Comprehensive evaluation of chemical breakers for multistage network ultra-high strength gel

Polymer gels have been accepted as a useful tool to address many sealing operations such as drilling and completion,well stimulation,wellbore integrity,water and gas shutoff,etc.Previously,we developed an ultra-high strength gel(USGel)for medium to ultra-low temperature reservoirs.However,the removal of USGel is a difficult problem for most temporary plugging operations.This paper first provides new insights into the mechanism of USGel,where multistage network structure and physical entanglement are the main reasons for USGel possessing ultra-high strength.Then the effects of acid breakers,encapsulated breakers,and oxidation breakers(including H_(2)O_(2),Na_(2)S_(2)O_(8),Ca(ClO)_(2),H_(2)O_(2)+NaOH,Na_(2)S_(2)O_(8)+NaOH,and Ca(ClO)_(2)+NaOH)were evaluated.The effects of component concentration and temperature on the breaking solution were studied,and the corrosion performance,physical simulation and formation damage tests of the breaking solution were carried out.The final formulation of 2%-4%NaOH+4.5%-6%H_(2)O_(2) breaking solution was determined,which can make USGel completely turn into water at 35e105C.The combinations of“acid t breaking solution”,“acid+encapsulated breaker”and“encapsulated breaker+breaking solution”were evaluated for breaking effect.The acid gradually reduced the volume of USGel,which increased the contact area between breaking solution and USGel,and the effect of“4%acid+breaking solution”was 23 times higher than that of breaking solution alone at 35C.However,the acid significantly reduced the strength of USGel.This paper provides new insights into the breaking of high-strength gels with complex network structures.

Multistage Triaxial Behavior of Shallow Landslide Hazard Site Soil of Rangamati Sadar Area, Bangladesh

The soil samples were collected from a shallow landslide hazard site of the Rangamati Sadar in Bangladesh to determine the shear strength properties of the soil. Multistage triaxial consolidation undrained test has become worldwide more accepted to determine the shear strength parameters. Multistage triaxial undrained tests were performed on five samples taken from five different depths of boreholes. Samples were evaluated under two natural conditions and three remolded situations. Samples were consolidated before shearing at confining pressures from 50 kPa to 1200 kPa. All the test results are discussed in terms of deviator stress versus axial strain, mean effective stress versus deviator curves, stress ratio versus axial strain, and excess p. w. p. versus axial strain curves. The samples consolidated at low effective stress first displayed peak positive values of excess p. w. p., followed by increased strains due to sample bulging failure, and only a few samples formed a shear surface failure. The strength parameters were estimated using the maximum deviator stress as the failure criterion i.e. the overall value of the cohesion is 20 kPa and the friction angle is 34°. Hence, the critical state line has been constructed and the critical state parameters have been calculated. The critical state stress ratio M was calculated to be 0.036. The shear strength of soil is one of the significant mechanical properties that are thoroughly used to assess the landslide and liquefaction potentiality of the soil.

Multistage Extension and Age Dating of the Xiaoqinling Metamorphic Core Complex,Central China

There are two extensional systems in the Xiaoqinling metamorphic core complex (XMCC). One is the detachment fault system developed along the peripheries of the XMCC, which extended in an ESE-WNW direction and whose upper plate moved towards the WNW. The other extensional system includes the retrograde shear zones and normal faults developed within the XMCC, which represent the collapse of the XMCC. Ar-Ar and K-Ar dating shows that the extension of the detachment fault system continued from 135 to 123 Ma, i.e. in the late stage of its evolution at about 127 Ma. The collapse represented by the extensional system within the XMCC was operative during 120-106 Ma, and its main activity occurred about 116 Ma ago. These suggest that the XMCC experienced two extensional stages in its evolution, i.e., the syn-orogenic regional extension and post-orogenic collapse extension.

Experimental mass transfer coefficients in a pilot plant multistage column extractor

The volumetric overall mass transfer coefficients in a multistage column have been measured using axial dispersion model for toluene–acetone–water system. The effect of operating parameters on the volumetric overall mass transfer coefficients has been investigated for both mass transfer directions. The results show that the mass transfer performance is strongly dependent on rotor speed and mass transfer direction, although only slightly dependent on phase flow rates. In addition, empirical correlations to predict the overall mass transfer coefficients have been developed. The proposed correlations based on dimensionless numbers can be considered as a useful tool for the possible scale up of the multistage column extractor.

FINITE ELEMENT SIMULATION AND OPTIMIZATION OF MULTISTAGE WARM/HOT FORMING FOR OUTER RACE

A multistage warm/hot forming is simulated for the cross grove outer race of constant velocity joint, using athermo-mechanical coupled rigid viscoplastic finite element method, and specially some problem for process develop-ment and die design are analyzed. A forming test shows that computed results have good agreement with experimentalresults. Above obtained results can be applied to development of multistage warm/hot forming process and die designfor outer race.

Variable selection-based SPC procedures for high-dimensional multistage processes

Monitoring high-dimensional multistage processes becomes crucial to ensure the quality of the final product in modern industry environments. Few statistical process monitoring(SPC) approaches for monitoring and controlling quality in highdimensional multistage processes are studied. We propose a deviance residual-based multivariate exponentially weighted moving average(MEWMA) control chart with a variable selection procedure. We demonstrate that it outperforms the existing multivariate SPC charts in terms of out-of-control average run length(ARL) for the detection of process mean shift.

Design of Computationally Efficient Sharp FIR Filter Utilizing Modified Multistage FRM Technique for Wireless Communications Systems

Modern wireless communications gadgets demand multi-standard communications facilities with least overlap between different input radio channels. A sharp digital filter of extremely narrow transition-width with lower stop band ripples offers alias-free switching among the preferred frequency bands. A computationally competent low pass filter (LPF) structure based on the multistage frequency response masking (FRM) approach is proposed for the design of sharp finite impulse response (FIR) filters which are suitable for wireless communications applications. In comparison of basic FRM with other existing multistage FRM structures, the proposed structure has a narrow transition bandwidth and higher stop band attenuation with significant reduction in terms of the number of computational steps. A design example is incorporated to demonstrate the efficiency of the proposed approach. Simulation results establish the improvement of the proposed scheme over other recently published design strategies.

Microstructure Design of High-Entropy Alloys Through a Multistage Mechanical Alloying Strategy for Temperature-Stable Megahertz Electromagnetic Absorption

Developing megahertz(MHz)electromagnetic wave(EMW)absorption materials with broadband absorption,multi-temperature adaptability,and facile preparation method remains a challenge.Herein,nanocrystalline FeCoNiCr_(0.4)Cu_(0.2) high-entropy alloy powders(HEAs)with both large aspect ratios and thin intergranular amorphous layers are constructed by a multistage mechanical alloying strategy,aiming to achieve excellent and temperature-stable permeability and EMW absorption.A single-phase face-centered cubic structure with good ductility and high crystallinity is obtained as wet milling precursors,via precisely controlling dry milling time.Then,HEAs are flattened to improve aspect ratios by synergistically regulating wet milling time.FeCoNiCr_(0.4)Cu_(0.2) HEAs with dry milling 20 h and wet milling 5 h(D20)exhibit higher and more stable permeability because of larger aspect ratios and thinner intergranular amorphous layers.The maximum reflection loss(RL)of D20/SiO_(2) composites is greater than-7 dB with 5 mm thickness,and EMW absorption bandwidth(RL<-7 dB)can maintain between 523 and 600 MHz from-50 to 150℃.Furthermore,relying on the“cocktail effect”of HEAs,D20 sample also exhibits excellent corrosion resistance and high Curie temperature.This work provides a facile and tunable strategy to design MHz electromagnetic absorbers with temperature stability,broadband,and resistance to harsh environments.

Multistage Numerical Picard Iteration Methods for Nonlinear Volterra Integral Equations of the Second Kind

Using the Picard iteration method and treating the involved integration by numerical quadrature formulas, we propose a numerical scheme for the second kind nonlinear Volterra integral equations. For enlarging the convergence region of the Picard iteration method, multistage algorithm is devised. We also introduce an algorithm for problems with some singularities at the limits of integration including fractional integral equations. Numerical tests verify the validity of the proposed schemes.

Experimental study on the working performance of different milling tools for multistage fracturing ball seats

To achieve the secondary production in multistage fracturing wells of tight oil,milling tools are usually used to remove the multistage fracturing ball seats to achieve production with a large diameter in later.In this paper,first of all,the working mechanism of milling tools for multistage fracturing ball seats was studied and a mechanical analysis model of single abrasive grain was established.Then,an experimental system for milling tools was developed,and the experimental tests of the flat,the blade,and the slope milling tool were conducted in order.Besides,the morphology of chips and the surface morphology of the workpiece after the experiment were analyzed.Also,the working performance of milling tools was evaluated from the perspectives of working safety,working efficiency,and wear resistance of the milling tool.The results show that the torque of the milling tool increases nonlinearly with the increase in the cutting depth of the abrasive grain and increases linearly with the increase in the cutting width.Also,the chips are irregular particles and the size is mainly from 10 to 50μm.So,the chips should be pumped up with a small pump pressure and a large displacement.Besides this,the cutting depths of the abrasive grains are from 216.20 to 635.47μm and the bottom surface of the milling tool should be eccentric to avoid the zero point of cutting speed.Furthermore,the torque of the slope milling tool is 23.8%larger than that of the flat milling tool,which is also 30.4%smaller than that of the blade milling tool.Compared with the flat milling tool,the working efficiency of the blade milling tool improves by 79.9%and the slope milling tool improves by 111.1%.Also,the wear resistance of the blade milling tool decreases by 102.7%,while the slope milling tool declines by 32.6%when compared with the flat milling tool.Therefore,the slope milling tool has the characteristics of moderate torque,stable working conditions,the highest working efficiency,and fine wear resistance,which is preferably used to mill multistage fracturing ball seats.This study provides a theoretical basis and guidance for milling multistage fracturing ball seats on-site and realizing production with a large diameter in later stages of multistage fracturing wells.

Multistage mineralization in the Haoyaoerhudong gold deposit, Central Asian Orogenic Belt: Constraints from the sedimentary-diagenetic and hydrothermal sulfides and gold

The Central Asian Orogenic Belt,as one of world-class gold economic belts,preserves a number of giant,large black shale-hosted gold deposits,while it is still debated for origin of sulfides and gold mainly due to lack of identification for multiple stages of sulfides.The Haoyaoerhudong gold deposit is hosted in a sequence of Mesoproterozoic carbonaceous and pyritic slate,phyllite,and schist that form a tight syncline along the north margin of the North China Craton.Detailed petrography of the host rocks and mineralization have defined five stages of pyrites.The earliest form of pyrite(Py_(1))occurs as fine-grained dispersed pyrite in black carbonaceous slate and medium-to coarse-grained disseminated pyrite in pyrite-rich layers,contains relative low gold and high arsenic content,indicating a syn-sedimentary or diagenetic in origin.Stage Ⅱ pyrite(Py_(2))occurs with garnet and quartz inclusions and Py_(3) occurs as pyrite veins,contains higher gold and lower As content,and are interpreted to have formed from the dissolution-reprecipitation of Py_(1) during the peak metamorphism or post-peak metamorphism.Stage Ⅳ pyrite(Py_(4))from the pyrite-quartz veins crosscut the metamorphic garnet,contains the highest gold concentrations and other trace elements,and is considered to have formed post-peak metamorphism.Abundant native gold,electrum,and maldonite occur as inclusions within Py_(4) and monazite and in fractures that crosscut garnet.While,Py_(5) with typical remobilized feature is thought to be a product of melting of former pyrites(Py_(1) to Py_(4))triggered by the large-scale Hercynian magmatism.The sedimentary/diagenetic Py_(1) have δ^(34)S values that range from +12.4‰to +16.2‰.Later generations of sulfides,including Py_(2) to Py_(5),and Ccp_(2) to Ccp_(3),have δ^(34)S values from +9.5‰to +12.7‰.Monazite with maldonite inclusions from quartz-pyrite veins yielded an intercept age of 341.3±6.6 Ma,while coarse grained monazite associated biotite along fractures in the reefs yielded an intercept age of 254.6±8.2 Ma.The paragenetic,textural,chemical,and isotopic data suggest three distinct gold producing episodes at Haoyaoerhudong gold deposit.Gold and arsenic were clearly initially concentrated in organic muds,and enriched along the structures of diagenetic arsenic-rich pyrite.Subsequently,accompanying metamorphism and deformation,gold was liberated from the dissolution of diagenetic pyrites to form the pyrite veins.Finally,accompanying transformation of pyrite into pyrrhotite,gold was released into the metamorphic fluids to become concentrated as native gold,electrum,and maldonite in pyrite-quart veins.Monazite with age of 341 Ma from quartz-pyrite veins suggests that the third major gold mineralizing event in Haoyaoerhudong occurred before the Hercynian magmatism,suggesting that the Haoyaoerhudong deposit is a typical orogenic gold deposit rather than intrusion-related deposit.

Bionic Design and Analysis of a Novel Quadruped Robot with a Multistage Buffer System

Large quadruped mammals,such as ruminants,have outstanding motion ability,including running and bounding.These advanced motion abilities are related to the buffer effect of their complicated musculoskeletal systems.However,the buffer effect of most bio-robots is not satisfactory owing to the simple design of their buffer systems.In this paper,a physiological analysis of the ruminant musculoskeletal system is presented to explain the intrinsic buffer mechanism of motion.Based on the physical buffer parts of the ruminant limbs,the corresponding bionic mappings were determined.These mappings were used to guide the mechanism design of the robot multistage buffer system.The multistage buffer system includes two main buffer mechanisms:the first stage and the second stage.The buffer mechanism analysis of the first stage and multiple stages is discussed in theory to compare the effects between the normal single buffer system and the novel multistage buffer system.Then,the detailed mechanical structure of the limbs was designed based on the limb mechanism design.To further verify the superior efficacy of the multistage buffer system,the corresponding walking simulation experiments were conducted after the virtual prototype of a quadruped robot with a novel limb was built completely.Both theoretical analysis and simulation experiments prove that the bionic robot design with the novel multistage buffer system achieves better motion performance than the traditional robot buffer design and can be regarded as the design template of the robot limb.

Design and Performance Study of Clutch Disc Assembly of Wide-Angle, Large-Hysteresis, Multistage Damper

The clutch is an important component of the vehicle driveline system.One of its major functions is to attenuate or eliminate the torsional vibration and noise of the driveline system caused by the engine.Based on experiments of vibration damping under different vehicle conditions,the structure and functional principle of a clutch-driven disc assembly for a wide-angle,large-hysteresis,multistage damper is investigated in this study using an innovative combined approach.Furthermore,a systematic integration of key technologies,including wide-angle low-stiffness damping technology,large-hysteresis clutch technology,a novel split pre-damping structure technology,damping structure technology for component cushioning,and multistage damping structure technology,is proposed.The results show that the total torsional angle of the wide-angle large-hysteresis,multistage damper is more than twice that of the traditional clutch damper.The multistage damping design allows a better consideration of various damping requirements under different vehicle conditions,which can effectively address problems of severe idle vibrations and torsional resonance that occur under idled and accelerated conditions.Meanwhile,the use of a large-hysteresis structure and wear-resistant materials not only improves the vibration damping performance,but also prolongs the product service life,consequently resulting in multi-faceted optimization and innovative products.

Removal of CO2 in a multistage fluidized bed reactor by amine impregnated activated carbon: optimization using response surface methodology

Carbon dioxide (CO2) is the major component of greenhouse gas. Increase in concentration of CO2 in the atmosphere leads to global warming. To remove the CO2 from waste flue gas a four-stage counter-current multistage fluidized bed adsorber was developed and operated in continuous bubbling fluidization regime for the two丒phase system. This paper describes the optimum condition for CO2 removal efficiency in a multistage fluidized bed reactor using amine impregnated activated carbon. Response surface methodology with central composite design was used to determine the effect of three variables on the response. The variables are inlet concentration of CO2 in ppm (ranging from 3000 to 20,000), impregnation ratio of monoethanol amine (ranging from 0.2 to 0.6) and weir height in mm (20-60). The response was CO2 removal efficiency. The factor which was most influential has been identified from the analysis of variance. The optimum CO2 removal efficiency for the amine impregnated activated carbon (MEA-AC) was found to be 95.17%, at initial concentration of CO2 7312.85 ppm, chemical impregnation ratio of 0.31, and weir height 48.65 mm. From the experiment, the CO2 removal efficiency was found to be 95.97% at the same operating conditions. The predicted response was found to relevance with experimental data.

Bayesian synthetic evaluation of multistage reliability growth with instant and delayed fix modes

In the multistage reliability growth tests with instant and delayed fix modes,the failure data can be assumed to follow Weibull processes with different parameters at different stages.For the Weibull process within a stage,by the proper selection of prior distribution form and the parameters,a concise posterior distribution form is obtained,thus simplifying the Bayesian analysis.In the multistage tests,the improvement factor is used to convert the posterior of one stage to the prior of the subsequent stage.The conversion criterion is carefully analyzed to determine the distribution parameters of the subsequent stage's variable reasonably.Based on the mentioned results, a new synthetic Bayesian evaluation program and algorithm framework is put forward to evaluate the multistage reliability growth tests with instant and delayed fix modes.The example shows the effectiveness and flexibility of this method.

Improved Quality Prediction Model for Multistage Machining Process Based on Geometric Constraint Equation

Product variation reduction is critical to improve process efficiency and product quality, especially for multistage machining process(MMP). However, due to the variation accumulation and propagation, it becomes quite difficult to predict and reduce product variation for MMP. While the method of statistical process control can be used to control product quality, it is used mainly to monitor the process change rather than to analyze the cause of product variation. In this paper, based on a differential description of the contact kinematics of locators and part surfaces, and the geometric constraints equation defined by the locating scheme, an improved analytical variation propagation model for MMP is presented. In which the influence of both locator position and machining error on part quality is considered while, in traditional model, it usually focuses on datum error and fixture error. Coordinate transformation theory is used to reflect the generation and transmission laws of error in the establishment of the model. The concept of deviation matrix is heavily applied to establish an explicit mapping between the geometric deviation of part and the process error sources. In each machining stage, the part deviation is formulized as three separated components corresponding to three different kinds of error sources, which can be further applied to fault identification and design optimization for complicated machining process. An example part for MMP is given out to validate the effectiveness of the methodology. The experiment results show that the model prediction and the actual measurement match well. This paper provides a method to predict part deviation under the influence of fixture error, datum error and machining error, and it enriches the way of quality prediction for MMP.

Multistage Enrichment of the Sawafuqi Uranium Deposit: New Insights into Sandstone-hosted Uranium Deposits in the Intramontane Basins of Tian Shan, China

Meso-Cenozoic intracontinental orogenic processes in the Tian Shan orogenic belt have significant effect on the sandstone-hosted uranium deposits in the intramontane basins and those adjacent to the orogen. The Sawafuqi uranium deposit, which is located in the South Tian Shan orogenic belt, is investigated to reveal the relationships between uranium mineralization and orogenies. Recent exploration results show that the Sawafuqi uranium deposit has tabular, stratiform, quasi-stratiform, and lens-like orebodies and various geological characteristics different from typical interlayer oxidation zone sandstone-hosted uranium deposits. Systematic studies of ore samples from the Sawafuqi uranium deposit using a variety of techniques, including thin section observation, α-track radiograph, electron microprobe and scanning electron microscope, suggest that uranium mineralization is closely related to pyrite and organic matter. Mineralization-related alterations in the host rocks are mainly silicification and argillation including kaolinite, illite(and illite-smectite mixed layer) and chlorite. Tree stages of mineralization were identified in the Sawafuqi uranium deposit:(i) uranium-bearing detritus and synsedimentary initial pre-enrichment;(ii) interlayer oxidization zone uranium mineralization; and(iii) vein-type uranium mineralization. The synsedimentary uranium pre-enrichment represents an early uranium enrichment in the Sawafuqi uranium deposit, and interlayer oxidation zone uranium mineralization formed the main orebodies, which are superimposed by the vein-type uranium mineralization. Combining the results of this study with previous studies on the Meso-Cenozoic orogenies of South Tian Shan, it is proposed that the synsedimentary uranium pre-enrichment of the Sawafuqi uranium deposit was caused by Triassic Tian Shan uplift, and the interlayer oxidation zone uranium mineralization occurred during the Eocence-Oligocene period, when tectonism was relatively quiet, whereas the vein-type uranium mineralization took place in relation to the strong orogeny of South Tian Shan since Miocene.

AN EPIDEMIOLOGICAL EVIDENCE OF MULTISTAGE PROCESS OF STOMACH CANCER

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RAPID QUENCHING AND LARGE UNDERCOOLING IN MULTISTAGE RAPID SOLIDIFICATION POWDER-MAKING PROCESS

The rapid quenching and large undercooling phenomena and device working principle in the rapid solidification process are analyzed, and the working characteristics are presented in detail. The results show that these multistage device are ideal for making amorphous, quasicrystalline, microcrystalline and fine metallic powders.