Effect of microwave modification on tapioca starch at different moisture contents was studied with polarized light microscope. It was observed that loss of birefringence was initiated at hilum of granule. The polariza...Effect of microwave modification on tapioca starch at different moisture contents was studied with polarized light microscope. It was observed that loss of birefringence was initiated at hilum of granule. The polarization cross of most granules had become somewhat unclear, and reduction in clarity of the polarization cross was proportioned with the moisture contents of native starch as modification by microwave. When the moisture contents reached to 35.0%, the polarization cross of most granules was lost, and the critical point of native starch was 30% in microwave modification.展开更多
Modification of metallurgical coke,biomass char and semi-coke was carried out using a microwave device with power of 450-850 W and irradiation time of 6-12 min.The desulfurization rates of three carbon materials befor...Modification of metallurgical coke,biomass char and semi-coke was carried out using a microwave device with power of 450-850 W and irradiation time of 6-12 min.The desulfurization rates of three carbon materials before and after modification were tested.The effects of microwave power and irradiation time on the pore texture and surface chemical characteristics of the three carbon materials were examined by SEM,BET and Fourier transform infrared spectroscopy（FTIR）.The results showed that the specific surface area,total pore volume and pore diameter of biomass char and semi-coke after irradiation decreased slightly.Noteworthily,the pore diameter turned small and the acidic functional groups on their surface decomposed,thereby the basicity of carbon surface increased by microwave modification.The optimal promotion of desulfurization rate of three carbon materials was semi-coke irradiated at 850 W for 9 min and the sulfur dioxide adsorption rate was up to 45%.展开更多
A simple method for the magnetic modification of various types of powdered agglomerate forming dia- magnetic materials was developed. Magnetic iron oxide particles were prepared from ferrous sulfate by microwave assis...A simple method for the magnetic modification of various types of powdered agglomerate forming dia- magnetic materials was developed. Magnetic iron oxide particles were prepared from ferrous sulfate by microwave assisted synthesis. A suspension of the magnetic particles in water soluble organic solvent （methanol, ethanol, propanol, isopropyl alcohol, or acetone） was mixed with the material to be modified and then completely dried at elevated temperature. The magnetically modified materials were found to be stable in water suspension at least for 2 months.展开更多
文摘Effect of microwave modification on tapioca starch at different moisture contents was studied with polarized light microscope. It was observed that loss of birefringence was initiated at hilum of granule. The polarization cross of most granules had become somewhat unclear, and reduction in clarity of the polarization cross was proportioned with the moisture contents of native starch as modification by microwave. When the moisture contents reached to 35.0%, the polarization cross of most granules was lost, and the critical point of native starch was 30% in microwave modification.
基金the National Natural Science Foundation of China(No.51604048)Fund of Chongqing Science and Technology(Nos.cstc2015shmszx20016 and cstc2016shmszx20015)China Postdoctoral Science Foundation(2016M590862)
文摘Modification of metallurgical coke,biomass char and semi-coke was carried out using a microwave device with power of 450-850 W and irradiation time of 6-12 min.The desulfurization rates of three carbon materials before and after modification were tested.The effects of microwave power and irradiation time on the pore texture and surface chemical characteristics of the three carbon materials were examined by SEM,BET and Fourier transform infrared spectroscopy（FTIR）.The results showed that the specific surface area,total pore volume and pore diameter of biomass char and semi-coke after irradiation decreased slightly.Noteworthily,the pore diameter turned small and the acidic functional groups on their surface decomposed,thereby the basicity of carbon surface increased by microwave modification.The optimal promotion of desulfurization rate of three carbon materials was semi-coke irradiated at 850 W for 9 min and the sulfur dioxide adsorption rate was up to 45%.
文摘A simple method for the magnetic modification of various types of powdered agglomerate forming dia- magnetic materials was developed. Magnetic iron oxide particles were prepared from ferrous sulfate by microwave assisted synthesis. A suspension of the magnetic particles in water soluble organic solvent （methanol, ethanol, propanol, isopropyl alcohol, or acetone） was mixed with the material to be modified and then completely dried at elevated temperature. The magnetically modified materials were found to be stable in water suspension at least for 2 months.
