Effect of current density on corrosion resistance of micro-arc oxide coatings on magnesium alloy

Oxide coatings were prepared on magnesium alloys in electrolyte solution of Na2SiO3 at different current densities(3,4 and 5 A/cm 2 )with micro-arc oxidation process.X-ray diffractometry(XRD)results show that the oxide coatings formed on magnesium alloys are mainly composed of MgO and MgAl2O4 phases;in addition,the content of MgO increases with increasing the current density.The morphology and surface roughness of the coatings were characterized by confocal laser scanning microscopy (CLSM).The results show that the surface roughness(Ra)decreases with increasing the current density.Moreover,the electrochemical corrosion results prove that the MgO coating produced in the electrolyte Na2SiO3 at current density of 5 A/cm 2 shows the best corrosion resistance.

Study on Effect of Welding Speed on Micro Structure and Mechanical Properties of Pulsed Current Micro Plasma Arc Welded Inconel 625 Sheets

Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. Micro Plasma Arc Welding (MPAW) is one of the important arc welding processes commonly using in fabric- cation of Nickel alloys. In the present paper welding of Inconel 625 sheets using pulsed current micro plasma arc weld- ing was discussed. The paper mainly focuses on studying the weld quality characteristics like weld pool geometry pa- rameters, microstructure, grain size, hardness and tensile properties of Pulsed Current Micro Plasma Arc Welded In- conel 625 sheets at different welding speeds. Results reveals that at a welding speed of 260 mm/minute better weld quality characteristics can be obtained.

Study on Weld Quality Characteristics of Pulsed Current Micro Plasma Arc Welding of Inconel625 Sheets

Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. In the present paper an attempt is made to study various weld quality characteristics like weld bead geometry dimensions, micro hardness, microstructure, grain size and tensile properties of Pulsed Current Micro Plasma Welding of Inconel625sheets. Weld joint was prepared by fusing the two parent metals of Inconel625 sheets. Square butt joint is used and welding was carried out using Pulsed DCEN, without filler wire. Peak current, back current, pulse and pulse width are considered as the main influential input variables during the welding.

交流驱动无电学接触GaN基Micro⁃LED器件光电特性

针对Micro‐LED器件微型化带来的尺寸效应、高速巨量转移、发光器件与驱动背板的高精度键合等问题,本文通过金属有机化学气相沉积和原子层沉积技术制备了一种垂直结构的交流驱动无电学接触型GaN基Micro‐LED器件,研究了其光电特性。结果表明,器件电路模型可等效为RC电路,随着交流驱动信号频率的增大,器件等效阻抗先快速减小后趋于稳定。当频率固定时,器件I⁃V特性呈线性关系,器件等效阻抗稳定,器件亮度随着驱动电压增大而增强。当驱动电压固定时,器件在16~22 MHz频率范围内达到最大亮度,且亮度随频率增加呈现先上升后下降趋势;此外,由于回路呈电容特性,无电学接触型Micro‐LED器件存在发光延迟效应和电流超前效应。对比传统Micro‐LED器件,无电学接触型Micro‐LED器件与外部电极无电学接触,在交流驱动条件下实现内部载流子复合发光,有望解决Micro‐LED芯片微型化带来的技术难题。

Compounded Surface Modification of ZK60 Mg Alloy by High Current Pulsed Electron Beam+Micro-plasma Oxidation

In this study, compounded surface modification technology-high current pulsed electron beam （HCPEB） ＋ micro-plasma oxidation （MPO） was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB＋MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB＋MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB＋MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB＋MPO-treated sample. This indicates the great application potential of the HCPEB＋MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.

Application of Hooke &Jeeves Algorithm in Optimizing Fusion Zone Grain Size and Hardness of Pulsed Current Micro Plasma Arc Welded AISI 304L Sheets

AISI 304L is an austenitic Chromium-Nickel stainless steel offering the optimum combination of corrosion resistance, strength and ductility. These attributes make it a favorite for many mechanical components. The paper focuses on developing mathematical models to predict grain size and hardness of pulsed current micro plasma arc welded AISI 304L joints. Four factors, five level, central composite rotatable design matrix is used to optimize the number of experiments. The mathematical models have been developed by Response Surface Method (RSM) and its adequacy is checked by Analysis of Variance (ANOVA) technique. By using the developed mathematical models, grain size and hardness of the weld joints can be predicted with 99% confidence level. The developed mathematical models have been optimized using Hooke and Jeeves algorithm to minimize grain size and maximize the hardness.

Study on Factors Effecting Weld Pool Geometry of Pulsed Current Micro Plasma Arc Welded AISI 304L Austenitic Stainless Steel Sheets Using Statistical Approach

Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters on weld pool geometry namely front width, back width, front height and back height of pulsed current micro plasma arc welded AISI 304L stainless steel sheets was analyzed. Four factors, five levels, central composite design was used to develop mathematical models, incorporating pulsed current parameters and weld pool geometry. The mathematical models have been developed by Response Surface Method. The adequacy of the models was checked by ANOVA technique. Variation of output responses with input process variables are discussed. By using the developed mathematical models, weld pool geometry parameters can be predicted.

Reversal current observed in micro-and submicro-channel flow under non-continuous DC electric field

In practical applications of biochips and bio-sensors, electrokinetic mechanisms are commonly employed to manipulate and analyze the characteristics of single bio-molecules. To accurately and flexibly control the movement of single molecule within micro-/submicro-fluidic channels, the characteristics of current signals at the initial stage of the flow are systematically studied based on a three-electrode system. The current response of micro-/submicro-fluidic channels filled with different electrolyte solutions in non-continuous external electric field are investigated. It is found, there always exists a current reversal phenomenon, which is an inherent property of the current signals in micro/submicro-fluidics Each solution has an individual critical voltage under which the steady current value is equal to zero The interaction between the steady current and external applied voltage follows an exponential function. All these results can be attributed to the overpotentials of the electric double layer on the electrodes. These results are helpful for the design and fabrication of functional micro/nano-scale fluidic sensors and biochips.

微电流对大鹏湾造礁石珊瑚种苗存活率及生长状况的影响

为研究造礁石珊瑚种苗在微电流作用下的存活和生长状况,以深圳市大鹏半岛大鹏湾霜鹿角珊瑚(Acropora pruinosa)、澄黄滨珊瑚(Porites lutea)、盾形陀螺珊瑚(Turbinaria peltata)、十字牡丹珊瑚(Pavona decussata)、膨胀蔷薇珊瑚(Montipora turgescens)为研究对象,在300 d的实验周期内,将电压为6、12、18 V的微电流分别作用于造礁石珊瑚种苗,分析比较不同电压微电流作用下各种造礁石珊瑚种苗的存活率及生长情况。在实验期间海水中pH值、溶解氧和营养盐的变化范围不大,微电流作用后,珊瑚脱落率由3.33%-6.67%降低到0.00%-5.00%,其中澄黄滨珊瑚6、12 V电压实验组的珊瑚脱落率降至0;珊瑚种苗存活率由91.67%-93.33%提升到93.33%-98.33%。不同种类的造礁石珊瑚生长率和生长速度受微电流促进效果不同,霜鹿角珊瑚的生长率最高,十字牡丹珊瑚的生长率最低;当电压为12 V时,微电流对霜鹿角珊瑚、十字牡丹珊瑚、澄黄滨珊瑚、膨胀蔷薇珊瑚、盾形陀螺珊瑚的存活状况和生长速度影响效果最佳。微电流通过促进造礁石珊瑚组织的延伸,降低了造礁石珊瑚种苗培育过程中的脱落率,并提高了造礁石珊瑚种苗的存活率和生长速度。

恒压恒流交互模式对AZ31B镁合金微弧氧化陶瓷膜组织与性能的影响

为探究恒压与恒流相互叠加模式对AZ31B镁合金微弧氧化膜层组织与性能的影响,利用AZ31B镁合金为基材,在电解液和电参数相同的前提下,采用恒流、恒压、先恒流再恒压、先恒压再恒流4种不同电源工作模式在AZ31B镁合金表面制备微弧氧化陶瓷膜。采用扫描电镜(SEM)、电化学工作站、X射线衍射仪(XRD)、高温摩擦磨损机等检测手段,对AZ31B镁合金微弧氧化陶瓷膜层进行测试。结果表明:基材经微弧氧化处理后,表面生成微弧氧化陶瓷膜。在先恒流再恒压(0.7 A/6 min+400 V/4 min)电源模式下制备的微弧氧化陶瓷膜的MgO、MgF_(2)以及Mg_(2)SiO_(4)等强化相的峰值比其他模式下制备的膜层高;膜层表面平整,微孔小且分布均匀,致密性较好,膜层与基体紧密结合;相对于其他模式下的膜层,其被磨穿时长最长,材料的耐磨性得到提升;其腐蚀电位相对于基体,从-1.4974 V增加到-1.3769 V,腐蚀速率从0.0091 mm/a降低到0.0020 mm/a,耐腐蚀性显著提升。

反应堆中子注量率对数测量技术研究

反应堆核仪表系统通过一系列布置在堆外的中子探测器进行反应堆中子注量率测量,为反应堆启动、运行和安全提供初始测量信号。中间量程中子注量率测量范围超过6个量级,同时探测器输出的电流十分微弱,最小达到10pA,对测量技术要求较高。线性电流测量方法会产生由量程切换带来的测量跳变,影响反应堆周期测量稳定性,从而影响反应堆安全。本文详细分析了对数测量原理,利用对数放大电路具有宽动态范围的特点,实现了很宽的动态范围的中子注量率快速测量,避免了量程切换带来的测量数值跳变,提高了中子注量率测量和周期计算的精度。模拟探测器信号输入10pA~100μA的微电流进行测量,结果表明,对于范围达7个数量级的输人电流,测量的相对误差低于0.5%,该方案适用于反应堆中子注量率的中间量程测量。

高频脉冲微TIG焊接电弧基值效应研究

为了探索微TIG焊接的焊接电流下限,研制了一种高频脉冲微TIG焊接电源,利用脉冲基值电弧电特性的改善提高焊接稳定性。通过电弧电流、电压波形,分析了电弧的电压滞后性,探讨了脉冲频率对脉冲电弧基值效应的影响,并进一步对零基值脉冲TIG进行了研究。结果表明,高频脉冲下的微电弧基值电压较稳态电弧大幅下降,更有利于维持微电弧的燃烧;在基值电流为0 A的条件下高频脉冲电弧也可维持燃烧,平均焊接电流可低至0.5 A,极限0基值时间与脉冲电流大小呈正相关。对于微细漆包线和端柱的微型工件连接,零基值脉冲微TIG焊获得了较好的焊接效果。

基于伏秒的反激式光伏微逆变器的仿真研究

针对传统反激式光伏微逆变器因2倍频电压纹波引起的进网电流畸变的问题,提出了1种用于励磁电感电流断续模式下反激式光伏微逆变器的基于伏秒的控制方法.根据谐波抑制策略,对反激式光伏微逆变器进行小信号建模,利用扫频验证建模的正确性.通过推导变压器参数的设计准则,结合变压器参数与输入电压调节范围和损耗的关系对其进行优化设计并进行仿真.结果证明了所提控制方法的准确性,与传统开闭环电流控制方法相比,输出电流的THD更低,达3.783%.

半直驱中速永磁同步发电机轴承发生微电流腐蚀的故障诊断分析

轴承滚道形貌出现“搓衣板”纹路的故障模式是风电机组常见的主要故障之一。针对半直驱中速永磁同步发电机轴承发生微电流腐蚀故障,首先通过在线监测系统采集发电机轴承运行时的振动信号,然后对振动信号故障特征进行提取与诊断分析,研究和复现轴承滚道微电流腐蚀的失效模式和故障发展历程,最后同步验证抑制轴电流的措施的有效性,以此保障风电机组健康可靠地运行。分析表明:该故障风电机组的发电机轴承滚道出现的“搓衣板”纹路并非轴承的主要失效模式,而是轴承滚道发生二次损伤的表现。随着时间推移,轴承滚道出现的损伤(浅坑)纹路逐渐重复叠加并变得更加清晰,说明该发电机的主要失效模式为轴承微电流腐蚀。

微电流电解灭菌抑藻箱在丘陵果园的应用研究

微电流电解灭菌抑藻技术及装置可通过电解时电极上产生的一系列活性物质有效杀灭菌藻,最大限度地避免丘陵果园滴灌系统菌藻堵塞现象。为了寻求一种高效、环保的果园灭菌抑藻方法,文章对微电流电解灭菌抑藻箱进行优化,并通过试验验证其杀灭菌藻的效果。试验结果显示,该装置菌藻杀灭率达91%,持续2 d,且对其他水质指标影响小。多次现场应用检测结果显示,微电流电解灭菌抑藻箱在江西省上犹县和德安县得以推广试用后,对当地典型集蓄雨水的处理能力约为1.5 m^(3)/h,菌藻灭活率达90%以上,降低了丘陵果园滴灌系统菌藻堵塞风险,为山区特色果业发展提供了技术支持。

铜合金接触线夹杂物缺陷的新型涡流检测探索

针对传统涡流检测法在铜合金接触线检测中的不足,提出了一种应用于铜合金接触线生产过程的新型在线涡流检测法,由永磁体和磁场传感器分别代替传统涡流检测法的激励和接收线圈。经实验测试表明,新型涡流检测法原理可行,实验装置简单有效,在现有实验条件下可达到100μm量级的检测精度。

基于新媒体时代高校“微思政”工作现状及策略研究

本文分析和研究了新媒体时代高校微思政的现状和策略。通过对高校“微思政”工作的现状进行分析,发现当前高校“微思政”工作当中,存在“微思政”平台吸引力不足、“微思政”队伍专业化程度不高、教育主客体的媒介素养不一、学生“微思政”的获得感不足、运行机制不健全等问题。对高校“微思政”工作存在问题的原因进行深入的分析,提出深化“微思政”阵地建设、加强“微思政”平台建设、推进“微思政”队伍建设、创新“微思政”工作方式、健全“微思政”工作机制等优化策略,增强高校思想政治教育工作的针对性和实效性。

高亮度Micro-LED外延和芯片制备

微米LED(Micro-LED)是指尺寸在50μm以下,去除外延衬底的LED,相比目前的LCD,OLED显示具有高亮度、高分辨率,低能耗等优势。本文首先介绍了Micro-LED外延和芯片制备中存在的主要问题。接着使用ABC模型以及载流子泄露模型分析了小电流密度下的Micro-LED外量子效率低的原因,给出了目前国际上解决这一问题的主要技术途径。在Micro-LED外延技术上重点介绍了NPSS外延Micro-LED的优势以及目前NPSS的制备、外延GaN的进展情况。在芯片制备上,则介绍了Micro-LED微纳出光结构,多芯片的高色域混光技术,AlInGaP红光,氮化物红光以及量子点激发的红光路线。最后讨论了Micro-LED外延和芯片当前的现状和未来的发展趋势。

面向Micro-LED驱动与检测的单端注入电致发光机理

Micro-LED具有高分辨率、高色域、高稳定性等优点,在近眼显示领域具有广阔的应用前景。然而,Mi-cro-LED存在着巨量电致发光检测和巨量金属键合两大技术瓶颈。本文提出了一种单端载流子注入的Micro-LED工作模式,并制备了一种基于该工作模式的Micro-LED器件,即单注入型Micro-LED。通过实验和仿真研究单注入型Micro-LED的工作过程,探究其工作机理。研究了单注入型Micro-LED在正弦交流电下的电流-驱动电压关系、电流-驱动频率关系、亮度-驱动频率关系,以及能带的周期性变化规律,并提出单注入型Micro-LED的载流子输运模型。最后,展示了单注入模式在垂直结构Micro-LED检测领域的应用,为Micro-LED检测提供了新思路。

无电学接触型氮化镓基Micro-LED器件光电性能

针对传统Micro-LED芯片巨量转移与键合、发光芯片与驱动电极高质量接触等技术难题,本文采用金属有机化合物化学气相沉积和原子层沉积工艺制备无电学接触型氮化镓基Micro-LED器件,研究了器件的伏安特性、亮度-频率特性、发光延迟特性及阻抗-频率特性等光电特性,并分析了器件工作机理。实验结果表明,交流驱动的无电学接触型Micro-LED器件的电流随着频率的增大而增大,且I-V特性呈线性关系。在20V_(pp)的驱动信号下,器件亮度随频率的增大先上升后下降,在频率为25 MHz时,器件亮度达到最大,且发光峰值滞后于电流峰值,说明器件的发光存在延迟。器件的等效阻抗随着频率的增大呈现先减小后趋于稳定的趋势,且器件在频率53 MHz附近出现负电容现象。