on air models.

China,America Have Coo[erated in Micro Biological Production Test

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可植入无线Micro LED光遗传学硬件设计

为将光遗传技术用于自由移动生物体的体内视觉神经调控,文中提出一种新的无线能量传输、可植入、光源参数可调、多通道的光遗传硬件结构。该硬件结构主要包括Micro LED阵列多通道光源、nRF52832控制器、光驱动电路、无线能量传输电路,硬件整体尺寸为18 mm×18 mm×2 mm,质量为1.54 g,满足轻量化植入的要求。其次,设计并流片Micro LED光源阵列,单颗光源的尺寸为60μm×60μm;并在此基础上为每颗光源设计光导,实现光导直径在10μm左右,能够完成神经元级的光刺激。最后,将光源阵列的参数与光源阵列组合,运用深度学习的方法进行优化,实现光源的最优刺激。实验结果表明,光源满足光遗传的要求。

工业固废-水泥固化腐殖土的力学响应和微观机制

为了推动腐殖土在岩土工程领域的资源化利用,采用工业固废(包括生物质飞灰、电石渣和磷石膏)协同水泥对腐殖土进行固化处理。以中国广东省某陈旧型简易垃圾填埋场开采的腐殖土为研究对象,通过常规三轴试验、干湿和冻融循环试验、扫描电镜(SEM)、X射线衍射(XRD)、傅立叶红外光谱(FTIR)和压汞(MIP)测试探究了工业固废-水泥固化腐殖土的三维力学特性、耐久性能及微观机制。试验结果表明:随着P_(o-b)(即工业固废替代水泥的比率)的增加,试样偏应力与轴向应变的关系逐渐由应变软化向应变硬化过渡。三元工业固废的适当掺入(P_(o-b)为25%~50%)有利于减缓干湿循环作用下工业固废-水泥固化腐殖土试样的劣化速率,而纯水泥固化腐殖土试样表现出相对优异的极限偏应力和抗冻性。微观结构分析表明大量钙矾石晶体和C―(A)―S―H凝胶等产物增强了腐殖土颗粒之间的黏结,同时填充了微观孔隙。研究结果可为垃圾填埋场开采的腐殖土修复及再利用提供理论依据。

深基坑双排微型桩-锚-撑组合支护结构受力与变形特性

为深入研究深厚杂填土地层深基坑微型桩-锚-撑组合支护结构随基坑开挖的受力与变形演化规律,首先,依托青岛市某深基坑工程开展双排微型桩-锚-撑原位试验,分析开挖工况下前、后排桩的桩身弯矩分布规律;然后,结合ABAQUS有限元模拟方法,明确微型桩、预应力锚索与钢支撑之间的协同作用及基坑变形规律;最后,揭示微型桩桩径变化、支护结构作用对桩身受力及基坑变形的影响机制。研究结果表明:增加开挖深度引起桩身正弯矩和负弯矩不断增大,极值点位置不断下移,桩身弯矩整体呈正“S”形分布;开挖至基底,前排桩的桩身反弯点分别位于钢支撑下方0.5 m和开挖面位置,后排桩的桩身反弯点分别位于钢支撑下方0.5 m和开挖面下方1.0 m范围内;基坑开挖竖向影响范围约为1.35H(H为基坑开挖深度),桩径增加近1倍,土体水平位移仅减少约51%,且随桩径继续增加,其对于限制基坑变形效果不显著;相较于桩锚支护结构,桩-锚-撑支护结构作用下,前、后排桩的最大水平位移分别减小34.9%和27.3%,基坑土体的最大水平位移减小46.0%。

FZG齿轮试验机方法在齿轮油上的应用研究

齿轮箱设备所用齿轮油最为关键的性能是承载性能。常规理化测试不足以全面评价齿轮油的承载性能,因此国内外研究机构结合机械设备开发了许多评价齿轮油承载性能的试验方法。研究表明:简单的台架测试方法一般与设备实际工况相关性差,在齿轮试验台上使用指定几何结构的齿轮可以更好地表征齿轮润滑剂的承载性能。文章主要阐述了润滑剂对齿轮不同失效模式的影响,以及如何用适当的测试方法量化,并准确表征润滑剂的承载性能。

水软化作用下页岩微观结构和力学性质演化特性

在雨水或者地下水的浸泡下,页岩力学性质会大幅度降低,容易导致泥石流、隧洞塌陷、滑坡等灾害。以页岩为研究对象,通过微观岩石力学试验研究了水软化作用下页岩的微观结构和力学特性演变规律。研究结果表明:在浸水10 d后,页岩表面粗糙度平均值和最大值分别增至259.1 nm和561.9 nm。页岩主要由石英、绿泥石、伊利石和钠长石组成,其中绿泥石为层状硅酸盐。在水软化作用下绿泥石发生崩解并且释放晶层间膨胀力,导致页岩样品粗糙度增加。随着浸水时间的增加,高、中、低3类强度矿物的弹性模量逐渐减小;低强度矿物的黏聚力呈现下降趋势,从16.7 MPa降低到6.0 MPa,而内摩擦角随浸泡时间轻微波动,其平均值为42.5°。

G.654.E微型光缆在骨干光缆网中的应用研究

G.654.E微型光缆作为一种全新的光缆类型,尚未在国内各大运营商干线光缆网中规模应用。为了验证G.654.E微型光缆的可用性,中国联通组织了相关厂商制作样品并进行测试。深入分析了测试数据,从结构尺寸、PMD参数、机械性能、温度循环特性等7个方面论证了G.654.E微型光缆的性能指标,为该型光缆在中国联通骨干光缆网中的应用提供试验基础,同时也为其他运营商的使用提供参考。

安全帽送风强度对人体呼吸微环境影响研究

为改善作业人员呼吸微环境,对送风式安全帽佩戴者呼吸微环境温度场、速度场和浓度场进行研究。通过假人试验方法测试安全帽在不同送风强度下的人体呼吸微环境温度、速度和粉尘质量浓度,研究人体呼吸微环境温度分布及速度分布规律,阐明安全帽送风强度对人体呼吸微环境中总尘及呼尘降尘效果的影响,进而分析佩戴者对安全帽送风强度的满意程度。结果显示,人体面中部位降温效果优于人体脸颊两侧,其中人体鼻子处降温效果较为明显;安全帽在不同送风强度下对人体呼吸微环境速度场的分布规律一致;当送风强度为Ⅳ级时,人体呼吸微环境内粉尘降尘效率最高,佩戴者满意率最高;人体微环境总尘和呼尘降尘效率分别可达到81.39%和82.89%。研究结果可为改善人体呼吸微环境提供参考。

超薄磨耗层抗滑性能的衰变规律及其影响因素

为了精确评价沥青超薄磨耗层开放交通后抗滑性能衰变过程、机理及影响因素,首先利用弧形模具及其配套的轮碾机来制备弧形超薄磨耗层试件;然后通过驱动轮式加速加载系统对4种级配类型和3个沥青胶结料等级的沥青超薄磨耗层试件进行加速加载试验;最后借助激光纹理扫描仪对一定轮载次数作用后的试件分别进行扫描。结合试验数据分别建立了基于S型函数的沥青超薄磨耗层宏观和微观构造深度衰变模型,以及基于灰色关联分析方法来分析各空隙率和沥青胶结料对抗滑性能的独立和耦合作用。试验研究结果显示:采用驱动轮式加速加载系统结合S型函数模型可以定量地评价和预测沥青超薄磨耗层性能的演变过程;空隙率影响超薄磨耗层宏观和微观构造深度的前期衰减速率,空隙率越大,则超薄磨耗层的宏观和微观构造深度的前期衰减速率越大;宏观构造深度的中后期衰减速率受沥青胶结料等级影响更大,沥青胶结料性能等级越高,则宏观构造深度的中后期衰减速率越慢;空隙率和沥青胶结料等级对超薄磨耗层微观构造深度中后期衰减速率的影响相当。因此,在进行超薄磨耗层抗滑性能设计时,选择大空隙率的开级配超薄磨耗层混合料级配对路面抗滑耐久性是有益的,而沥青胶结料的性能等级则可以根据交通量的大小合理选择。