The microstructure transformation and precipitation behavior of nano-carbides in Ti microalloyed steel during isothermal process were studied by a compression test on a Gleeble 3800 thermomechanical simulator and anal...The microstructure transformation and precipitation behavior of nano-carbides in Ti microalloyed steel during isothermal process were studied by a compression test on a Gleeble 3800 thermomechanical simulator and analyzed by optical microscopy,transmission electron microscopy and other methods.The results show thatγ→αphase transformation and TiC precipitation take place in Ti microalloyed steel during the isothermal process,and time–temperature–transformation curve and precipitation–time–temperature(PTT)curve are all of“C”-type.During the isothermal process,the interphase precipitation of TiC mostly occurs at the period of the phase transformation,and the random precipitation of TiC mostly occurs on the ferrite after the phase transformation.The increment in yield strength at the initial stage of isothermal transformation mainly comes from phase transformation strengthening.With the increase in isothermal time,the precipitation hardening effect becomes more important for nucleation and growth of titanium carbides and eventually reaches the maximum value at the precipitation finished point of the PTT curve.展开更多
With the help of solidification kinetics, precipitation and growth of TiNhave been studied theoretically and the effect of cooling rate on the growth of TiN has beendiscussed. Through induction electric furnace experi...With the help of solidification kinetics, precipitation and growth of TiNhave been studied theoretically and the effect of cooling rate on the growth of TiN has beendiscussed. Through induction electric furnace experiment and electroslag remelting experiment withdifferent cooling rates, the distribution and particle size of TiN were investigated. It is provedthat the higher cooling rate is, the smaller the final size of TiN is and the more TiN particles canbe found in the steel. That TiN can restrain the growth of columnar crystal and enhance theproportion of equiaxed crystals to refine solidification structure as the heterogeneous nucleationsites of δ-ferrite is confirmed preliminarily. A new method to reduce macrosegregation incontinuous cast steel is provided.展开更多
With the increase in the content of carbon, nitrogen and titanium in 430 ferritic stainless steel, the refinement of the solidification structure is obvious and the proportion of equiaxed grain increases remarkably as...With the increase in the content of carbon, nitrogen and titanium in 430 ferritic stainless steel, the refinement of the solidification structure is obvious and the proportion of equiaxed grain increases remarkably as well. This is attributed to the increasing role of the inhomogeneous nucleation by TiN particles during solidification. In addition, more fine precipitations of (Ti ,Nb)N are found in steel with increased carbon and nitrogen content.展开更多
The microstructural evolution and precipitation behaviour of Nb–V–Mo and single V containing transformation induced plasticity assisted steels were investigated during thermomechanical processing. A plane strain com...The microstructural evolution and precipitation behaviour of Nb–V–Mo and single V containing transformation induced plasticity assisted steels were investigated during thermomechanical processing. A plane strain compression testing machine was used to simulate the thermomechanical processing. Microstructures were characterised by optical microscopy, scanning-transmission electron microscopy and microanalysis, and X-ray diffraction analysis, and Vickers hardness was obtained from the deformed specimens. The resulting microstructure of both Nb–V–Mo and V steels at room temperature primarily consisted of an acicular/bainitic ferrite, retained austenite and martensite surrounded by allotriomorphic ferrite.The TEM analysis showed that a significant number of Nb(V,Mo)(C,N) precipitates were formed in the microstructure down to the finishing stage in Nb–V–Mo steel(i.e. 830℃). It was also found that the V(C,N)precipitation primarily occurred in both ferrite and deformed austenite below the finishing stage. The results suggested that Nb–Mo additions considerably increased the temperature stability of microalloy precipitates and controlled the microstructural evolution of austenite. However, the microalloy precipitation did not cause a significant precipitation strengthening in both Nb–V–Mo and V steels at room temperature.展开更多
文摘The microstructure transformation and precipitation behavior of nano-carbides in Ti microalloyed steel during isothermal process were studied by a compression test on a Gleeble 3800 thermomechanical simulator and analyzed by optical microscopy,transmission electron microscopy and other methods.The results show thatγ→αphase transformation and TiC precipitation take place in Ti microalloyed steel during the isothermal process,and time–temperature–transformation curve and precipitation–time–temperature(PTT)curve are all of“C”-type.During the isothermal process,the interphase precipitation of TiC mostly occurs at the period of the phase transformation,and the random precipitation of TiC mostly occurs on the ferrite after the phase transformation.The increment in yield strength at the initial stage of isothermal transformation mainly comes from phase transformation strengthening.With the increase in isothermal time,the precipitation hardening effect becomes more important for nucleation and growth of titanium carbides and eventually reaches the maximum value at the precipitation finished point of the PTT curve.
基金This work was financially supported by the National Basic Research on New Generation Steel (973) (No.J1998061511-3)
文摘With the help of solidification kinetics, precipitation and growth of TiNhave been studied theoretically and the effect of cooling rate on the growth of TiN has beendiscussed. Through induction electric furnace experiment and electroslag remelting experiment withdifferent cooling rates, the distribution and particle size of TiN were investigated. It is provedthat the higher cooling rate is, the smaller the final size of TiN is and the more TiN particles canbe found in the steel. That TiN can restrain the growth of columnar crystal and enhance theproportion of equiaxed crystals to refine solidification structure as the heterogeneous nucleationsites of δ-ferrite is confirmed preliminarily. A new method to reduce macrosegregation incontinuous cast steel is provided.
基金this project by both the National Natural Science Foundation of China(NSF 50734002)and Baosteel is fully acknowledged.
文摘With the increase in the content of carbon, nitrogen and titanium in 430 ferritic stainless steel, the refinement of the solidification structure is obvious and the proportion of equiaxed grain increases remarkably as well. This is attributed to the increasing role of the inhomogeneous nucleation by TiN particles during solidification. In addition, more fine precipitations of (Ti ,Nb)N are found in steel with increased carbon and nitrogen content.
文摘The microstructural evolution and precipitation behaviour of Nb–V–Mo and single V containing transformation induced plasticity assisted steels were investigated during thermomechanical processing. A plane strain compression testing machine was used to simulate the thermomechanical processing. Microstructures were characterised by optical microscopy, scanning-transmission electron microscopy and microanalysis, and X-ray diffraction analysis, and Vickers hardness was obtained from the deformed specimens. The resulting microstructure of both Nb–V–Mo and V steels at room temperature primarily consisted of an acicular/bainitic ferrite, retained austenite and martensite surrounded by allotriomorphic ferrite.The TEM analysis showed that a significant number of Nb(V,Mo)(C,N) precipitates were formed in the microstructure down to the finishing stage in Nb–V–Mo steel(i.e. 830℃). It was also found that the V(C,N)precipitation primarily occurred in both ferrite and deformed austenite below the finishing stage. The results suggested that Nb–Mo additions considerably increased the temperature stability of microalloy precipitates and controlled the microstructural evolution of austenite. However, the microalloy precipitation did not cause a significant precipitation strengthening in both Nb–V–Mo and V steels at room temperature.