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Archean Basement and a Paleoproterozoic Collision Orogen in the Huoqiu Area at the Southeastern Margin of North China Craton: Evidence from Sensitive High Resolution Ion Micro-Probe U-Pb Zircon Geochronology 被引量:37
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作者 WAN Yusheng DONG Chunyan WANG Wei XIE Hangqiang LIU Dunyi 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2010年第1期91-104,共14页
This paper reports sensitive high resolution ion micro-probe U-Pb zircon ages for the "Huoqiu Group" and granitoids of the Early Precambrian basement in the Huoqiu area, southeastern margin of the North China Craton... This paper reports sensitive high resolution ion micro-probe U-Pb zircon ages for the "Huoqiu Group" and granitoids of the Early Precambrian basement in the Huoqiu area, southeastern margin of the North China Craton. The "Huoqiu Group" is similar in rock association and metamorphism to the khondalite series, apart from it containing considerable amounts of banded iron formation. All detrital zircons from the "Huoqiu Group" meta-sedimentary rocks are 3.0 Ga and 2.75 Ga, without any 2.5 Ga and younger ones, as is commonly found in Paleoproterozoic khondalite series in other areas of the North China Craton. In the Huoqiu area, 2.75 Ga and 2.56 Ga granitoids have also been identified. This basement assemblage underwent strong metamorphism during the late Paleoproterozoic (-1.84 Ga) tectonothermal event that is widely developed in the North China Craton. Thus the formation time of the "Huoqiu Group" can be constrained between 2.75 and 1.84 Ga in terms of detrital and metamorphic zircon ages. It is considered, combined with regional data, that there may be a Paleoproterozoic collision orogen extending in a NWW-SEE direction to the southern margin of the North China Craton. 展开更多
关键词 khondalite series trondhjemite-tonalite-granodiorite sensitive high resolution ion micro-probe U-Pb dating ARCHEAN PALEOPROTEROZOIC collision orogen North China Craton
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Endoscopic mucosal resection for rectal carcinoids under micro-probe ultrasound guidance 被引量:6
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作者 Fu-Run Zhou Liu-Ye Huang Cheng-Rong Wu 《World Journal of Gastroenterology》 SCIE CAS 2013年第16期2555-2559,共5页
AIM: To assess the therapeutic value of endoscopic mucosal resection (EMR) under micro-probe ultrasound guidance for rectal carcinoids less than 1 cm in diameter. METHODS: Twenty-one patients pathologically diagnosed ... AIM: To assess the therapeutic value of endoscopic mucosal resection (EMR) under micro-probe ultrasound guidance for rectal carcinoids less than 1 cm in diameter. METHODS: Twenty-one patients pathologically diagnosed with rectal carcinoids following colonoscopy in our hospital from January 2007 to November 2012 were included in this study. The patients consisted of 14 men and 7 women, with a mean age of 52.3 ± 12.2 years (range: 36-72 years). The patients with submucosal tumors less than 1 cm in diameter arising from the rectal and muscularis mucosa detected by micro-probe ultrasound were treated with EMR and followed up with conventional endoscopy and micro-probe ultrasound. RESULTS: All of the 21 tumors were confirmed by micro-probe ultrasound as uniform hypoechoic masses originating from the rectal and muscularis mucosa, without invasion of muscularis propria and vessels, and less than 1 cm in diameter. EMR was successfully completed without bleeding, perforation or other complications. The resected specimens were immunohistochemically confirmed to be carcinoids. Patients were followed up for one to two years, and no tumor recurrence was reported. CONCLUSION: EMR is a safe and effective treatment for rectal carcinoids less than 1 cm in diameter. 展开更多
关键词 micro-probe ultrasound ENDOSCOPIC MUCOSAL resection Rectal CARCINOID ENDOSCOPIC SUBMUCOSAL dissection SUBMUCOSAL tumors
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Hydrogen isotope composition of mantle-derived mica megacryst from ion micro probe analysis 被引量:2
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作者 夏群科 陈道公 支霞臣 《Science China Earth Sciences》 SCIE EI CAS 1999年第4期392-398,共7页
The hydrogen isotope composition of a mantle-derived mica megacryst from Cenozoic basanite from NUshan, Anhui Province has been determined by ion micro probe. The results demonstrate that δD and water content of the ... The hydrogen isotope composition of a mantle-derived mica megacryst from Cenozoic basanite from NUshan, Anhui Province has been determined by ion micro probe. The results demonstrate that δD and water content of the megacryst were heterogeneous on the micro scale, which resulted from reaction with meteoric water after being brought to the surface. The primary δD of mica megacrysts was about-23‰, suggesting the recycled crustal materials in its source. By combining these values with those of other researchers, it is believed that the hydrogen isotope composition of the mantle is heterogeneous at least on the large scale. 展开更多
关键词 MICA MEGACRYST hydrogen isotope ION micro probe.
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Development of MEMS-based micro capacitive tactile probe
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作者 雷李华 李源 +4 位作者 范国芳 吴俊杰 简黎 蔡潇雨 李同保 《Chinese Physics B》 SCIE EI CAS CSCD 2014年第11期646-650,共5页
In this paper, a micro capacitive sensor with nanometer resolution is presented for ultra-precision measurement of micro components, which is fabricated by the MEMS (micro electromechanical systems) non-silicon tech... In this paper, a micro capacitive sensor with nanometer resolution is presented for ultra-precision measurement of micro components, which is fabricated by the MEMS (micro electromechanical systems) non-silicon technique. Based on the sensor, a micro capacitive tactile probe is constructed by stylus assembly and packaging design for dimension metrology on micro/nano scale, in which a data acquiring system is developed with AD7747. Some measurements of the micro capacitive tactile probe are performed on a nano positioning and measuring machine (NMM). The measurement results show good linearity and hysteresis with a range of 11.6 μm and resolution of better than 5 nm. Hence, the micro capacitive tactile probe can be integrated on NMM to realize measurement of micro structures with nanometer accuracy. 展开更多
关键词 micro tactile probe micro capacitive sensor MEMS nano measuring machine
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碳酸盐岩微观测试技术对比与应用——以济阳坳陷乐安油田潜山为例
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作者 吴兆徽 刘显太 +1 位作者 杜玉山 吴颖昊 《吉林大学学报(地球科学版)》 CAS CSCD 北大核心 2024年第5期1519-1529,共11页
微观测试结果能反映很多油藏信息。目前关于微孔缝的镜下测试技术不断丰富,但仍缺少对微孔缝最全面的微观分析。为了便于对比各类测试技术,以济阳坳陷乐安油田草桥潜山区域为典型代表实例,先采用不同的精细微观专项测试技术对孔缝储集... 微观测试结果能反映很多油藏信息。目前关于微孔缝的镜下测试技术不断丰富,但仍缺少对微孔缝最全面的微观分析。为了便于对比各类测试技术,以济阳坳陷乐安油田草桥潜山区域为典型代表实例,先采用不同的精细微观专项测试技术对孔缝储集空间特征进行分析,具体包括微溶孔电子探针成分分析、扫描电镜、薄片和阴极发光测试等技术,然后总结了通过各种不同的微观测试技术观察到的现象及规律。具体结果和得出认识如下:通过电子探针成分分析技术,能够分辨出灰岩微溶孔内诸如有机质、方解石、黄铁矿、白云石、石膏等成分;薄片内可见灰岩含油段砾间砾内孔洞发育,溶蚀孔洞边部有轻微方解石化;通过扫描电镜分析,能够分辨出代表区块的白云岩结晶孔比灰岩溶蚀孔大两个以上数量级,能通过晶间孔或溶蚀孔推断岩石的脆性以及是否易于压裂;通过岩样阴极发光测试,能够区分出共有几期成分不同的孔洞充填物;通过扫描电镜和压汞都可以得到孔喉大小,比较两项技术,扫描电镜得到的是局部纳米级的孔喉直径,而压汞测试得到的是单块样品微米级孔喉半径。从应用对象来看,前者适合对应到矿物的孔喉,后者更适合开发区块的孔喉对比研究。 展开更多
关键词 碳酸盐岩 微溶孔 电子探针 扫描电镜 阴极发光 薄片 乐安油田
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AlSc15中间合金中Al_(3)Sc金属间化合物的电化学行为及对局部腐蚀的影响
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作者 蒋伟 高坤元 +6 位作者 胡秀华 文胜平 黄晖 吴晓蓝 魏午 聂祚仁 启世亮 《轻合金加工技术》 CAS 2024年第2期54-58,共5页
将过共晶AlSc15合金加热至液态,以10℃/h速率冷却得到毫米级尺寸的Al_(3)Sc金属间化合物。利用微区电化学和扫描开尔文探针力显微镜(SKPFM)研究了Al_(3)Sc金属间化合物在不同pH值的0.1 mol/L NaCl溶液中的电化学特征及对局部腐蚀敏感性... 将过共晶AlSc15合金加热至液态,以10℃/h速率冷却得到毫米级尺寸的Al_(3)Sc金属间化合物。利用微区电化学和扫描开尔文探针力显微镜(SKPFM)研究了Al_(3)Sc金属间化合物在不同pH值的0.1 mol/L NaCl溶液中的电化学特征及对局部腐蚀敏感性的影响。结果表明,Al_(3)Sc金属间化合物存在自钝化现象,且在碱性环境中有明显的维钝区域;随着pH值的增加,Al_(3)Sc腐蚀电位逐渐降低,在中性和碱性条件下的腐蚀速率明显低于酸性条件下的;Al_(3)Sc金属间化合物与周围铝基体之间的伏打电位差约为40 mV,在铝合金中可能作为较弱的局部阴极,对电偶腐蚀的影响不大。 展开更多
关键词 Al_(3)Sc金属间化合物 微电化学技术 扫描开尔文 局部腐蚀
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1-[^(18)F]氟代乙基吲哚丙酸作为PET显像剂可行性的初步研究
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作者 董伟璇 秦开心 +3 位作者 沈聪 施冬梅 胡文豪 段小艺 《西安交通大学学报(医学版)》 CAS CSCD 北大核心 2024年第6期1020-1026,共7页
目的吲哚丙酸在肿瘤免疫检查点阻断治疗中有关键作用,本研究拟设计合成^(18)F-标记的吲哚丙酸即1-[^(18)F]氟代乙基-吲哚丙酸(1-[^(18)F]-IPA),并对其作为肿瘤PET显像剂进行初步研究。方法前体1-(2-对甲苯磺酸氧乙基)-吲哚丙酸甲酯与^(1... 目的吲哚丙酸在肿瘤免疫检查点阻断治疗中有关键作用,本研究拟设计合成^(18)F-标记的吲哚丙酸即1-[^(18)F]氟代乙基-吲哚丙酸(1-[^(18)F]-IPA),并对其作为肿瘤PET显像剂进行初步研究。方法前体1-(2-对甲苯磺酸氧乙基)-吲哚丙酸甲酯与^(18)F-发生亲核取代反应,粗产品经高效液相色谱法分离纯化并收集中间体,最后水解得1-[^(18)F]-IPA。目测产品的澄清度,精密试纸测定pH值,高效液相色谱检测放射化学纯度和稳定性。ICR健康小鼠尾静脉注射1-[^(18)F]-IPA(0.2 mL,7 MBq),于5、15、25、45、75、120 min各不同时间点处死并解剖,测定1-[^(18)F]-IPA在正常小鼠体内的生物学分布;荷BxPC-3裸鼠行micro-PET/CT显像并进行图像分析。组织器官不同时间点生物学分布的比较采用Student t检验。结果1-[^(18)F]-IPA总制备时间约35~40 min,放射化学产率(45±5)%,放射化学纯度>95%。产品溶液澄清无颗粒,pH值约6.5,体内外稳定性好。于各时间点处死ICR健康小鼠并解剖后测定1-[^(18)F]-IPA在正常小鼠体内的生物学分布,结果表明除外脑组织,在ICR健康小鼠全身各主要脏器均有1-[^(18)F]-IPA的一定摄取,以肝脏、胆囊以及肾脏摄取最明显,胆囊处随时间推移放射性逐渐增高,在120 min时达到(39.86±6.56)%ID/g,骨摄取随时间无明显变化。Micro-PET/CT表明,荷BxPC-3裸鼠在注射1-[^(18)F]-IPA 30 min后的BxPC-3肿瘤处有一定量放射性摄取,但并不明显,此时最大标准摄取值(SUVmax)约为55.18±14.62。这与生物分布结果一致,脑在各时间点摄取均较低。结论1-[^(18)F]-IPA合成时间短、产率高,有望成为一种探查色氨酸吲哚代谢途径以及进一步揭示肿瘤免疫抵抗的工具。 展开更多
关键词 1-[^(18)F]氟代乙基吲哚丙酸(1-[^(18)F]-IPA) 放射化学 小动物PET/CT 分子探针
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电子探针微区分析在石油炼制与化工催化剂研究中的应用
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作者 何文会 刁玉霞 +3 位作者 邱丽美 向彦娟 郑爱国 徐广通 《石油学报(石油加工)》 EI CAS CSCD 北大核心 2024年第6期1783-1794,共12页
电子探针微区分析(EPMA)方法在炼油化工催化材料研发与催化剂失活研究中发挥着重要的作用。简述该方法的工作原理及检测优势,根据该方法在炼油化工催化材料表征时面临的样品制备方法困境,概述适用于炼油化工催化材料的EPMA样品制备方法... 电子探针微区分析(EPMA)方法在炼油化工催化材料研发与催化剂失活研究中发挥着重要的作用。简述该方法的工作原理及检测优势,根据该方法在炼油化工催化材料表征时面临的样品制备方法困境,概述适用于炼油化工催化材料的EPMA样品制备方法,并介绍EPMA技术参数的优化原则与经验参数。综述EPMA在不同炼油化工催化材料的研究工作,主要包括分子筛催化剂、催化裂化催化剂、加氢催化剂及重整催化剂在研发过程及失活剖析过程中截面微区元素探测与分布信息,对于催化剂的设计与性质优化、催化剂的装填以及反应器的操作,乃至寻找缓解催化剂失活的策略等都具有重要意义。最后,对该方法在未来发展方向的应用进行展望。 展开更多
关键词 电子探针 炼油化工催化材料 样品制备方法 微区元素分析
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Ball Tips of Micro/Nano Probing Systems:A Review 被引量:1
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作者 Ruijun LI Chen CHEN +4 位作者 Dandong LI Kuang-Chao FAN Zhenying CHENG Qiangxian HUANG Xueming DANG 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2017年第2期222-230,共9页
To satisfy the measuring demands for the micro components of the industry, micro/nano probing systems with various ball tips have been developed. However, most of them cannot be used to measure the real micro geometri... To satisfy the measuring demands for the micro components of the industry, micro/nano probing systems with various ball tips have been developed. However, most of them cannot be used to measure the real micro geometrical features high precisely because the parameters of the ball tips are not appropriate. The ball tips with a diameter of less than 100 μm, a sphericity and eccentricity of far less than 1 μm are required urgently. A review on the state-of-the-art of ball tips of micro/nano probing systems is presented. The material characteristics and geometric parameters of now available ball tips are introduced sepa- rately. The existing fabrication methods for the ball tips are demonstrated and summarized. The ball tips' future trends, which are smaller diameter, better sphericity and smaller eccentricity, are proposed in view of the practical requirements of high-precision measurement for micro geometrical features. Some challenges have to be faced in future, such as the promotion and high-precision measurement for the small ball tip's sphericity and eccentricity. Fusion method without the gravity effect when the molten ball tip solidifying is a more suitable way to fabricate a small diameter ball tip together with a shaft. 展开更多
关键词 Ball tip · probe - micro/nano CMMs · microcomponents
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基于大数据聚类的飞行探测器复合跟踪控制系统设计
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作者 周怡伶 陶金 王建刚 《计算机测量与控制》 2024年第8期161-167,180,共8页
飞行探测器会受到气象条件、磁场等环境干扰,影响探测器的运动轨迹,进而影响跟踪精度;为实现对飞行探测器运动轨迹的实时跟踪与控制,设计基于大数据聚类的飞行探测器复合跟踪控制系统;在复合框架体系中,设置主控芯片、伺服驱动设备两类... 飞行探测器会受到气象条件、磁场等环境干扰,影响探测器的运动轨迹,进而影响跟踪精度;为实现对飞行探测器运动轨迹的实时跟踪与控制,设计基于大数据聚类的飞行探测器复合跟踪控制系统;在复合框架体系中,设置主控芯片、伺服驱动设备两类应用结构,并联合信标机元件,调节微惯性传感器器件的实时连接状态,完成飞行探测器复合跟踪控制系统的硬件设计;完善大数据聚类算法,根据跟踪路径节点标定结果,定义具体的复合跟踪坐标系,完成对飞行探测器复合跟踪的实时控制建模,结合相关硬件,实现基于大数据聚类的飞行探测器复合跟踪控制系统的设计;实验结果表明,所设计系统在跟踪1号、2号目标的跟踪准确率平均值分别为96.5%、97.0%,对目标跟踪时延的平均值为0.9 ms,可以保证基站主机对飞行探测器运动轨迹的实时控制能力。 展开更多
关键词 大数据聚类 飞行探测器 跟踪控制 伺服驱动设备 信标机 微惯性传感器 路径节点 复合坐标系
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New Measuring Temperature Setup with Optical Probe
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作者 HOU Peiguo, LIU Jianming(Yanshan University, Qinbuangdao 066004, CHN ) 《Semiconductor Photonics and Technology》 CAS 1997年第1期71-73,共3页
Abstract: A new setup of measuring temperature is developed, which the probe is a micro- power consumptive one with CMOS circuit and is driven by optical power. For transmitting the measured signal and optical power s... Abstract: A new setup of measuring temperature is developed, which the probe is a micro- power consumptive one with CMOS circuit and is driven by optical power. For transmitting the measured signal and optical power signal in a long distance, the fiber technology is applied in this setup. 展开更多
关键词 micro - power Consumptive probe Optical Fiber Transmission Sen-sors Temperature Measurement
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中国首次发现的氟闪叶石矿物学特征 被引量:1
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作者 葛祥坤 李婷 +2 位作者 范光 邰宗尧 沈敢富 《岩石矿物学杂志》 CAS CSCD 北大核心 2023年第4期568-576,共9页
闪叶石族矿物是富含Sr、Na、Ca和Ba等的钛硅酸盐矿物的总称,迄今共有19个矿物种,其中的氟闪叶石矿物首次发现于巴西Serrote山碱性岩中。本文利用电子探针和X射线衍射仪等分析测试手段,从化学成分和晶体结构等方面对产出于中国辽宁赛马... 闪叶石族矿物是富含Sr、Na、Ca和Ba等的钛硅酸盐矿物的总称,迄今共有19个矿物种,其中的氟闪叶石矿物首次发现于巴西Serrote山碱性岩中。本文利用电子探针和X射线衍射仪等分析测试手段,从化学成分和晶体结构等方面对产出于中国辽宁赛马碱性岩体中的闪叶石族矿物进行了详细的矿物学特征研究,发现其中常呈柱状、针状和纤维状集合体产出的闪叶石的晶体化学式为(Sr_(1.00)Na_(1.00))_(Σ2.00)Ti_(2)(Na_(1.98)Sr_(_(0.33))Mn_(0.26)K_(0.12)Mg_(0.10)Ca_(0.09)Ba_(0.05))_(Σ2.93)(Ti_(0.69)Fe_(0.33)^(3+)Al_(0.02))_(Σ1.04)(Si_(3.80)O_(14))O_(2)(F_(1.16)OH_(0.84))_(Σ2.00),属于单斜晶系,空间群为C2/m,晶胞参数a=19.2719(8)Å,b=7.0779(3)Å,c=5.3882(2)Å,β=96.780(2)°,V=729.84(5)Å^(3),Z=2。上述矿物学特征均与巴西发现的新矿物氟闪叶石的矿物学特征一致,表明赛马碱性岩体产出的氟闪叶石堪称该矿物种在中国的首次发现。不仅如此,赛马碱性岩体也有闪叶石产出,而且,迄今已发现多个新矿物,寓示该岩体仍有良好的新矿物发现前景。 展开更多
关键词 闪叶石族 氟闪叶石 电子探针 X射线衍射仪 赛马碱性岩体
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Web-Based Data Management and Sharing System for Electron Proke Micro-analysis
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作者 HE Yutong TIAN Di +3 位作者 GAO Ranran FAN Runlong YAO Li CHEN Pengfei 《Journal of Donghua University(English Edition)》 EI CAS 2018年第4期315-320,共6页
This paper proposes a useful web-based system for the management and sharing of electron probe micro-analysis( EPMA)data in geology. A new web-based architecture that integrates the management and sharing functions is... This paper proposes a useful web-based system for the management and sharing of electron probe micro-analysis( EPMA)data in geology. A new web-based architecture that integrates the management and sharing functions is developed and implemented.Earth scientists can utilize this system to not only manage their data,but also easily communicate and share it with other researchers.Data query methods provide the core functionality of the proposed management and sharing modules. The modules in this system have been developed using cloud GIS technologies,which help achieve real-time spatial area retrieval on a map. The system has been tested by approximately 263 users at Jilin University and Beijing SHRIMP Center. A survey was conducted among these users to estimate the usability of the primary functions of the system,and the assessment result is summarized and presented. 展开更多
关键词 ELECTRON probe micro-analysis ( EPMA ) DATA management DATA sharing WEB-BASED architecture DATA query GIS
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微阴极电弧推力器羽流探针诊断研究 被引量:2
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作者 王帅 刘向阳 +4 位作者 赵子靖 郭浩然 耿金越 沈岩 王宁飞 《中国空间科学技术》 CSCD 北大核心 2023年第2期47-54,共8页
微阴极电弧推力器(micro-cathode arc thruster,μCAT)具备功率低和结构简单的特点,能够满足微纳卫星的任务需求,具有良好的发展前景。μCAT羽流的诊断可以揭示推力器的加速机理,对提高其性能具有重要意义。利用朗缪尔三探针对μCAT羽... 微阴极电弧推力器(micro-cathode arc thruster,μCAT)具备功率低和结构简单的特点,能够满足微纳卫星的任务需求,具有良好的发展前景。μCAT羽流的诊断可以揭示推力器的加速机理,对提高其性能具有重要意义。利用朗缪尔三探针对μCAT羽流进行诊断,得到了μCAT羽流不同位置的电子温度、电子密度和离子速度等羽流特性,研究了外加磁场、充电时间和阴极材料对羽流特性的影响。研究结果表明,μCAT放电初期产生的等离子体电子温度较高,密度较大;随着等离子体向下游运动,电子温度和电子密度降低,离子速度增大;外加磁场的磁感应强度越强,电子温度和离子速度越高,电子密度有所降低;磁场位置适当向推力器下游平移,能够有效提高推力器中轴线的电子密度;μCAT充电时间越长,电子温度、电子密度和离子速度越大;相比于CuW和AgW阴极,Ti阴极羽流的电子温度更高,电子密度更低。 展开更多
关键词 微阴极电弧推力器 羽流诊断 朗缪尔探针 等离子体特性 离子速度
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电子探针的研制现状与分析 被引量:1
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作者 葛祥坤 《山东国土资源》 2023年第9期17-22,共6页
电子探针分析具有微区、原位、无损、分析速度快、分析元素范围广、定量分析准确度高等特点,是固体物质微区原位元素组成定量分析的主要技术手段,广泛应用于材料、地质、冶金、矿产、电子、生物、考古、空间科学等领域,但我国的电子探... 电子探针分析具有微区、原位、无损、分析速度快、分析元素范围广、定量分析准确度高等特点,是固体物质微区原位元素组成定量分析的主要技术手段,广泛应用于材料、地质、冶金、矿产、电子、生物、考古、空间科学等领域,但我国的电子探针长期依赖于进口,存在着“卡脖子”的风险。本文回顾了电子探针的研制历史,梳理了国内外电子探针的研制现状,总结了我国电子探针研制存在的问题和短板,指出了电子探针研制的发展趋势,以期为我国电子探针的研制提供借鉴。 展开更多
关键词 电子探针 研制现状 日本电子 日本岛津 法国卡梅卡
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光纤预制棒中元素的线分析定量化方法
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作者 李明辉 吴金金 +3 位作者 魏慧欣 郜鲜辉 宋武林 丁雨葵 《理化检验(物理分册)》 CAS 2023年第7期34-38,共5页
采用电子探针显微分析法对光纤预制棒进行元素线分析定量化,光纤预制棒心部Yb和Al等元素的含量较低、基体效应的复杂影响以及测试条件的差异等因素导致线分析定量化结果误差较大。采用多点法的测试结果对光纤预制棒中Yb、Al元素的线分... 采用电子探针显微分析法对光纤预制棒进行元素线分析定量化,光纤预制棒心部Yb和Al等元素的含量较低、基体效应的复杂影响以及测试条件的差异等因素导致线分析定量化结果误差较大。采用多点法的测试结果对光纤预制棒中Yb、Al元素的线分析定量化结果进行校正。结果表明:在两点法的基础上引入修正因子,可以简化测试过程,快速、准确地得到元素线分析定量化结果。 展开更多
关键词 电子探针显微分析 光纤预制棒 线分析定量化 修正因子 基体效应
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Temperature measurement based on radialization power for micro-hotplate 被引量:1
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作者 张彤 漆奇 +3 位作者 刘奎学 刘丽 张蕾 徐宝琨 《中国有色金属学会会刊:英文版》 CSCD 2006年第B02期780-784,共5页
A novel method to measure the temperature on the surface of micro-hotplate was presented. The tiny fiber probe and the optical power meter were employed to measure the sample radialization power. By means of comparing... A novel method to measure the temperature on the surface of micro-hotplate was presented. The tiny fiber probe and the optical power meter were employed to measure the sample radialization power. By means of comparing the relationship between the radialization power and the temperature, sample surface temperature can be discerned accurately. Such an approach has provided more accuracy than traditional temperature measurements. The experimental result based on this method is quite similar to that of simulation by the finite element analysis (FEA) software of Ansys in theory. This measurement is very useful for measuring temperature for these micro samples prone to be untouchable. 展开更多
关键词 气体传感器 微型热盘 辐射功率 温度测量 热分布
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A method for calibrating the confocal volume of a confocal three-dimensional micro-x-ray fluorescence setup
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作者 Peng Zhou Xin-Ran Ma +2 位作者 Shuang Zhang Tian-Xi Sun Zhi-Guo Liu 《Chinese Physics B》 SCIE EI CAS CSCD 2020年第2期190-195,共6页
The measurement of the confocal volume of a confocal three-dimensional micro-x-ray fluorescence(3D-XRF)setup is a key step in the field of confocal 3D-XRF analysis.With the development of x-ray facilities and optical ... The measurement of the confocal volume of a confocal three-dimensional micro-x-ray fluorescence(3D-XRF)setup is a key step in the field of confocal 3D-XRF analysis.With the development of x-ray facilities and optical devices,3D-XRF analysis with a micro confocal volume will create a great potential for 2D and 3D microstructural analysis and accurate quantitative analysis.However,the classic measurement method of scanning metal foils of a certain thickness leads to inaccuracy.A method for calibrating the confocal volume is proposed in this paper.The new method is based on the basic content of the textbook,and the theoretical results and the feasibility are given in detail for the 3D-XRF mono-chromatic x-ray condition and the poly-chromatic x-ray condition.We obtain a set of experimental confirmation using the poly-chromatic x-ray tube in the laboratory.It is proved that the sensitivity factor of the 3D-XRF can be directly and accurately obtained in a real calibration process. 展开更多
关键词 THREE-DIMENSIONAL micro-x-ray fluorescence(3D-XRF) depth analysis CONFOCAL VOLUME probe calibrating
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微型贯入试验与无侧限抗压强度试验结果的对比
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作者 董猛荣 杨俊杰 +3 位作者 阮媚媚 王思雨 孙涛 王子玉 《中国海洋大学学报(自然科学版)》 CAS CSCD 北大核心 2023年第11期140-151,共12页
本文探讨了探头锥尖角度和探头直径对微型贯入试验结果的影响及微型贯入试验结果与无侧限抗压强度试验结果的相关性。结果表明,探头锥尖角度和直径对贯入曲线性状没有影响,即贯入阻力随贯入深度线性增加,达到某一贯入深度时贯入曲线出... 本文探讨了探头锥尖角度和探头直径对微型贯入试验结果的影响及微型贯入试验结果与无侧限抗压强度试验结果的相关性。结果表明,探头锥尖角度和直径对贯入曲线性状没有影响,即贯入阻力随贯入深度线性增加,达到某一贯入深度时贯入曲线出现拐点,之后贯入阻力趋于稳定,定义此时的比贯入阻力为贯入强度。探头锥尖角度越大,达到贯入曲线拐点前贯入阻力随贯入深度增长越快;贯入强度随探头锥尖角度的增加先减小后增大,当锥尖角度为60°时贯入强度最小,锥尖角度为30°、90°和180°时的贯入强度与锥尖角度为60°时贯入强度的关系呈线性关系;探头直径对比贯入曲线的影响可忽略不计,但随着探头直径的增大,贯入强度呈线性减小趋势,探头直径3.4 mm的贯入强度比7.0 mm的贯入强度增大2.5%,比10.0 mm的贯入强度增大5.0%;可用贯入曲线拐点前直线段斜率换算无侧限抗压强度,也可利用贯入强度换算无侧限抗压强度;水泥土强度的形成条件对贯入曲线拐点前直线段斜率及贯入强度与无侧限抗压强度之间的关系没有明显影响。 展开更多
关键词 微型贯入试验 探头锥尖角度 探头直径 贯入强度 无侧限抗压强度
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基于粒子群优化算法的轨迹控制研究
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作者 郭宇祥 高星 《吕梁学院学报》 2023年第2期12-14,共3页
为精确控制加工轨迹从而获得高质量有序的微/纳米结构,本文针对传统算法的不足,对粒子群算法进行优化改进,提出了混合粒子群算法.并通过加工实例验证了该算法加载稳定,优化了轨迹运动时间.
关键词 粒子群算法 探针悬臂 微/纳加工
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