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Investigation of the serum oxidative stress in broilers fed on diets supplemented with nickel chloride
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作者 Bangyuan Wu Hengmin Cui +4 位作者 Xi Peng Jing Fang Zhicai Zuo Junliang Deng Jianying Huang 《Health》 2013年第3期454-459,共6页
The purpose of this study was to investigate the serum oxidative stress induced by dietary nickel chloride (NiCl2) in broilers. A total of 240 one-day-old avian broilers were divided into four groups and fed on a corn... The purpose of this study was to investigate the serum oxidative stress induced by dietary nickel chloride (NiCl2) in broilers. A total of 240 one-day-old avian broilers were divided into four groups and fed on a cornsoybean basal diet as control diet or the same basal diet supplemented with 300 mg/kg, 600 mg/kg and 900 mg/kg NiCl2. During the experimental period of 42 days, oxidative stress parameters were determined for both control and experimental groups. The results showed that malondialdehyde (MDA) content was significantly higher (p < 0.05 or p < 0.01) in the 300 mg/kg, 600 mg/kg and 900 mg/kg groups than that in the control group. In contrast, the activities of superoxide dismutase (SOD), catalase (CAT) and glutathione per- oxidase (GSH-Px), and the ability to inhibit hydroxy radical, and glutathione hormone (GSH) content were significantly decreased (p < 0.05 or p < 0.01) in the 300 mg/kg, 600 mg/kg and 900 mg/kg groups in comparison with those of the control group. It was concluded that dietary NiCl2 in excess of 300 mg/kg could cause oxidative stress, which could finally impaired the antioxidant function in broilers. 展开更多
关键词 BROILER nickel CHLORIDE OXIDATIVE stress SERUM
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Effect of Heat Treatment on High Temperature Stress Rupture Strength of Brazing Seam for Nickel-base Superalloy 被引量:2
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作者 Junying Zhang, Zhongtai Zhang, Jisheng Sun, Xiaofang Liu, Wei Tian (State Key Laboratory of New Ceramics and Fine Processing, Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China) (Beijing Institute of Aeronautical 《Journal of University of Science and Technology Beijing》 CSCD 2001年第2期123-125,共3页
In order to enhance the high-temperature stress rupture strength of brazing seam by heat treatment, it was diffusion treated, then solution heat treated, and finally aging treated. The microstructure of brazing seam e... In order to enhance the high-temperature stress rupture strength of brazing seam by heat treatment, it was diffusion treated, then solution heat treated, and finally aging treated. The microstructure of brazing seam especially morphology of gamma ' phase and boride was observed and the strength of brazing seam was measured in this process. The results show that heat treatment can enhance high-temperature stress rupture strength by improving the microstructure of brazing seam. The strength of brazing seam after solution heat treatment decreases in comparison with that only after diffusion treatment while aging treatment after solution heat treatment increases the strength of brazing seam. 展开更多
关键词 wide-gap brazing high temperature stress rupture strength MICROSTRUCTURE nickel-base superalloy
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Influence of Co, W and Ti on the Stress-rupture Lives of a Single Crystal Nickel-base Superalloy 被引量:1
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作者 Dayun YANG Tao JIN Nairen ZHAO Zhihui WANG Xiaofeng SUN Hengrong GUAN Zhuangqi HU 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2006年第2期169-172,共4页
The influence of Co, W and Ti on stress-rupture lives of a Ni-Cr-AI-Mo-Ta-Co-W-Ti single crystal nickel-base superalloy has been investigated using a L9 (34) orthogonal array design (OAD) by statistical analysis. ... The influence of Co, W and Ti on stress-rupture lives of a Ni-Cr-AI-Mo-Ta-Co-W-Ti single crystal nickel-base superalloy has been investigated using a L9 (34) orthogonal array design (OAD) by statistical analysis. At a selected composition range, Ti content was the most important factor to the effect of the stress-rupture lives and then followed by Co content. W content had the minimum effect on stress-rupture lives. The optimal alloy should contain 10 wt pct Co, 8 wt pct W and zero Ti. The optimized alloy also had good microstructural stability during thermal exposure at 870℃ for 500 h. 展开更多
关键词 nickel-base single crystal superalloy Orthogonal array design stress-RUPTURE
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Stress Measurement with an Improved Hollow Inclusion Technique In Jinchuan Nickel Mine 被引量:5
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作者 Meifeng Cai, Lan Qiao, Bo Yu, Shuanghong Wang (Resources Engineering School, University of Science and Technology Beijing, Beijing 100083) 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2000年第3期157-160,共4页
Borehole overcoring stress measurement with an improved hollow inclusion technique was carried out at 10 points on 3 levels in Jinchuan nickel mine which is situated in north-west of China. Through the measurement, 3-... Borehole overcoring stress measurement with an improved hollow inclusion technique was carried out at 10 points on 3 levels in Jinchuan nickel mine which is situated in north-west of China. Through the measurement, 3-D in situ stress state at the measuring points and distribution characteristics of the stress field in the mine were obtained. The stress state in Jinchuan mine is dominated by the horizontal tectonic stress field. The maximum principal stress is horizontal which is about twice the weight of the overburden and its orientation is approximately vertical to the regional tectonic line. The difference between two horizontal principal stresses is quite large which is an important reason to cause failure of underground excavations. 展开更多
关键词 stress measurement overcoring technique hollow inclusion cell IMPROVEMENT Jinchuan nickel mine
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MICROSTRUCTURE AND THERMAL STRESS RELAXATION OF ZrO_2-Ni FUNCTIONALLY GRADED MATERIAL 被引量:1
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作者 Zhu Jingchuan Yin Zhongda +1 位作者 Lai Zhonghong Li Jian(School of Materials Science and Engineering,Harbin Institute of Technology,Harbin 150001) 《中国有色金属学会会刊:英文版》 CSCD 1996年第4期94-99,共6页
MICROSTRUCTUREANDTHERMALSTRESSRELAXATIONOFZrO_2-NiFUNCTIONALLYGRADEDMATERIAL¥ZhuJingchuan;YinZhongda;LaiZhon... MICROSTRUCTUREANDTHERMALSTRESSRELAXATIONOFZrO_2-NiFUNCTIONALLYGRADEDMATERIAL¥ZhuJingchuan;YinZhongda;LaiZhonghong;LiJian(Scho?.. 展开更多
关键词 functionally GRADED MATERIAL zirconia nickel MICROSTRUCTURE THERMAL stress RELAXATION
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Lanthanum Relieved Toxic Effects Caused by Nickel in Hydrocharis dubia B L. Backer Leaves 被引量:3
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作者 张小兰 施国新 +4 位作者 徐勤松 谷巍 周红卫 曾晓敏 徐楠 《Journal of Rare Earths》 SCIE EI CAS CSCD 2003年第2期185-189,共5页
The paper briefly dealt with relieving toxic effects of La on high aquatic plant-Hydrocharis dubia B L. Backer growing in the solution containing different concentration of Ni. The results show that La can relieve the... The paper briefly dealt with relieving toxic effects of La on high aquatic plant-Hydrocharis dubia B L. Backer growing in the solution containing different concentration of Ni. The results show that La can relieve the reduction of chlorophyll content, the accumulation of MDA(malondiadehyde) and the elevation of relative membrane penetrability (RMP). After adding 10 mg . L-1 La to the solution, the activities of SOD and CAT in the leaves of Hydrocharis dubia B L. Backer increases compared with those of the single treatment of Ni, while the activity of POD decreases. It reveals that la enhances the abilities of scavenging the activated oxygen in the plant and alleviates the damage to the membranes. The soluble protein content with Ni and La compound treatment is higher than that of single Ni does, and proline content is contrary to the soluble protein content. So La improves the resistance of Hydrocharis dubia B. L. Backer to the stress of Ni. However, La can aggravate the damage to the cells under the extremely high concentration of Ni treatment. 展开更多
关键词 potany rare earths LANTHANUM nickel Hydrocharis dubia B L. Backer stress relieving
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Physiological effects of nickel chloride on the freshwater cyanobacterium <i>Synechococcus</i>sp. IU 625
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作者 Brian Nohomovich Bao T. Nguyen +3 位作者 Michael Quintanilla Lee H. Lee Sean R. Murray Tin-Chun Chu 《Advances in Bioscience and Biotechnology》 2013年第7期10-14,共5页
Harmful algal blooms (HABs) are a serious environmental problem globally. The ability of cyanobacteria, one of the major causative agents of HABs, to grow in heavy metal polluted areas is proving a challenge to enviro... Harmful algal blooms (HABs) are a serious environmental problem globally. The ability of cyanobacteria, one of the major causative agents of HABs, to grow in heavy metal polluted areas is proving a challenge to environmental restoration initiatives. Some cyanobacteria secrete toxins, such as microcystin, that are potentially dangerous to animals and humans. In this study, the physiology of a cyanobacterium was assessed to nickel chloride exposure. Cell growths were monitored throughout the study with various nickel chloride concentrations (0, 10, 25 or 50 mg/L). Morphological abnormalities were observed with microscopic image analyses. Inductively coupled plasma mass spectrometry (ICP-MS) was carried out to trace the distribution of nickel during the growth period. This study provides insight on potential nickel response mechanisms in freshwater cyanobacteria, which may lead to effective HAB prevention strategy development. 展开更多
关键词 Harmful Algal BLOOMS (HABs) Cyanobacteria nickel Chloride stress Response ICP-MS
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Laser Shock Processing of an Austenitic Stainless Steel and a Nickel-base Superalloy 被引量:1
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作者 Huaming WANG, Xijun SUN and Xiaoxuan LILaboratory of Laser Materials Processing and Surface Engineering, School of Materials Science and Engineering, Beihang University (formerly Beijing University of Aeronautics and Astronautics), Beijing 100083, China 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2003年第5期402-404,共3页
An austenitic stainless steel 1Cr18Ni9Ti and a solid solution-strengthened Ni-base superalloy GH30 were shock processed using a Q-switched pulsed Nd-glass laser. Microstructure, hardness and residual stress of the las... An austenitic stainless steel 1Cr18Ni9Ti and a solid solution-strengthened Ni-base superalloy GH30 were shock processed using a Q-switched pulsed Nd-glass laser. Microstructure, hardness and residual stress of the laser shock processed surface were investigated as functions of laser processing parameters. Results show that high density of dislocations and fine deformation twins are produced in the laser shock processed surface layers in both the austenitic stainless steel and the nickel-base superalloy. Extensive strain-induced martensite was also observed in the laser shock processed zone of the austenitic steel. The hardness of the laser shock processed surface was significantly enhanced and compressive stress as high as 400 MPa was produced in the laser shock processed surface. 展开更多
关键词 Laser shock processing Austenitic stainless steel nickel-base superalloy Surface mechanical properties Residual stress
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Corrosion performance and applicability evaluation of nickel-based alloys for oil and gas production tubing applications
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作者 ZHOU Qingjun ZHANG Zhonghua YANG Jianqiang 《Baosteel Technical Research》 CAS 2015年第4期52-56,共5页
The sulfide stress corrosion cracking( SSC) performance of G3 and 028 nickel-based alloys w as studied using slow strain rate test( SSRT) and the four-point bend( FPB) test under simulated dow nhole conditions. ... The sulfide stress corrosion cracking( SSC) performance of G3 and 028 nickel-based alloys w as studied using slow strain rate test( SSRT) and the four-point bend( FPB) test under simulated dow nhole conditions. The effect of high temperature,high H2 S / CO2 partial pressure,and the presence of sulfur on SSC susceptibility w as investigated. The G3 alloy w as found to have a higher SSC resistance than the 028 alloy. Presence of sulfur and temperature bear a strong influence on the SSC performance of the metals,particularly on the 028 alloy. The applicability of 028 and G3 alloys may be expanded and both could safely be used beyond the limits set by the ISO15156-3 standard. 展开更多
关键词 nickel-based alloy sulfide stress corrosion oil tubing
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高温模拟压水堆一回路水中枝晶取向对Inconel 182镍基合金焊接金属应力腐蚀开裂的影响
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作者 李锴 张维 +5 位作者 郑会 杨双亮 许鑫和 潘登 崔同明 吕战鹏 《腐蚀与防护》 CAS CSCD 北大核心 2024年第5期6-11,共6页
在模拟压水堆(PWR)一回路高温水中对Inconel182镍基合金焊接金属进行了应力腐蚀开裂(SCC)试验,研究了枝晶取向对其SCC行为的影响。结果表明:在320℃下模拟压水堆一回路水中,182合金LT取向试样断口上出现全面沿晶应力腐蚀裂纹扩展带,其... 在模拟压水堆(PWR)一回路高温水中对Inconel182镍基合金焊接金属进行了应力腐蚀开裂(SCC)试验,研究了枝晶取向对其SCC行为的影响。结果表明:在320℃下模拟压水堆一回路水中,182合金LT取向试样断口上出现全面沿晶应力腐蚀裂纹扩展带,其平均裂纹扩展速率以及最大裂纹扩展速率均大于290℃下相同试样,表明在模拟压水堆一回路水中升高温度对182合金焊接金属应力腐蚀裂纹扩展有促进作用;290℃下182合金LT取向试样的平均裂纹扩展速率、最大裂纹扩展速率以及裂纹扩展区宽度占比均大于TL取向试样,表明裂纹沿LT枝晶取向更容易扩展。 展开更多
关键词 核电站 焊接金属 182镍基合金 应力腐蚀开裂 枝晶取向 裂纹扩展速率
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Waspaloy镍基合金高温流变应力及其本构模型构建
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作者 许罗鹏 郝梦全 +5 位作者 熊磊 张儒伦 李志欣 张宏 杨卫波 邹华维 《科学技术与工程》 北大核心 2024年第17期7406-7413,共8页
针对涡轮发动机涡轮叶片复杂应力状态下的时效变形问题,以涡轮叶片材料Waspaloy镍基合金为研究对象,开展Waspaloy镍基合金时效处理,完成时效态Waspaloy镍基合金600、700和750℃准静态高温力学拉伸试验。利用Ludwik和Hollomon经验公式预... 针对涡轮发动机涡轮叶片复杂应力状态下的时效变形问题,以涡轮叶片材料Waspaloy镍基合金为研究对象,开展Waspaloy镍基合金时效处理,完成时效态Waspaloy镍基合金600、700和750℃准静态高温力学拉伸试验。利用Ludwik和Hollomon经验公式预测Waspaloy镍基合金高温塑性段流变应力,引入平均误差(the mean error,E_(r))和均方根误差(root mean square error,RMSE)评价流变应力的预测准确度。结果表明,时效处理后合金的硬度得到有效提升,而其塑性性能有所降低。Waspaloy镍基合金的抗拉强度和延伸率在600~750℃区间范围内与加载温度呈负相关关系。Ludwik模型较Hollomon模型有更高的流变应力预测精度,而在高温高应变区域Ludwik模型预测流变应力仍存在较大误差。在Ludwik模型的基础上引入指数项,修正后的Ludwik模型能更好地预测Waspaloy镍基合金高温塑性段的流变应力。 展开更多
关键词 Waspaloy镍基合金 时效处理 流变应力 本构模型
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喷丸工艺参数对718镍基合金表面性能的影响
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作者 周兆锋 金芹 +2 位作者 刘青 董小飞 宋树权 《兵器材料科学与工程》 CAS CSCD 北大核心 2024年第2期36-41,共6页
为全面理解718镍基合金喷丸强化工艺参数的作用,用精确的三维建模对弹丸和基体进行模拟,并结合仿真分析方法考察喷丸尺寸、速度及入射角度对喷丸强化的影响。重点分析了表面粗糙度和残余应力分布,以全面展现喷丸强化的关键特征。结果表... 为全面理解718镍基合金喷丸强化工艺参数的作用,用精确的三维建模对弹丸和基体进行模拟,并结合仿真分析方法考察喷丸尺寸、速度及入射角度对喷丸强化的影响。重点分析了表面粗糙度和残余应力分布,以全面展现喷丸强化的关键特征。结果表明:随弹丸直径和速度的增加,残余应力呈规律性变化,入射角度为0°~10°时对残余应力影响较小,但可轻微降低表面粗糙度。当入射角度从10°增至30°时,喷丸强化效果减弱,同时表面粗糙度增加。这为工艺参数选择提供了重要参考。通过试验验证仿真结果,进一步证实了本研究的准确性和实用性。 展开更多
关键词 718镍基合金 喷丸 残余应力 粗糙度 有限元分析
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Analysis on mechanical properties of nickel-iron steel after post-weld heat treatment
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作者 WANG Baosen XU Ke +1 位作者 MA Tianjun ZHU Shuangchun 《Baosteel Technical Research》 CAS 2013年第3期19-22,共4页
X-ray diffraction was utilized to measure the residual stress of 45 mm UNS N08810 plates after post-weld heat treatment at temperatures of 680℃ and 900℃, which showed reductions of 86.9% and 71.6% in the residual st... X-ray diffraction was utilized to measure the residual stress of 45 mm UNS N08810 plates after post-weld heat treatment at temperatures of 680℃ and 900℃, which showed reductions of 86.9% and 71.6% in the residual stress, respectively. This indicates that post-weld heat treatment can play a significant role in reducing residual stress, while no significant effects on tensile stress and micro-hardness of the welding joint were observed after treatment. 展开更多
关键词 nickel-iron alloy post-weld heat treatment weld residual stress PRECIPITATE
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激光冲击诱导应力波对残余应力孔洞形成的影响
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作者 盛湘飞 谭慧勇 +2 位作者 袁文志 苟江龙 李智 《表面技术》 EI CAS CSCD 北大核心 2024年第19期153-163,共11页
目的揭示残余应力孔洞形成的影响机制。方法采用有限元动力学仿真,实现对激光冲击诱导应力波传播过程的捕捉和特性分析。结果在2000 ns以内的光斑作用区域,材料的初始应力仅受到激光冲击诱导Ⅱ类应力波的扰动作用,此扰动作用由光斑中心... 目的揭示残余应力孔洞形成的影响机制。方法采用有限元动力学仿真,实现对激光冲击诱导应力波传播过程的捕捉和特性分析。结果在2000 ns以内的光斑作用区域,材料的初始应力仅受到激光冲击诱导Ⅱ类应力波的扰动作用,此扰动作用由光斑中心向外依次减弱,引起的应力波动幅值由2459 MPa降至224 MPa;在其他工艺参数相同的情况下,残余应力孔洞随着峰值压力和脉宽的增加而变得更加明显,应力幅值差σ_(k)分别由0、114 MPa增至454、568 MPa,孔洞直径d_(k)分别由0、0.8 mm增至约1.4 mm,光斑直径的影响相对较弱。在激光能量3 J的作用下,空间高斯分布对应结果存在应力孔洞,σ_(k)、d_(k)分别为190 MPa、1 mm。将空间平顶分布激光能量增至7 J,对应结果由3 J激光能量时的无应力孔洞转变为存在明显应力孔洞,σ_(k)、d_(k)分别为634 MPa、1.4 mm。另外,在激光能量3 J的作用下,材料1的应力孔洞最显著,σ_(k)、d_(k)分别为207 MPa、1.4 mm,均高于材料2和材料3的对应值。凸圆面、平面和凹圆面对应的σ_(k)分别为212、190、83 MPa,d_(k)均为1 mm。结论在圆形光斑激光冲击载荷作用下,加载和卸载过程中形成的应力波在光斑中心的汇聚作用均较强,导致光斑中心区域材料持续出现正反向屈服,进而形成残余应力孔洞;在相同参数条件下,激光能量越高,则材料的力学性能越低,应力波扰动作用越强,应力孔洞现象越明显。 展开更多
关键词 激光冲击 应力波 残余应力 应力孔洞 有限元分析 镍基高温合金
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孔挤压强化对GH4169孔结构高温疲劳裂纹扩展行为影响研究
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作者 毛建兴 咸志帆 +4 位作者 王欣 刘茜 刘海燕 王荣桥 胡殿印 《推进技术》 EI CAS CSCD 北大核心 2024年第9期184-193,共10页
为探究孔挤压强化对镍基高温合金GH4169孔结构疲劳裂纹扩展行为的影响规律,针对孔挤压强化后螺栓孔特征模拟件开展残余应力松弛及疲劳裂纹扩展试验。结果表明,经热松弛稳定后,孔边依旧可以保持至少400 MPa的残余压应力水平,且孔壁表面... 为探究孔挤压强化对镍基高温合金GH4169孔结构疲劳裂纹扩展行为的影响规律,针对孔挤压强化后螺栓孔特征模拟件开展残余应力松弛及疲劳裂纹扩展试验。结果表明,经热松弛稳定后,孔边依旧可以保持至少400 MPa的残余压应力水平,且孔壁表面残余应力松弛幅度高于内部;孔挤压强化后疲劳裂纹扩展速率降低一个数量级,随着相对挤压量增加,疲劳裂纹扩展速率降低幅度增大,疲劳裂纹扩展寿命增幅为4~22倍。结合有限元仿真及断口分析,孔挤压强化对疲劳裂纹扩展的影响机制可归结为松弛至稳定后的残余压应力抵消部分外载应力,导致有效应力强度因子范围减小,使得疲劳裂纹扩展速率降低。基于该机制,利用残余应力修正的Walker模型对疲劳裂纹扩展寿命进行预测,误差在1.8倍分散带以内。 展开更多
关键词 镍基高温合金 冷挤压 残余应力 疲劳裂纹扩展 应力强度因子
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兆声功率密度对同轴兆声辅助喷射电沉积镍的影响
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作者 翟科 周丰 +3 位作者 梁勇康 马仕豪 李腾楠 杜立群 《电镀与涂饰》 CAS 北大核心 2024年第1期1-6,共6页
[目的]金属微器件在电沉积过程中往往会产生较大的残余应力,对微器件的尺寸精度、力学性能和良率产生不利影响。[方法]为降低镀层的残余应力,在喷射电沉积镍过程中施加同轴兆声辅助。研究了兆声功率密度对Ni镀层形貌、表面粗糙度、显微... [目的]金属微器件在电沉积过程中往往会产生较大的残余应力,对微器件的尺寸精度、力学性能和良率产生不利影响。[方法]为降低镀层的残余应力,在喷射电沉积镍过程中施加同轴兆声辅助。研究了兆声功率密度对Ni镀层形貌、表面粗糙度、显微硬度和残余应力的影响。[结果]施加同轴兆声辅助后,所得Ni镀层的宏观和微观形貌都有所变差,表面粗糙度略微增大,显微硬度变化不大,但残余应力显著降低。当兆声功率密度为10 W/cm2时,Ni镀层的残余应力最低,比无兆声辅助时所得Ni镀层低了37.75%。[结论]在电沉积过程中施加兆声辅助能够有效降低镀层的残余应力。 展开更多
关键词 微器件 喷射电沉积 残余应力 兆声辅助 功率密度
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微量元素Zr对高温合金铸件凝固缺陷及持久性能的影响
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作者 周阳 崔艳娜 +3 位作者 王博 李淑苹 李明 王俊 《有色金属材料与工程》 CAS 2024年第5期10-17,共8页
高温合金中微量元素含量虽然极低,但是其对合金的高温性能产生的重要作用不可忽略。以Zr为例,其存在对高温合金铸造特性和高温力学性能的影响仍需要进一步探索。研究了微量合金元素Zr对K417合金凝固过程中凝固缺陷的形成、组织演变以及... 高温合金中微量元素含量虽然极低,但是其对合金的高温性能产生的重要作用不可忽略。以Zr为例,其存在对高温合金铸造特性和高温力学性能的影响仍需要进一步探索。研究了微量合金元素Zr对K417合金凝固过程中凝固缺陷的形成、组织演变以及持久性能的影响。研究结果表明,Zr的加入会影响合金铸态组织中共晶组织的含量,同时也影响凝固过程中的固液相线。随着Zr含量的增加,凝固温度区间先下降后增加;从而影响合金铸造流动性以及组织凝固缺陷的形成。900℃、314 MPa下的持久性能测试结果表明,随着Zr含量的增加,寿命先延长后降低,Zr含量为0.07%时达到最大值。为铸造高温合金母合金中微量元素含量的控制,提高铸件冶金质量提供实验支撑。 展开更多
关键词 镍基高温合金 微量元素Zr 凝固缺陷 高温持久性能
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SiC芯片封装纳米银烧结层的热机械分析及疲劳寿命预测
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作者 倪艳 陈丹阳 +1 位作者 蔡苗 杨道国 《电子元件与材料》 CAS 北大核心 2024年第2期238-245,共8页
纳米银的热膨胀系数与模块中其他组件存在较大差异,导致在严苛环境下工作时发生热疲劳失效。因此,预测纳米银烧结层的热疲劳寿命成为关键问题。以SiC功率模块为对象,利用有限元仿真和修正的Coffin-Manson寿命预测模型,分析了纳米银烧结... 纳米银的热膨胀系数与模块中其他组件存在较大差异,导致在严苛环境下工作时发生热疲劳失效。因此,预测纳米银烧结层的热疲劳寿命成为关键问题。以SiC功率模块为对象,利用有限元仿真和修正的Coffin-Manson寿命预测模型,分析了纳米银烧结层在热循环载荷下的最大等效应力和疲劳寿命。进一步通过响应面法分析,以疲劳寿命为优化目标,选取了SiC芯片和纳米银烧结层最佳参数组合,并探究铜基板镀镍对疲劳寿命的影响。研究结果显示:在累积的热循环下,纳米银烧结层边角处的等效应力最大,最容易发生热疲劳失效。通过优化设计,当SiC芯片厚度取0.15 mm,纳米银烧结层厚度取0.1 mm时,最大等效应力降低了1.36%,疲劳寿命增加了1.57倍。此外,铜基板上的镍层与纳米银烧结层具有相适应的材料属性,能够降低纳米银烧结层的等效应力,并增加其疲劳寿命。 展开更多
关键词 有限元分析 纳米银 应力 疲劳寿命 镀镍
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超临界水环境中应变速率对国产镍基合金应力腐蚀开裂敏感性的影响
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作者 钟犁 刘学莹 +3 位作者 马辰昊 徐鸿 张乃强 朱忠亮 《腐蚀与防护》 CAS CSCD 北大核心 2024年第3期7-16,共10页
采用慢应变速率试验(SSRT),研究了不同应变速率下国产镍基合金C-HRA-1在650℃、25MPa超临界水环境中的应力腐蚀开裂(SCC)敏感性。采用扫描电子显微镜(SEM)观察了试样的断口形貌和表面裂纹形貌,采用能谱仪(EDS)分析了裂纹尖端附近的元素... 采用慢应变速率试验(SSRT),研究了不同应变速率下国产镍基合金C-HRA-1在650℃、25MPa超临界水环境中的应力腐蚀开裂(SCC)敏感性。采用扫描电子显微镜(SEM)观察了试样的断口形貌和表面裂纹形貌,采用能谱仪(EDS)分析了裂纹尖端附近的元素组成及分布。结果表明:在不同应变速率下,C-HRA-1均表现出SCC敏感性,随着应变速率的降低,SCC敏感性逐渐升高;在应力腐蚀过程中,裂纹的形成与扩展受氧化和力学耦合作用的影响,裂纹尖端发生了晶界氧化,裂尖结合力降低,从而导致裂纹扩展。 展开更多
关键词 镍基合金 应变速率 应力腐蚀开裂(SCC) 超临界水
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绝缘子引线腐蚀断裂研究
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作者 高明起 徐玉娟 +2 位作者 张亚刚 董东 王强 《电镀与涂饰》 CAS 北大核心 2024年第1期50-58,共9页
[目的]绝缘子作为微波组件内、外部的连接器件,其引线与玻璃封接处容易断裂。[方法]采用金相显微镜、扫描电镜、能谱仪等手段对上述断裂的原因进行分析。[结果]通过机理探讨与现场观察相结合,确定症结在于应力腐蚀开裂。绝缘子引线断裂... [目的]绝缘子作为微波组件内、外部的连接器件,其引线与玻璃封接处容易断裂。[方法]采用金相显微镜、扫描电镜、能谱仪等手段对上述断裂的原因进行分析。[结果]通过机理探讨与现场观察相结合,确定症结在于应力腐蚀开裂。绝缘子引线断裂分为3个阶段:点蚀过程及裂纹萌生,裂纹扩展,以及纯力学快速断裂。[结论]采用化学抛光与机械研磨相结合、镍金交叉镀覆的新工艺可以消除绝缘子引线封接处镀层应力敏感性和应力条件,令镀层的结合力、耐盐雾性能及焊接性能均达到工艺要求。 展开更多
关键词 绝缘子 引线 断裂 应力腐蚀 化学抛光 交叉镀覆
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