Oxide coatings were prepared on magnesium alloys in electrolyte solution of Na2SiO3 at different current densities(3,4 and 5 A/cm 2 )with micro-arc oxidation process.X-ray diffractometry(XRD)results show that the oxid...Oxide coatings were prepared on magnesium alloys in electrolyte solution of Na2SiO3 at different current densities(3,4 and 5 A/cm 2 )with micro-arc oxidation process.X-ray diffractometry(XRD)results show that the oxide coatings formed on magnesium alloys are mainly composed of MgO and MgAl2O4 phases;in addition,the content of MgO increases with increasing the current density.The morphology and surface roughness of the coatings were characterized by confocal laser scanning microscopy (CLSM).The results show that the surface roughness(Ra)decreases with increasing the current density.Moreover,the electrochemical corrosion results prove that the MgO coating produced in the electrolyte Na2SiO3 at current density of 5 A/cm 2 shows the best corrosion resistance.展开更多
Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aeros...Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. Micro Plasma Arc Welding (MPAW) is one of the important arc welding processes commonly using in fabric- cation of Nickel alloys. In the present paper welding of Inconel 625 sheets using pulsed current micro plasma arc weld- ing was discussed. The paper mainly focuses on studying the weld quality characteristics like weld pool geometry pa- rameters, microstructure, grain size, hardness and tensile properties of Pulsed Current Micro Plasma Arc Welded In- conel 625 sheets at different welding speeds. Results reveals that at a welding speed of 260 mm/minute better weld quality characteristics can be obtained.展开更多
Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aeros...Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. In the present paper an attempt is made to study various weld quality characteristics like weld bead geometry dimensions, micro hardness, microstructure, grain size and tensile properties of Pulsed Current Micro Plasma Welding of Inconel625sheets. Weld joint was prepared by fusing the two parent metals of Inconel625 sheets. Square butt joint is used and welding was carried out using Pulsed DCEN, without filler wire. Peak current, back current, pulse and pulse width are considered as the main influential input variables during the welding.展开更多
In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of...In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB+MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB+MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB+MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB+MPO-treated sample. This indicates the great application potential of the HCPEB+MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.展开更多
AISI 304L is an austenitic Chromium-Nickel stainless steel offering the optimum combination of corrosion resistance, strength and ductility. These attributes make it a favorite for many mechanical components. The pape...AISI 304L is an austenitic Chromium-Nickel stainless steel offering the optimum combination of corrosion resistance, strength and ductility. These attributes make it a favorite for many mechanical components. The paper focuses on developing mathematical models to predict grain size and hardness of pulsed current micro plasma arc welded AISI 304L joints. Four factors, five level, central composite rotatable design matrix is used to optimize the number of experiments. The mathematical models have been developed by Response Surface Method (RSM) and its adequacy is checked by Analysis of Variance (ANOVA) technique. By using the developed mathematical models, grain size and hardness of the weld joints can be predicted with 99% confidence level. The developed mathematical models have been optimized using Hooke and Jeeves algorithm to minimize grain size and maximize the hardness.展开更多
Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters o...Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters on weld pool geometry namely front width, back width, front height and back height of pulsed current micro plasma arc welded AISI 304L stainless steel sheets was analyzed. Four factors, five levels, central composite design was used to develop mathematical models, incorporating pulsed current parameters and weld pool geometry. The mathematical models have been developed by Response Surface Method. The adequacy of the models was checked by ANOVA technique. Variation of output responses with input process variables are discussed. By using the developed mathematical models, weld pool geometry parameters can be predicted.展开更多
In practical applications of biochips and bio-sensors, electrokinetic mechanisms are commonly employed to manipulate and analyze the characteristics of single bio-molecules. To accurately and flexibly control the move...In practical applications of biochips and bio-sensors, electrokinetic mechanisms are commonly employed to manipulate and analyze the characteristics of single bio-molecules. To accurately and flexibly control the movement of single molecule within micro-/submicro-fluidic channels, the characteristics of current signals at the initial stage of the flow are systematically studied based on a three-electrode system. The current response of micro-/submicro-fluidic channels filled with different electrolyte solutions in non-continuous external electric field are investigated. It is found, there always exists a current reversal phenomenon, which is an inherent property of the current signals in micro/submicro-fluidics Each solution has an individual critical voltage under which the steady current value is equal to zero The interaction between the steady current and external applied voltage follows an exponential function. All these results can be attributed to the overpotentials of the electric double layer on the electrodes. These results are helpful for the design and fabrication of functional micro/nano-scale fluidic sensors and biochips.展开更多
基金Project(20080505)supported by Science and Technology Department of Jilin Province,China
文摘Oxide coatings were prepared on magnesium alloys in electrolyte solution of Na2SiO3 at different current densities(3,4 and 5 A/cm 2 )with micro-arc oxidation process.X-ray diffractometry(XRD)results show that the oxide coatings formed on magnesium alloys are mainly composed of MgO and MgAl2O4 phases;in addition,the content of MgO increases with increasing the current density.The morphology and surface roughness of the coatings were characterized by confocal laser scanning microscopy (CLSM).The results show that the surface roughness(Ra)decreases with increasing the current density.Moreover,the electrochemical corrosion results prove that the MgO coating produced in the electrolyte Na2SiO3 at current density of 5 A/cm 2 shows the best corrosion resistance.
文摘Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. Micro Plasma Arc Welding (MPAW) is one of the important arc welding processes commonly using in fabric- cation of Nickel alloys. In the present paper welding of Inconel 625 sheets using pulsed current micro plasma arc weld- ing was discussed. The paper mainly focuses on studying the weld quality characteristics like weld pool geometry pa- rameters, microstructure, grain size, hardness and tensile properties of Pulsed Current Micro Plasma Arc Welded In- conel 625 sheets at different welding speeds. Results reveals that at a welding speed of 260 mm/minute better weld quality characteristics can be obtained.
文摘Nickel alloys had gathered wide acceptance in the fabrication of components which require high temperature resistance and corrosion resistance, such as metallic bellows used in expansion joints used in aircraft, aerospace and petroleum industry. In the present paper an attempt is made to study various weld quality characteristics like weld bead geometry dimensions, micro hardness, microstructure, grain size and tensile properties of Pulsed Current Micro Plasma Welding of Inconel625sheets. Weld joint was prepared by fusing the two parent metals of Inconel625 sheets. Square butt joint is used and welding was carried out using Pulsed DCEN, without filler wire. Peak current, back current, pulse and pulse width are considered as the main influential input variables during the welding.
基金supported by Liaoning BaiQianWan Talents Program of China (No. 2008921028)Doctoral Fund of Ministry of Education of China (No. 200801451082)
文摘In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB+MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB+MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB+MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB+MPO-treated sample. This indicates the great application potential of the HCPEB+MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.
文摘AISI 304L is an austenitic Chromium-Nickel stainless steel offering the optimum combination of corrosion resistance, strength and ductility. These attributes make it a favorite for many mechanical components. The paper focuses on developing mathematical models to predict grain size and hardness of pulsed current micro plasma arc welded AISI 304L joints. Four factors, five level, central composite rotatable design matrix is used to optimize the number of experiments. The mathematical models have been developed by Response Surface Method (RSM) and its adequacy is checked by Analysis of Variance (ANOVA) technique. By using the developed mathematical models, grain size and hardness of the weld joints can be predicted with 99% confidence level. The developed mathematical models have been optimized using Hooke and Jeeves algorithm to minimize grain size and maximize the hardness.
文摘Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters on weld pool geometry namely front width, back width, front height and back height of pulsed current micro plasma arc welded AISI 304L stainless steel sheets was analyzed. Four factors, five levels, central composite design was used to develop mathematical models, incorporating pulsed current parameters and weld pool geometry. The mathematical models have been developed by Response Surface Method. The adequacy of the models was checked by ANOVA technique. Variation of output responses with input process variables are discussed. By using the developed mathematical models, weld pool geometry parameters can be predicted.
基金supported by the National Natural Science Foundation of China(Grant Nos.61378083 and 11672229)the International Cooperation Foundation of the National Science and Technology Major Project of the Ministry of Science and Technology of China(Grant No.2011DFA12220)+2 种基金the Major Research Plan of the National Natural Science Foundation of China(Grant No.91123030)the Natural Science Foundation of Shaanxi Province of China(Grant Nos.2010JS110,14JS106,14JS107,and 2013SZS03-Z01)the Natural Science Basic Research Program of Shaanxi Province-Major Basic Research Project(Grant No.2016ZDJC-15)
文摘In practical applications of biochips and bio-sensors, electrokinetic mechanisms are commonly employed to manipulate and analyze the characteristics of single bio-molecules. To accurately and flexibly control the movement of single molecule within micro-/submicro-fluidic channels, the characteristics of current signals at the initial stage of the flow are systematically studied based on a three-electrode system. The current response of micro-/submicro-fluidic channels filled with different electrolyte solutions in non-continuous external electric field are investigated. It is found, there always exists a current reversal phenomenon, which is an inherent property of the current signals in micro/submicro-fluidics Each solution has an individual critical voltage under which the steady current value is equal to zero The interaction between the steady current and external applied voltage follows an exponential function. All these results can be attributed to the overpotentials of the electric double layer on the electrodes. These results are helpful for the design and fabrication of functional micro/nano-scale fluidic sensors and biochips.