Room-temperature and high-temperature magnetic permeability of Co-doped nanocrystalline alloys

Influence of composition and annealing temperature on structure and magnetic properties of amorphous and nanocrystalline Fe78.4-xCoxSi9B9Nb2.6Cu1 （x=27.4, 40.0, 51.0, 78.4） alloys was investigated by X-ray diffraction （XRD） and the temperature dependence of permeability. According to the initial crystallization temperature （Tx1） from differential scanning calorimetry （DSC） curves of as-quenched amorphous alloys, 490-700 ℃ isothermal annealing was carded out to obtain the characteristic nanocrystalline structure. Furthermore, the soft magnetic properties were measured by temperature evolution of magnetic permeability to obtain the correlation between Co content, annealing temperature and magnetic permeability. The results show that, on the one hand, the annealing temperature exerts a significant effect on phase structure and initial permeability （μi）. The higher-temperature （from 550 to 610 ℃） annealed Co content nanocrystalline samples can remain higher μi at elevated temperature. On the other hand, partial substitution Fe by Co can improve the high-temperature magnetic stability;however, the room-temperature permeability of higher Co content alloys decreases obviously at the same time. This phenomenon was analyzed from the viewpoint of the saturation magnetic induction （Bs）, magnetic anisotropy （〈K〉） and magnetostriction （λs）.

Giant magneto-impedance effects in nanocrystalline soft magnetic alloy ribbons

SINCE the discovery of the giant magneto-impedance (GMI) effects in amorphous wire (or rib-bon) of CoFeSiB and nanocrystalline wire (or film) of FeCuNbSiB, it has attracted greatattention due to its promising potential applications in industry. Amorphous (and nanocrys-talline) soft magnetic alloys have very large magnetic permeability, when an ac driving currentand an external magnetic field (EMF) are applied, the EMF will damp the magnetic fluxchange caused by the ac driving current, thus the magnetic permeability will decrease; as a re-

Giant magnetoimpedance effect of multilayered structure(F/SiO_2)_3/Ag/(SiO_2/F)_3 films deposited in a longitudinal magnetic field

The soft magnetic properties and giant magnetoimpedance(GMI) effect of the multilayered structure(F/SiO2)3/Ag/(SiO2/F)3(F≡Fe71.5Cu1Cr2.5V4Si12B9) films,which were prepared by radio frequency sputtering without and with a longitudinal magnetic field of about 72 kA/m,are studied.The results show that the GMI effect almost cannot be detected in the samples deposited without field,whereas,a longitudinal magnetic field applied during deposition process obviously optimizes the soft magnetic properties of the films,and noticeable GMI effect is obtained.The maximum values of the longitudinal and transverse GMI ratios are 45% and 44% at the frequency of 6.81 MHz,respectively.In addition,the dependence of magnetoimpedance ratio,magnetoresistance ratio,magnetoreactance ratio and effective permeability ratio on the frequency has been investigated.We found that the GMI spectrum curves in the longitudinal and transverse cases almost overlap for the field-deposited sample.The GMI effect is mainly a giant magnetoinductive effect at low frequencies.When f >9 MHz,magnetoreactance ratio changes to a negative,i.e.,the property of reactance changes from inductive to capacitive.

纳米晶软磁合金环形试样有效磁各向异性的研究(英文)

采用趋近饱和定律首次测定了纳米晶合金环形试样有效磁各向异性常数〈K〉。为了对比测量的准确度,同时测试了传统的晶态坡莫合金环形试样的磁晶各向异性。结果表明,用环形试样可以完成对低矫顽力的软磁材料进行磁各向异性的测定。

FeNbB合金有效各向异性与温度关系

研究了Fe83 Nb6B11合金有效各向异性〈k〉与温度t的关系 ,结果表明 :淬态Fe83Nb6B11非晶有效各向异性随温度的升高呈线性减小 ,热处理后的非晶和纳米双相合金的有效各向异性〈k〉随温度的升高变化不同 ,热处理温度低于 5 30℃时样品的有效各向异性〈k〉值在非晶居里温度减小 ,而热处理温度为 5 80℃时样品的有效各向异性〈k〉值在非晶居里温度变化很小·

压应力对FeMnCuSiBNb纳米晶合金磁导率与微结构的影响

采用单辊快淬法制备Fe_(74)Mn_(2)Cu_(1)Si_(13)B_(8)Nb_(2)合金带材,然后制成环形磁芯进行不同形式的退火处理。通过阻抗分析仪、X射线衍射仪(XRD)和磁光克尔显微镜(MOKE)等手段研究了原位压(缩)应力对淬态、常规退火和横向磁场退火态高磁感Fe_(74)Mn_(2)Cu_(1)Si_(13)B_(8)Nb_(2)合金的磁导率、相结构、微观结构与磁畴结构的影响。结果表明,压应力不会改变合金的相结构和微观结构,但对不同样品的磁导率和磁畴结构有着明显的影响。560℃常规和横向磁场退火样品的磁导率对压应力非常敏感,归因于压应力诱发的磁各向异性比0 MPa下的磁各向异性高1个数量级。与磁场退火相比,560℃常规退火样品经原位压缩后磁导率要高,归因于其磁化更容易。

热等静压对铁基非晶纳米晶合金软磁性能的影响

在铁基非晶纳米晶合金,普通氮气热处理最佳退火温度的基础上,将热等静压工艺引入到非晶带材磁芯的退火工艺中,探究热等静压工艺对Fe基非晶纳米晶合金软磁性能的影响。用X射线衍射仪、精密磁性元件测试仪和软磁交流设备测量了铁基非晶带材的晶体结构、磁芯的电感L和磁损耗Ps等。结果表明,在频率100 kHz和工作磁感应强度Bm=0.1 T时,普通氮气保护退火样品的矫顽力和磁损耗为2.04 A/m、10.10 W/kg,而热等静压样品则为1.33 A/m、6.58 W/kg,分别降低了53.4%、34.9%;普通氮气保护退火样品的有效磁导率和品质因数为11 579、0.46,而热等静压则为15 980、0.70,分别增加了38.0%、52.2%。

Fe_(39.4-x)Co_(40)Si_9B_9Nb_(2.6)Cu_x纳米晶合金的有效磁各向异性研究

采用多晶材料趋近饱和定律研究了非晶Fe39.4-xCo40Si9B9Nb2.6Cux(x=0.5,1,1.5)合金在不同温度纳米晶化后的有效磁各向异性常数〈K〉.结果表明,Cu含量较低(x=0.5)时,纳米晶粒较大并且在较低的退火温度(550℃)下析出硬磁相,〈K〉随退火温度Ta升高显著增加;随着Cu含量的增加,有效地细化了晶粒,并且抑制了硼化物的析出,〈K〉明显减小.讨论了〈K〉与晶粒尺寸D及初始磁导率的关系.