The density of Ni-AI alloys in both liquid state and solid-liquid coexistence state was measured with a modified pycnometric method. It was found that the density of Ni-AI alloys decreases with increasing temperature ...The density of Ni-AI alloys in both liquid state and solid-liquid coexistence state was measured with a modified pycnometric method. It was found that the density of Ni-AI alloys decreases with increasing temperature and Al concentration in the alloys. The molar volume of liquid Ni-AI binary alloys increases with the increase of temperature and Al concentration. The partial molar volume of Al in Ni-AI binary alloy was calculated approximately. The molar volume of liquid Ni-AI alloy determined in the present work shows a negative deviation from the ideal linear molar volume.展开更多
The density of liquid binary Ni-Mo alloys with molybdenum concentration from 0 to 20% (mass fraction) wasmeasured by a modified sessile drop method. It has been found that the density of the liquid Ni-Mo alloys decrea...The density of liquid binary Ni-Mo alloys with molybdenum concentration from 0 to 20% (mass fraction) wasmeasured by a modified sessile drop method. It has been found that the density of the liquid Ni-Mo alloys decreaseswith increasing temperature, but increases with the increase of molybdenum concentration in the alloys. The molarvolume of liquid Ni-Mo binary alloys increases with the increase of temperature and molybdenum concentration. Thepartial molar volume of molybdenum in Ni-Mo binary alloy has been approximately calculated as [13.18-2.65×10^(-3)T+(-47.94+3.10×10^(-2)T)×10^(-2)X_(Mo)]×10^(-6)m^3·mol^(-1). The molar volume of Ni-Mo alloy determined inthe present work shows a negative deviation from the ideal linear mixing molar volume.展开更多
The density of liquid Ni-Ta alloys was measured by using a modified sessile drop method. It is found that the density of the liquid Ni-Ta alloys decreases with the increasing temperature, but increases with the increa...The density of liquid Ni-Ta alloys was measured by using a modified sessile drop method. It is found that the density of the liquid Ni-Ta alloys decreases with the increasing temperature, but increases with the increase of tantalum concentration in the alloys. The molar volume of liquid Ni-Ta binary alloys increases with the increase of temperature and tantalum concentration.展开更多
The densities of liquid NiCoAlCr quaternary alloys with a fixed molar ratio of Ni to Co to Al (x(Ni):x(Co):x(Al)≈73:12.15) which is close to the average value of the commercial Ni-based superalloys TMS75, INCO713, CM...The densities of liquid NiCoAlCr quaternary alloys with a fixed molar ratio of Ni to Co to Al (x(Ni):x(Co):x(Al)≈73:12.15) which is close to the average value of the commercial Ni-based superalloys TMS75, INCO713, CM247LC and CMSX-4, and the mass fraction of chromium changes from 0 to 9% were measured by a modified sessile drop method. It is found that with increasing temperature and chromium concentration in the alloys, the densities of the liquid NiCoAlCr quaternary alloys decrease, whereas the molar volume of the liquid NiCoAlCr quaternary alloys increases. And the liquid densities of NiCoAlCr quaternary alloys calculated from the partial molar volumes of nickel, cobalt, aluminum and chromium in the corresponding Ni-bases binary alloys are in good agreement with the experimental ones, i.e. within the error tolerance range the densities of the liquid Ni-based multi-component alloys can be predicted from the partial volumes of elements in Ni-based binary alloys in liquid state. The molar volume of liquid NiCoAlCr binary alloy shows a negative deviation from the ideal linear mixing and the deviation changes small with the increase of chromium concentration at the same temperature.展开更多
Pure K2Ti4O9 whiskers were prepared by KDC（Kneading-Drying-Calcination） method with TiO2 and K2CO3 as raw materials. The influences of TiO2/K2CO3 molar ratio（RT/K）, calcination temperature（TC） and cooling proces...Pure K2Ti4O9 whiskers were prepared by KDC（Kneading-Drying-Calcination） method with TiO2 and K2CO3 as raw materials. The influences of TiO2/K2CO3 molar ratio（RT/K）, calcination temperature（TC） and cooling process on phase composition and morphology of the whiskers were investigated by TG-DSC（thermo gravimetric-differential scanning calorimeter）, XRD（X-ray diffraction）, and SEM（scanning electron microscope）. Pure K2Ti4O9 potassium titanate whiskers with large length-diameter ratio（r）（over 250） can be obtained at RT/K = 2.9 and TC = 950 ℃.展开更多
目的:评估牙根先脱位法拔除下颌骨埋伏第三磨牙(impacted lower third molar,ILTM)对邻近第二磨牙(mandibular second molar,M2M)远中成骨效果、牙髓状态和牙根外吸收(external root resorption,ERR)进展的影响。方法:选择2023年1月—2...目的:评估牙根先脱位法拔除下颌骨埋伏第三磨牙(impacted lower third molar,ILTM)对邻近第二磨牙(mandibular second molar,M2M)远中成骨效果、牙髓状态和牙根外吸收(external root resorption,ERR)进展的影响。方法:选择2023年1月—2023年10月于新疆医科大学第一附属医院进行ILTM拔除的患者64例,其中,32例采用牙根先脱位法拔除ILTM(实验组),32例采用牙冠先脱位法拔除ILTM(对照组)。术前、术后记录M2M松动度、牙髓状态、ERR情况、术后疼痛视觉模拟评分(VAS),术后3、6个月拍摄CBCT,测量M2M骨缺损深度、M2M骨高度、骨高度百分比和骨灰度等指标。采用SPSS 26.0软件包对数据进行统计学分析。结果:实验组术后第3天疼痛VAS评分显著低于对照组(P<0.05),手术时间、M2M牙髓活力和松动度两组均无显著差异(P>0.05);实验组去骨量显著少于对照组(P<0.05)。实验组术后即刻近中颊侧、远中舌侧PD显著低于对照组(P<0.05)。不同程度的ERR中,实验组术后3个月和6个月骨缺损深度、骨高度、骨高度百分比和骨灰度显著低于对照组(P<0.05)。不同阻生类型的2组术后骨缺损深度、骨高度、骨高度百分比和骨灰度比较,差异有统计学意义(P<0.05)。阻生深度与ERR严重程度比较,差异无统计学意义(P>0.05)。所有患者术后均未出现感染和神经损伤等并发症。结论:牙根先脱位法拔除ILTM对M2M远中成骨效果具有一定引导作用,对M2M远中牙周健康改善和术后反应均有效果。展开更多
文摘The density of Ni-AI alloys in both liquid state and solid-liquid coexistence state was measured with a modified pycnometric method. It was found that the density of Ni-AI alloys decreases with increasing temperature and Al concentration in the alloys. The molar volume of liquid Ni-AI binary alloys increases with the increase of temperature and Al concentration. The partial molar volume of Al in Ni-AI binary alloy was calculated approximately. The molar volume of liquid Ni-AI alloy determined in the present work shows a negative deviation from the ideal linear molar volume.
文摘The density of liquid binary Ni-Mo alloys with molybdenum concentration from 0 to 20% (mass fraction) wasmeasured by a modified sessile drop method. It has been found that the density of the liquid Ni-Mo alloys decreaseswith increasing temperature, but increases with the increase of molybdenum concentration in the alloys. The molarvolume of liquid Ni-Mo binary alloys increases with the increase of temperature and molybdenum concentration. Thepartial molar volume of molybdenum in Ni-Mo binary alloy has been approximately calculated as [13.18-2.65×10^(-3)T+(-47.94+3.10×10^(-2)T)×10^(-2)X_(Mo)]×10^(-6)m^3·mol^(-1). The molar volume of Ni-Mo alloy determined inthe present work shows a negative deviation from the ideal linear mixing molar volume.
文摘The density of liquid Ni-Ta alloys was measured by using a modified sessile drop method. It is found that the density of the liquid Ni-Ta alloys decreases with the increasing temperature, but increases with the increase of tantalum concentration in the alloys. The molar volume of liquid Ni-Ta binary alloys increases with the increase of temperature and tantalum concentration.
基金Project(NCET-05-0764) supported by the Program for New Century Excellent Talent in Universityproject(2004527) supported by SRF for ROCS, SEM
文摘The densities of liquid NiCoAlCr quaternary alloys with a fixed molar ratio of Ni to Co to Al (x(Ni):x(Co):x(Al)≈73:12.15) which is close to the average value of the commercial Ni-based superalloys TMS75, INCO713, CM247LC and CMSX-4, and the mass fraction of chromium changes from 0 to 9% were measured by a modified sessile drop method. It is found that with increasing temperature and chromium concentration in the alloys, the densities of the liquid NiCoAlCr quaternary alloys decrease, whereas the molar volume of the liquid NiCoAlCr quaternary alloys increases. And the liquid densities of NiCoAlCr quaternary alloys calculated from the partial molar volumes of nickel, cobalt, aluminum and chromium in the corresponding Ni-bases binary alloys are in good agreement with the experimental ones, i.e. within the error tolerance range the densities of the liquid Ni-based multi-component alloys can be predicted from the partial volumes of elements in Ni-based binary alloys in liquid state. The molar volume of liquid NiCoAlCr binary alloy shows a negative deviation from the ideal linear mixing and the deviation changes small with the increase of chromium concentration at the same temperature.
基金Funded by the Natural Science Foundation Key Project of Hubei Province(No.2011CDA060)
文摘Pure K2Ti4O9 whiskers were prepared by KDC（Kneading-Drying-Calcination） method with TiO2 and K2CO3 as raw materials. The influences of TiO2/K2CO3 molar ratio（RT/K）, calcination temperature（TC） and cooling process on phase composition and morphology of the whiskers were investigated by TG-DSC（thermo gravimetric-differential scanning calorimeter）, XRD（X-ray diffraction）, and SEM（scanning electron microscope）. Pure K2Ti4O9 potassium titanate whiskers with large length-diameter ratio（r）（over 250） can be obtained at RT/K = 2.9 and TC = 950 ℃.
文摘目的:评估牙根先脱位法拔除下颌骨埋伏第三磨牙(impacted lower third molar,ILTM)对邻近第二磨牙(mandibular second molar,M2M)远中成骨效果、牙髓状态和牙根外吸收(external root resorption,ERR)进展的影响。方法:选择2023年1月—2023年10月于新疆医科大学第一附属医院进行ILTM拔除的患者64例,其中,32例采用牙根先脱位法拔除ILTM(实验组),32例采用牙冠先脱位法拔除ILTM(对照组)。术前、术后记录M2M松动度、牙髓状态、ERR情况、术后疼痛视觉模拟评分(VAS),术后3、6个月拍摄CBCT,测量M2M骨缺损深度、M2M骨高度、骨高度百分比和骨灰度等指标。采用SPSS 26.0软件包对数据进行统计学分析。结果:实验组术后第3天疼痛VAS评分显著低于对照组(P<0.05),手术时间、M2M牙髓活力和松动度两组均无显著差异(P>0.05);实验组去骨量显著少于对照组(P<0.05)。实验组术后即刻近中颊侧、远中舌侧PD显著低于对照组(P<0.05)。不同程度的ERR中,实验组术后3个月和6个月骨缺损深度、骨高度、骨高度百分比和骨灰度显著低于对照组(P<0.05)。不同阻生类型的2组术后骨缺损深度、骨高度、骨高度百分比和骨灰度比较,差异有统计学意义(P<0.05)。阻生深度与ERR严重程度比较,差异无统计学意义(P>0.05)。所有患者术后均未出现感染和神经损伤等并发症。结论:牙根先脱位法拔除ILTM对M2M远中成骨效果具有一定引导作用,对M2M远中牙周健康改善和术后反应均有效果。
基金Sponsored by the Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry under grant No.2004527 and by the Natural Science Foundation of Chongqing Municipality under grant No.8427 and 8656
