The important supporting component in a gas turbine is the casing,which has the characteristics of large size,complex structure,and thin wall.In the context of existing 3DP sand casting processes,casting crack defects...The important supporting component in a gas turbine is the casing,which has the characteristics of large size,complex structure,and thin wall.In the context of existing 3DP sand casting processes,casting crack defects are prone to occur.This leads to an increase in the scrap rate of casings,causing significant resource wastage.Additionally,the presence of cracks poses a significant safety hazard after the casings are put into service.The generation of different types of crack defects in stainless steel casings is closely related to casting stress and the high-temperature concession of the sand mold.Therefore,the types and causes of cracks in stainless steel casing products,based on their structural characteristics,were systematically analyzed.Various sand molds with different internal topology designs were printed using the 3DP technology to investigate the impact of sand mold structures on high-temperature concession.The optimal sand mold structure was used to cast casings,and the crack suppression effect was verified by analyzing its eddy current testing results.The experimental results indicate that the skeleton structure has an excellent effect on suppressing cracks in the casing.This research holds important theoretical and engineering significance in improving the quality of casing castings and reducing production costs.展开更多
The Resin Infusion or the VARTM (Vacuum Assisted Resin Transfer Molding) process has significant potential to be used to manufacture curved composites. Another way to produce curved or complex geometry is to use 3D pr...The Resin Infusion or the VARTM (Vacuum Assisted Resin Transfer Molding) process has significant potential to be used to manufacture curved composites. Another way to produce curved or complex geometry is to use 3D printers. 3D or FDM (Fused Deposition Modelling) printers are now being used to produce relatively cheaper curved parts using thermoplastics such as PLA. However, the strength and mechanical performance of these parts is limited and can be enhanced if the polymer is reinforced with a type of fiber for instance. Research is being carried out to produce fiber rein-forced thermoplastic composites but that process is expected to be more expensive than the alternative methods such as injection or compression molding. Furthermore, to understand the manufacture of a hybrid composite using thermoplastics, fibers and epoxy resin, research and investigation need to be carried out. In this research</span></span></span></span><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;">, there are</span></span></span></span></span><span><span><span><span><span style="font-family:""><span style="font-family:Verdana;"> single-sided, double-sided, reusable, disposable and consumable molds. Most of the molds were created either using an FDM printer or manually. These molds were then used to manufacture flat and curved composite structures via the resin injection process, </span><i><span style="font-family:Verdana;">i.e.</span></i><span style="font-family:Verdana;"> VARTM with epoxy resin system and glass/carbon/flax fiber reinforcement. By replacing the costly metallic molds by significantly cheaper molds, the cost of production was expected to further reduce. Furthermore, using double-sided PLA molds was not expected to be a threat to the overall cost of the composite part in question compared to double-sided matched molds used in compression molding. Shear strength, tensile strength and charpy impact strength of most of the manufactured composite parts were also investigated. The strengths were compared based on the method of mold usage. The results showed that this method is effective for a cheaper production of curved epoxy resin composites. However, the strength of the part will decrease as the curved profile gets more complicated unless the basic resin infusion process is altered.展开更多
The effects of metallurgical and processing parameters on the formation of shrinkage cavities and porosities in spheroidal graphite cast iron have been studied, considering the parameters of carbon equivalent, inocula...The effects of metallurgical and processing parameters on the formation of shrinkage cavities and porosities in spheroidal graphite cast iron have been studied, considering the parameters of carbon equivalent, inoculation, casting modulus, mold type (green or dry) and pouring temperature within specific ranges of these variables. Based on the orthogonal experiments, the metallurgical and processing parameters of the minimum casting shrinkage and the maximum casting shrinkage were obtained, and the effects of metallurgical and processing parameters on the formation of shrinkage cavities and porosities in spheroidal graphite cast iron castings were discussed. Finally, two regression equations relating these variables to the formation of shrinkage porosity were derived based upon the orthogonal experiments conducted.展开更多
Twenty-eight molds were isolated from clinical blood cultures and were unidentifiable by cellular morphology using conventional microscopy. Using the utility of amplification and direct sequencing of internal transcri...Twenty-eight molds were isolated from clinical blood cultures and were unidentifiable by cellular morphology using conventional microscopy. Using the utility of amplification and direct sequencing of internal transcribed spacer region of ribosomal RNA gene, 93% of these fungi were identified. Seventy-one percents of the molds were found to be associated with plants or soil with no or few published cases of human disease. These include species of basidiomycetes and ascomycetes such as Botryosphaeria dothidea, Phomopsis flavodonflavus, Inonotus pachyphloeus, Earlilella scabrosa, Calocybe indica, Athelia pellicularis, Tinctoporellus epimiltinus, Trametes lactinea, Coprinellus aureogranulat and Xylaria feejeensis. Some of the nonsporulating molds were identified as pathogen or potential pathogens in immunocompetent or immunocompromised hosts. These include Schizophylum commune and hyphomycetes such as Cladosporium cladosporoides, Aspergillus niger and Fusarium equiseti. Basidiomycetes and hyphomycetes identified in the current study are ubiquitous in the environment and are almost similar to the species of molds reported from cutaneous and respiratory samples suggesting that the fungi may represent contaminants rather than true fangaemia. Results of this study emphasize the need of an effort to minimise blood culture contamination and support the recommendation to incorporate clinical, radiologic findings and positive blood culture for molds in the diagnosis and management of invasive mycosis.展开更多
In order to improve and evaluate the proficiency testing of cosmetic microorganism detection laboratory,strengthen the control of cosmetic microbial detection quality.In 2019 and 2020,the laboratory of the author’s u...In order to improve and evaluate the proficiency testing of cosmetic microorganism detection laboratory,strengthen the control of cosmetic microbial detection quality.In 2019 and 2020,the laboratory of the author’s unit participated in the proficiency testing(NIFDC-PT-242)and measurement audit(NIFDC-MA-2020-148)for molds and yeasts in cosmetics organized by the National Institutes for Food and Drug Control,respectively.According to the operation instruction for counting molds and yeasts in cosmetics and the Safety and Technical Standards for Cosmetics,the results of the sample for proficiency testing numbered NIFDC-PT-242 were unsatisfactory,and the results of the sample for measurement audit numbered NIFDC-MA-2020-148 were satisfactory.In view of the unsatisfactory results,the laboratory analyzed and summarized from the aspects of“human,machine,material,method and environment”,providing reference for the laboratories participating in proficiency testing and measurement audit..展开更多
The aim of this paper was to study the reaction between a Ti-6Al-4V alloy and boron nitride based investment shell molds used for investment casting titanium. In BN based investment shell molds, the face coatings are ...The aim of this paper was to study the reaction between a Ti-6Al-4V alloy and boron nitride based investment shell molds used for investment casting titanium. In BN based investment shell molds, the face coatings are made of pretreated hexagonal boron nitride (hBN) with a few yttria (Y2O3) and colloidal yttria as binder. The Ti-6Al-4V alloy was melted in a controlled atmosphere induction furnace with a segment water-cooled copper crucible. The cross-section of reaction interface between Ti alloys and shell mold was investigated by electron probe micro-analyzer (EPMA) and microhardness tester. The results show that the reaction is not serious, the thickness of the reacting layer is about 30-50 μm, and the thickness of α-case is about 180-200 pro. Moreover the α-case formation mechanism was also discussed.展开更多
At present, most TiAl components are produced by an investment casting process. Environmental and economic pressures have, however, resulted in a need for the industry to improve the current casting quality, reduce ma...At present, most TiAl components are produced by an investment casting process. Environmental and economic pressures have, however, resulted in a need for the industry to improve the current casting quality, reduce manufacturing costs and explore new markets for the process. Currently, the main problems for investment casting of TiAl alloys are cracks, porosities, and surface defects. To solve these problems, many studies have been conducted around the world, and it is found that casting defects can be reduced by improving composition and properties of the shell molds. It is important to make a summary for the related research progress for quality improvement of TiAl castings. So, the development on refractory composition of shell molds for TiAl alloy investment castings was reviewed, and research progress on deformability of shell mold for TiAl alloy castings both at home and abroad in recent years was introduced. The existing methods for deformability characterization and methods for improving the deformability of shell molds were summarized and discussed. The updated advancement in numerical simulation of TiAl alloy investment casting was presented, showing the necessity for considering the deformability of shell mold during simulation. Finally, possible research points for future studies on deformability of shell mold for TiAl alloy investment casting were proposed.展开更多
The correlation between the impact toughness and microstructural characteristics of a large bainitic steel bloom has been investigated. The study focuses on microcrack nucleation and propagation in the basic cleavage ...The correlation between the impact toughness and microstructural characteristics of a large bainitic steel bloom has been investigated. The study focuses on microcrack nucleation and propagation in the basic cleavage plane. To analyze the phase transformation during the wind-cooling process, the temperature field of the bloom was acquired by computer simulation, and a continuous cooling transformation experiment was conducted. The results show that compared with the surface of the bloom, the toughness of the bloom’s core is decreased by the increase in proeutectoid ferrite and the coarsening of tempered martensite–austenite constituents. The proeutectoid ferrite decreases the toughness via its effects on carbide precipitation, the formation of martensite–austenite constituents, and the bainite transformation. The relatively large tempered martensite–austenite constituents are conducive to microcrack nucleation and propagation.展开更多
In order to improve the performance of plaster molds for investment casting,a diverse content of glass fiber and polypropylene(PP)fiber was incorporated into the slurry for the preparation of a fiber-reinforced mold.T...In order to improve the performance of plaster molds for investment casting,a diverse content of glass fiber and polypropylene(PP)fiber was incorporated into the slurry for the preparation of a fiber-reinforced mold.The green and fired bending strengths,thermal expansion properties,permeability,and thermal shock resistance of the mold were examined,and the scanning electron microscope(SEM)with energy dispersive spectrometer(EDS)was applied for the observation of fracture morphology.With appropriate content,the introduction of glass fiber was proved to increase the green bending strength and fired bending strength,restrain the thermal expansion and improve the thermal shock resistance of the mold,while the polypropylene fiber added was able to raise the green bending strength and the permeability,reduce the thermal expansion and heighten the thermal shock resistance as well,though the fired bending strength would be weakened slightly.Evenly distributed fibers were capable of enhancing the mechanical properties of the matrix,but agglomerations and bundles of fibers resulting from excessive addition had a negative impact.Meanwhile,it was also manifested that micropores left by ablative polypropylene fibers could improve the permeability and reduce the thermal expansion of the mold,and the fired bending strength would be decreased slightly by the deterioration of continuous structure.Three different ratios of hybrid fiber were employed in plaster molds,which can meet altered requirement of castings.The samples modified with hybrid fiber possessed lower thermal deformation,higher air permeability,and better resistance of thermal shock,while the mechanical strength was equal to the fiber free sample or slightly increased.展开更多
In order to develop super-board and super-thick slabs, the flow and temperatur fields were studied in slab continuous casting molds under different practical conditions, such as slab dimensions, with-drawing slab spee...In order to develop super-board and super-thick slabs, the flow and temperatur fields were studied in slab continuous casting molds under different practical conditions, such as slab dimensions, with-drawing slab speed, design of nozzles, and superheat tempera-ture. The results showed that it is preferred to incline nozzle bores downwards and the submerged depth of the nozzles is best kept be-tween 250-300 mm. In addition, the solidified shell is thicker at the wide face than that at the narrow face, while the thin points alongthe wide face ekist both in the center and in the some area toward each respective end.展开更多
A new continuous casting mold repairing method--cold gas dynamic spraying (CGDS) is introduced. The study investigates the advantages of the CGDS process regarding repairing operation, such as convenient, in-situ re...A new continuous casting mold repairing method--cold gas dynamic spraying (CGDS) is introduced. The study investigates the advantages of the CGDS process regarding repairing operation, such as convenient, in-situ repairation,little heat delivery, microstructural and dimensional stability and other special applications. Microstructure and mechanical properties of the copper alloy coating, nickel coating, ceramic composite coating, and their interface to the substrates ,which are usually used in repairing operation have been researched by means of optical microscopy ( OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and micro-hardness tests. Experimental results have demonstrated the relative density of the copper alloy coating is as high as 98.7%, and that no obvious difference can be observed between the CrZrCu substrate and the Cu alloy coating in terms of microstructures; thus the interface is quite difficult to be identified. The bonding strength and micro-hardness of the Cu alloy coating reach up to 37 MPa and 310 HV0.2 ,respectively. The interface between the copper alloy coating and the nickel coating is either zigzag or wave shaped, and the cohesion is relatively good. As-sprayed nickel coating is dominated by severely deformed particles,and the relative density is up to 98.5%. Complete recrystallization occurred after annealing at 900℃ for one hour,while its micro-hardness remains as high as 124.1 HV02. All these results have indicated that CGDS is a promising technology for repairing the continuous casting mold and that its future development is prosperous as well.展开更多
We implemented the process of producing a new Rib in three different ways, and we selected the process that was the most affordable and required the least labor, and we did it. This paper also considers the influence ...We implemented the process of producing a new Rib in three different ways, and we selected the process that was the most affordable and required the least labor, and we did it. This paper also considers the influence of the cost of the form from MDF, Alumina and Steel on the quality of the product.展开更多
Two types of diacetatozirconic acid-yttria molds which were labeled as ZYW mold(diacetatozirconic acidyttria mold with traces of ammoium metatungstate in the slurry) and ZY mold(diacetatozirconic acid-yttria mold with...Two types of diacetatozirconic acid-yttria molds which were labeled as ZYW mold(diacetatozirconic acidyttria mold with traces of ammoium metatungstate in the slurry) and ZY mold(diacetatozirconic acid-yttria mold without ammonium metatungstate) were prepared by traditional investment casting.The ZYW and ZY molds were sintered in a carbon-reducing atmosphere and in air,respectively,at 1550℃ for 4 h.Interactions between Ti-47Al-2Cr-2Nb(at%) alloys and the molds at 1650℃ for 30 min were studied.The microstructures of the metalmold interfaces and the presence of inclusions and oxygen contamination in the TiAl bulk alloy were analyzed,and the influences of ammonium metatungstate were discussed.The results indicate that WO_(3)releases O into the TiAl melt,introducing tungsten metal into the alloy matrix.The TiAl alloy ingots cast in the ZY molds had the fewest inclusions and the lowest oxygen contamination.展开更多
Direct milling of sand molds is an important development in rapid manufacturing of sand molds. Direct milling is an effective method for manufacturing single or small batches of cast parts. This paper describes experi...Direct milling of sand molds is an important development in rapid manufacturing of sand molds. Direct milling is an effective method for manufacturing single or small batches of cast parts. This paper describes experimental investigations to find sand blocks with the appropriate strength, to describe wear patterns of different tools (high-speed steel (HSS), carbide, and polycrystalline diamond (PCD) tools), and to analyze sand mold cutting mechanisms. The results show that the PCD tool outperformes the other tools in terms of tool life. Average flank wear and micro-tipping are the dominant tool failure modes in the sand mold milling process. With a flank wear limit of 0.3 mm, the PCD tool works continuously for about 70 h under the experimental conditions. The experimental results show that the cutting mechanism for direct milling sand molds differs from metal cutting.展开更多
Occasional irregular initial solidification phenomena,including stickers,deep oscillation marks,depressions,and surface cracks of strand shells in continuous casting molds,are important limitations for developing the ...Occasional irregular initial solidification phenomena,including stickers,deep oscillation marks,depressions,and surface cracks of strand shells in continuous casting molds,are important limitations for developing the high-efficiency continuous casting of steels.The application of mold thermal monitoring(MTM) systems,which use thermocouples to detect and respond to temperature variations in molds,has become an effective method to address irregular initial solidification phenomena.Such systems are widely applied in numerous steel companies for sticker breakout prediction.However,monitoring the surface defects of strands remains immature.Hence,indepth research is necessary to utilize the potential advantages and comprehensive monitoring of MTM systems.This paper summarizes what is included in the irregular initial solidification phenomena and systematically reviews the current state of research on these phenomena by the MTM systems.Furthermore,the influences of mold slag behavior on monitoring these phenomena are analyzed.Finally,the remaining problems of the formation mechanisms and investigations of irregular initial solidification phenomena are discussed,and future research directions are proposed.展开更多
The effects of the water-cement ratio and the molding temperature on the hydration heat of cement were investigated with semi-adiabatic calorimetry.The specimens were prepared with water-cement ratios of 0.31,0.38,and...The effects of the water-cement ratio and the molding temperature on the hydration heat of cement were investigated with semi-adiabatic calorimetry.The specimens were prepared with water-cement ratios of 0.31,0.38,and 0.45,and the molding temperature was specified at 10 and 20℃.The experimental results show that,as the water-binder ratio increases,the value of the second temperature peak on the temperature curve of the cement paste decreases,and the age at which the peak appears is delayed.The higher the water-cement ratio,the higher the hydration heat release in the early period of cement hydration,but this trend reverses in the late period.There are intersection points of the total hydration heat curve of the cement pastes under the influence of the water-cement ratio,and this law can be observed at both molding temperatures.With the increase in the molding temperature,the age of the second temperature peak on the temperature curve of the cement paste will advance,but the temperature peak will decrease.The higher the molding temperature,the earlier the acceleration period of the cement hydration began,and the larger the hydration heat of the cement in the early stage,but the smaller the total heat in the late period.A subsection function calculation model of the hydration heat,which was based on the existing models,was proposed in order to predict the heat of the hydration of the concrete.展开更多
To address the common issues of wrinkling,tearing,and uneven wall thickness in the actual sheet metal stamp-ing process of the outer ring of needle roller bearings,this study analyzes critical technical indicators suc...To address the common issues of wrinkling,tearing,and uneven wall thickness in the actual sheet metal stamp-ing process of the outer ring of needle roller bearings,this study analyzes critical technical indicators such asforming limits,thickness distribution,and principal strains in the forming process in detail.Three-dimensionalmodels of the concave and convex dies were constructed.The effects of different process parameters,includingstamping speed,edge pressure,sheet metal thickness,and friction coefficient,on the quality of the forming partswere investigated by varying these parameters.Subsequently,the orthogonal experimental method was used todetermine an optimal experimental group from multiple sets of experiments.It was found that under the processparameters of a stamping speed of 3000 mm/s,edge pressure of 2000 N,sheet metal thickness of 0.9 mm,andfriction coefficient of 0.125,the forming quality of the outer ring of the bearing is ideal.展开更多
Existing microfabricated atomic vapor cells have only one optical channel,which is insufficient for supporting the multiple orthogonal beams required by atomic devices.In this study,we present a novel wafer-level manu...Existing microfabricated atomic vapor cells have only one optical channel,which is insufficient for supporting the multiple orthogonal beams required by atomic devices.In this study,we present a novel wafer-level manufacturing process for fabricating multi-optical-channel atomic vapor cells and an innovative method for batch processing the inner sidewalls of millimeter glass holes to meet optical channel requirements.Surface characterization and transmittance tests demonstrate that the processed inner sidewalls satisfy the criteria for an optical channel.In addition,the construction of an integrated processing platform enables multilayer non-isothermal anode bonding,the filling of inert gases,and the recovery and recycling of noble gases.Measurements of the absorption spectra and free-induction decay signals of xenon-129(^(129)Xe)and xenon-131(^(131)Xe)under different pump-probe schemes demonstrate the suitability of our vapor cell for use in atomic devices including atomic gyroscopes,dual-beam atomic magnetometers,and other optical/atomic devices.The proposed micromolding technology has broad application prospects in the field of optical-device processing.展开更多
基金financially supported by the National Natural Science Foundation of China(No.52175352)the Xing Liao Ying Cai Project of Liaoning Province(No.XLYC2008036)the Shenyang Youth Innovation Talent Support Program(No.RC220429)。
文摘The important supporting component in a gas turbine is the casing,which has the characteristics of large size,complex structure,and thin wall.In the context of existing 3DP sand casting processes,casting crack defects are prone to occur.This leads to an increase in the scrap rate of casings,causing significant resource wastage.Additionally,the presence of cracks poses a significant safety hazard after the casings are put into service.The generation of different types of crack defects in stainless steel casings is closely related to casting stress and the high-temperature concession of the sand mold.Therefore,the types and causes of cracks in stainless steel casing products,based on their structural characteristics,were systematically analyzed.Various sand molds with different internal topology designs were printed using the 3DP technology to investigate the impact of sand mold structures on high-temperature concession.The optimal sand mold structure was used to cast casings,and the crack suppression effect was verified by analyzing its eddy current testing results.The experimental results indicate that the skeleton structure has an excellent effect on suppressing cracks in the casing.This research holds important theoretical and engineering significance in improving the quality of casing castings and reducing production costs.
文摘The Resin Infusion or the VARTM (Vacuum Assisted Resin Transfer Molding) process has significant potential to be used to manufacture curved composites. Another way to produce curved or complex geometry is to use 3D printers. 3D or FDM (Fused Deposition Modelling) printers are now being used to produce relatively cheaper curved parts using thermoplastics such as PLA. However, the strength and mechanical performance of these parts is limited and can be enhanced if the polymer is reinforced with a type of fiber for instance. Research is being carried out to produce fiber rein-forced thermoplastic composites but that process is expected to be more expensive than the alternative methods such as injection or compression molding. Furthermore, to understand the manufacture of a hybrid composite using thermoplastics, fibers and epoxy resin, research and investigation need to be carried out. In this research</span></span></span></span><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;"><span style="font-family:Verdana;">, there are</span></span></span></span></span><span><span><span><span><span style="font-family:""><span style="font-family:Verdana;"> single-sided, double-sided, reusable, disposable and consumable molds. Most of the molds were created either using an FDM printer or manually. These molds were then used to manufacture flat and curved composite structures via the resin injection process, </span><i><span style="font-family:Verdana;">i.e.</span></i><span style="font-family:Verdana;"> VARTM with epoxy resin system and glass/carbon/flax fiber reinforcement. By replacing the costly metallic molds by significantly cheaper molds, the cost of production was expected to further reduce. Furthermore, using double-sided PLA molds was not expected to be a threat to the overall cost of the composite part in question compared to double-sided matched molds used in compression molding. Shear strength, tensile strength and charpy impact strength of most of the manufactured composite parts were also investigated. The strengths were compared based on the method of mold usage. The results showed that this method is effective for a cheaper production of curved epoxy resin composites. However, the strength of the part will decrease as the curved profile gets more complicated unless the basic resin infusion process is altered.
基金The paper was financially supported by the National Natural Science Foundation of China(Grant No.59235102).
文摘The effects of metallurgical and processing parameters on the formation of shrinkage cavities and porosities in spheroidal graphite cast iron have been studied, considering the parameters of carbon equivalent, inoculation, casting modulus, mold type (green or dry) and pouring temperature within specific ranges of these variables. Based on the orthogonal experiments, the metallurgical and processing parameters of the minimum casting shrinkage and the maximum casting shrinkage were obtained, and the effects of metallurgical and processing parameters on the formation of shrinkage cavities and porosities in spheroidal graphite cast iron castings were discussed. Finally, two regression equations relating these variables to the formation of shrinkage porosity were derived based upon the orthogonal experiments conducted.
文摘Twenty-eight molds were isolated from clinical blood cultures and were unidentifiable by cellular morphology using conventional microscopy. Using the utility of amplification and direct sequencing of internal transcribed spacer region of ribosomal RNA gene, 93% of these fungi were identified. Seventy-one percents of the molds were found to be associated with plants or soil with no or few published cases of human disease. These include species of basidiomycetes and ascomycetes such as Botryosphaeria dothidea, Phomopsis flavodonflavus, Inonotus pachyphloeus, Earlilella scabrosa, Calocybe indica, Athelia pellicularis, Tinctoporellus epimiltinus, Trametes lactinea, Coprinellus aureogranulat and Xylaria feejeensis. Some of the nonsporulating molds were identified as pathogen or potential pathogens in immunocompetent or immunocompromised hosts. These include Schizophylum commune and hyphomycetes such as Cladosporium cladosporoides, Aspergillus niger and Fusarium equiseti. Basidiomycetes and hyphomycetes identified in the current study are ubiquitous in the environment and are almost similar to the species of molds reported from cutaneous and respiratory samples suggesting that the fungi may represent contaminants rather than true fangaemia. Results of this study emphasize the need of an effort to minimise blood culture contamination and support the recommendation to incorporate clinical, radiologic findings and positive blood culture for molds in the diagnosis and management of invasive mycosis.
文摘In order to improve and evaluate the proficiency testing of cosmetic microorganism detection laboratory,strengthen the control of cosmetic microbial detection quality.In 2019 and 2020,the laboratory of the author’s unit participated in the proficiency testing(NIFDC-PT-242)and measurement audit(NIFDC-MA-2020-148)for molds and yeasts in cosmetics organized by the National Institutes for Food and Drug Control,respectively.According to the operation instruction for counting molds and yeasts in cosmetics and the Safety and Technical Standards for Cosmetics,the results of the sample for proficiency testing numbered NIFDC-PT-242 were unsatisfactory,and the results of the sample for measurement audit numbered NIFDC-MA-2020-148 were satisfactory.In view of the unsatisfactory results,the laboratory analyzed and summarized from the aspects of“human,machine,material,method and environment”,providing reference for the laboratories participating in proficiency testing and measurement audit..
文摘The aim of this paper was to study the reaction between a Ti-6Al-4V alloy and boron nitride based investment shell molds used for investment casting titanium. In BN based investment shell molds, the face coatings are made of pretreated hexagonal boron nitride (hBN) with a few yttria (Y2O3) and colloidal yttria as binder. The Ti-6Al-4V alloy was melted in a controlled atmosphere induction furnace with a segment water-cooled copper crucible. The cross-section of reaction interface between Ti alloys and shell mold was investigated by electron probe micro-analyzer (EPMA) and microhardness tester. The results show that the reaction is not serious, the thickness of the reacting layer is about 30-50 μm, and the thickness of α-case is about 180-200 pro. Moreover the α-case formation mechanism was also discussed.
基金financially supported by the Technical Development Foundation of China Academy of Machinery Science and Technology under project:Investment Casting Technology Research for TiAl Alloy Turbocharger Turbine
文摘At present, most TiAl components are produced by an investment casting process. Environmental and economic pressures have, however, resulted in a need for the industry to improve the current casting quality, reduce manufacturing costs and explore new markets for the process. Currently, the main problems for investment casting of TiAl alloys are cracks, porosities, and surface defects. To solve these problems, many studies have been conducted around the world, and it is found that casting defects can be reduced by improving composition and properties of the shell molds. It is important to make a summary for the related research progress for quality improvement of TiAl castings. So, the development on refractory composition of shell molds for TiAl alloy investment castings was reviewed, and research progress on deformability of shell mold for TiAl alloy castings both at home and abroad in recent years was introduced. The existing methods for deformability characterization and methods for improving the deformability of shell molds were summarized and discussed. The updated advancement in numerical simulation of TiAl alloy investment casting was presented, showing the necessity for considering the deformability of shell mold during simulation. Finally, possible research points for future studies on deformability of shell mold for TiAl alloy investment casting were proposed.
文摘The correlation between the impact toughness and microstructural characteristics of a large bainitic steel bloom has been investigated. The study focuses on microcrack nucleation and propagation in the basic cleavage plane. To analyze the phase transformation during the wind-cooling process, the temperature field of the bloom was acquired by computer simulation, and a continuous cooling transformation experiment was conducted. The results show that compared with the surface of the bloom, the toughness of the bloom’s core is decreased by the increase in proeutectoid ferrite and the coarsening of tempered martensite–austenite constituents. The proeutectoid ferrite decreases the toughness via its effects on carbide precipitation, the formation of martensite–austenite constituents, and the bainite transformation. The relatively large tempered martensite–austenite constituents are conducive to microcrack nucleation and propagation.
文摘In order to improve the performance of plaster molds for investment casting,a diverse content of glass fiber and polypropylene(PP)fiber was incorporated into the slurry for the preparation of a fiber-reinforced mold.The green and fired bending strengths,thermal expansion properties,permeability,and thermal shock resistance of the mold were examined,and the scanning electron microscope(SEM)with energy dispersive spectrometer(EDS)was applied for the observation of fracture morphology.With appropriate content,the introduction of glass fiber was proved to increase the green bending strength and fired bending strength,restrain the thermal expansion and improve the thermal shock resistance of the mold,while the polypropylene fiber added was able to raise the green bending strength and the permeability,reduce the thermal expansion and heighten the thermal shock resistance as well,though the fired bending strength would be weakened slightly.Evenly distributed fibers were capable of enhancing the mechanical properties of the matrix,but agglomerations and bundles of fibers resulting from excessive addition had a negative impact.Meanwhile,it was also manifested that micropores left by ablative polypropylene fibers could improve the permeability and reduce the thermal expansion of the mold,and the fired bending strength would be decreased slightly by the deterioration of continuous structure.Three different ratios of hybrid fiber were employed in plaster molds,which can meet altered requirement of castings.The samples modified with hybrid fiber possessed lower thermal deformation,higher air permeability,and better resistance of thermal shock,while the mechanical strength was equal to the fiber free sample or slightly increased.
文摘In order to develop super-board and super-thick slabs, the flow and temperatur fields were studied in slab continuous casting molds under different practical conditions, such as slab dimensions, with-drawing slab speed, design of nozzles, and superheat tempera-ture. The results showed that it is preferred to incline nozzle bores downwards and the submerged depth of the nozzles is best kept be-tween 250-300 mm. In addition, the solidified shell is thicker at the wide face than that at the narrow face, while the thin points alongthe wide face ekist both in the center and in the some area toward each respective end.
文摘A new continuous casting mold repairing method--cold gas dynamic spraying (CGDS) is introduced. The study investigates the advantages of the CGDS process regarding repairing operation, such as convenient, in-situ repairation,little heat delivery, microstructural and dimensional stability and other special applications. Microstructure and mechanical properties of the copper alloy coating, nickel coating, ceramic composite coating, and their interface to the substrates ,which are usually used in repairing operation have been researched by means of optical microscopy ( OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and micro-hardness tests. Experimental results have demonstrated the relative density of the copper alloy coating is as high as 98.7%, and that no obvious difference can be observed between the CrZrCu substrate and the Cu alloy coating in terms of microstructures; thus the interface is quite difficult to be identified. The bonding strength and micro-hardness of the Cu alloy coating reach up to 37 MPa and 310 HV0.2 ,respectively. The interface between the copper alloy coating and the nickel coating is either zigzag or wave shaped, and the cohesion is relatively good. As-sprayed nickel coating is dominated by severely deformed particles,and the relative density is up to 98.5%. Complete recrystallization occurred after annealing at 900℃ for one hour,while its micro-hardness remains as high as 124.1 HV02. All these results have indicated that CGDS is a promising technology for repairing the continuous casting mold and that its future development is prosperous as well.
文摘We implemented the process of producing a new Rib in three different ways, and we selected the process that was the most affordable and required the least labor, and we did it. This paper also considers the influence of the cost of the form from MDF, Alumina and Steel on the quality of the product.
基金financially supported by the Beijing Natural Science Foundation (No.2164054)the National Natural Science Foundation of China (No.51301005)。
文摘Two types of diacetatozirconic acid-yttria molds which were labeled as ZYW mold(diacetatozirconic acidyttria mold with traces of ammoium metatungstate in the slurry) and ZY mold(diacetatozirconic acid-yttria mold without ammonium metatungstate) were prepared by traditional investment casting.The ZYW and ZY molds were sintered in a carbon-reducing atmosphere and in air,respectively,at 1550℃ for 4 h.Interactions between Ti-47Al-2Cr-2Nb(at%) alloys and the molds at 1650℃ for 30 min were studied.The microstructures of the metalmold interfaces and the presence of inclusions and oxygen contamination in the TiAl bulk alloy were analyzed,and the influences of ammonium metatungstate were discussed.The results indicate that WO_(3)releases O into the TiAl melt,introducing tungsten metal into the alloy matrix.The TiAl alloy ingots cast in the ZY molds had the fewest inclusions and the lowest oxygen contamination.
基金Supported by the National Natural Science Foundation of China(No. 50775092)the China International Science and Technology Cooperation Project (No. 2008DF71250)
文摘Direct milling of sand molds is an important development in rapid manufacturing of sand molds. Direct milling is an effective method for manufacturing single or small batches of cast parts. This paper describes experimental investigations to find sand blocks with the appropriate strength, to describe wear patterns of different tools (high-speed steel (HSS), carbide, and polycrystalline diamond (PCD) tools), and to analyze sand mold cutting mechanisms. The results show that the PCD tool outperformes the other tools in terms of tool life. Average flank wear and micro-tipping are the dominant tool failure modes in the sand mold milling process. With a flank wear limit of 0.3 mm, the PCD tool works continuously for about 70 h under the experimental conditions. The experimental results show that the cutting mechanism for direct milling sand molds differs from metal cutting.
基金supported by the National Natural Science Foundation of China(No.52274319)。
文摘Occasional irregular initial solidification phenomena,including stickers,deep oscillation marks,depressions,and surface cracks of strand shells in continuous casting molds,are important limitations for developing the high-efficiency continuous casting of steels.The application of mold thermal monitoring(MTM) systems,which use thermocouples to detect and respond to temperature variations in molds,has become an effective method to address irregular initial solidification phenomena.Such systems are widely applied in numerous steel companies for sticker breakout prediction.However,monitoring the surface defects of strands remains immature.Hence,indepth research is necessary to utilize the potential advantages and comprehensive monitoring of MTM systems.This paper summarizes what is included in the irregular initial solidification phenomena and systematically reviews the current state of research on these phenomena by the MTM systems.Furthermore,the influences of mold slag behavior on monitoring these phenomena are analyzed.Finally,the remaining problems of the formation mechanisms and investigations of irregular initial solidification phenomena are discussed,and future research directions are proposed.
基金the National Natural Science Foundation of China(Nos.52368032 and 51808272)the China Postdoctoral Science Foundation(No.2023M741455)+1 种基金the Tianyou Youth Talent Lift Program of Lanzhou Jiaotong UniversityGansu Province Youth Talent Support Project(No.GXH20210611-10)。
文摘The effects of the water-cement ratio and the molding temperature on the hydration heat of cement were investigated with semi-adiabatic calorimetry.The specimens were prepared with water-cement ratios of 0.31,0.38,and 0.45,and the molding temperature was specified at 10 and 20℃.The experimental results show that,as the water-binder ratio increases,the value of the second temperature peak on the temperature curve of the cement paste decreases,and the age at which the peak appears is delayed.The higher the water-cement ratio,the higher the hydration heat release in the early period of cement hydration,but this trend reverses in the late period.There are intersection points of the total hydration heat curve of the cement pastes under the influence of the water-cement ratio,and this law can be observed at both molding temperatures.With the increase in the molding temperature,the age of the second temperature peak on the temperature curve of the cement paste will advance,but the temperature peak will decrease.The higher the molding temperature,the earlier the acceleration period of the cement hydration began,and the larger the hydration heat of the cement in the early stage,but the smaller the total heat in the late period.A subsection function calculation model of the hydration heat,which was based on the existing models,was proposed in order to predict the heat of the hydration of the concrete.
基金supported by the China Postdoctoral Science Founda-tion(Grant No.2022M721395)the National Natural Science Foun-dation of China(Grant No.72072089).Author Shichao Zhu and Linhan Ouyang received research support.
文摘To address the common issues of wrinkling,tearing,and uneven wall thickness in the actual sheet metal stamp-ing process of the outer ring of needle roller bearings,this study analyzes critical technical indicators such asforming limits,thickness distribution,and principal strains in the forming process in detail.Three-dimensionalmodels of the concave and convex dies were constructed.The effects of different process parameters,includingstamping speed,edge pressure,sheet metal thickness,and friction coefficient,on the quality of the forming partswere investigated by varying these parameters.Subsequently,the orthogonal experimental method was used todetermine an optimal experimental group from multiple sets of experiments.It was found that under the processparameters of a stamping speed of 3000 mm/s,edge pressure of 2000 N,sheet metal thickness of 0.9 mm,andfriction coefficient of 0.125,the forming quality of the outer ring of the bearing is ideal.
基金supported in part by the National Key Research and Development Plan(2022YFB3203400)the National Natural Science Foundation of China(62103324 and U1909221)the Natural Science Foundation of Shaanxi(2022JQ-554).
文摘Existing microfabricated atomic vapor cells have only one optical channel,which is insufficient for supporting the multiple orthogonal beams required by atomic devices.In this study,we present a novel wafer-level manufacturing process for fabricating multi-optical-channel atomic vapor cells and an innovative method for batch processing the inner sidewalls of millimeter glass holes to meet optical channel requirements.Surface characterization and transmittance tests demonstrate that the processed inner sidewalls satisfy the criteria for an optical channel.In addition,the construction of an integrated processing platform enables multilayer non-isothermal anode bonding,the filling of inert gases,and the recovery and recycling of noble gases.Measurements of the absorption spectra and free-induction decay signals of xenon-129(^(129)Xe)and xenon-131(^(131)Xe)under different pump-probe schemes demonstrate the suitability of our vapor cell for use in atomic devices including atomic gyroscopes,dual-beam atomic magnetometers,and other optical/atomic devices.The proposed micromolding technology has broad application prospects in the field of optical-device processing.