Effects of different helium cooling conditions on the structures of GH4169 alloy vacuum arc remelting ingots

The effects of different helium cooling conditions on the molten pool depth,dendrite structure,and microsegregation of GH4169 alloy ?508 mm vacuum arc remelting( VAR) ingots were studied using an optical microscope and an electron probe. The results show that under different helium cooling conditions,the growth of columnar crystals in the VAR ingot is the same with a certain angle running from the edge to the center and the dendrites at the edges are relatively small whereas the dendrites near the center are large. As the helium cooling increased,the molten pool depth decreased from 137 mm to 120 mm. Observations of the microstructure showed that as the helium cooling increased,the secondary dendrite arm spacing( SDAS) decreased at the center and R/2 region. Also,the Laves phase content markedly decreased. Under the same helium cooling conditions,the SDAS and Laves phase content at the center were higher than that at the R/2 region. Thus,more intense helium cooling effectively reduced segregation in VAR ingots and improved the metallurgical quality.

航空用GH4169合金组织检测标准分析

针对先进航空发动机关键零件广泛应用的骨干高温合金GH4169，介绍了国内外材料组织检测标准现状，分析国外IN718合金低倍和显微组织检验与评定标准、不均匀晶粒度评定标准的特点，以及国内航空用GH4169合金组织检测标准现状，提出研究制定《航空用GH4169合金低倍和显微组织检验与评定55,《航空用GH4169合金晶粒度评定方法》国军标的建议，为航空用GH4169合金高低倍组织检测与评价提供技术依据。

Temperature dependence in tensile properties and deformation behavior of GH4169 alloy

The effect of temperature on the tensile properties and deformation mechanism of GH4169 alloy has been systematically studied over a wide range of room temperature(RT)to 1000℃.The results indicate that the stress–strain curve of the alloy shows serrations at 200–600℃,and the character of the serrations changes from type A to type B and then to type C at different temperatures.The ultimate tensile strength of the alloy decreases gradually from RT to 600℃.The yield strength decreases slowly from RT to 700℃ but decreases rapidly above 800℃.Transmission electron microscopy analysis relieves that the primary deformation mechanism of the alloy below 500℃ is Orowan bypass mechanism.At temperatures between 600 and 700℃,the coordinated deformation of twins and cross-slip of dislocations are activated.The transformation of\upgamma^{\prime\prime}phase toδphase above 650℃ will decrease the strength.The primary deformation mechanism above 800℃ transforms into the repeated shearing of\upgamma^{\prime\prime}by dislocations to form multiple stacking faults.Recrystallized grains were observed above 800℃,and continuous dynamic recrystallization and discontinuous dynamic recrystallization were observed.The stress concentration caused by Nb-rich carbides is the cause of intracrystalline crack nucleation.At 700℃,grain boundary crack sprouting is caused by the combined effect of slip band impact on grain boundaries and grain boundary dislocation plugging.The relationship between the serrated flow behavior and the deformation mechanism has been discussed based on the experimental results.

Oxidation damage zone formed in creep fatigue crack growth of GH4169 alloy at 650℃

In the creep fatigue crack growth of GH4169 alloy,oxidation is a prominent damage source,which is mainly manifested as the oxidation damage zone in front of crack tip.In order to investigate the property of the oxidation damage zone formed in the creep fatigue crack growth,crack growth tests of directly aged GH4169 alloy were conducted at 650℃ in air under various load conditions.Interrupted tests were performed to observe the damage characteristics at crack tip.Block tests were systematically executed to quantify the dependency of oxidation damage zone size on load and holding time.The crack propagation of the GH4169 alloy has a close relationship with grain boundary oxidation at 650℃.An oxidation damage zone in front of crack tip includes intergranular microcracks and oxidised but uncracked grain boundaries.Its size has been calculated from transient crack growth rate and described as a function of maximum stress intensity factor and holding time.Based on oxidation damage zone size,a novel model has been developed to predict the creep fatigue crack growth rate of the GH4169 alloy at 650℃.

Performance of GH4169 brazed joint using a new designed nickel-based filler metal via cluster-plus-glue-atom model

A novel Ni-Cr-Si-B filler metal with the cluster formula of[Cr-Ni12]B2Cr+[B-Ni8Cr]BSi Cr based on the cluster-plus-glue-atom model was designed for vacuum brazing GH4169 alloy.The effect of brazing temperature and brazing time on microstructure and shear strength of GH4169 alloy joints was investigated.The brazed seam was mainly composed ofγ-Ni solid solution.(Nb,Ti)-rich phase and(Cr,Nb,Mo)-rich borides distributed in diffusion zones.The diffusion and aggregation of B,Cr,Nb,and Mo resulted in the variation of phase contrast and morphology of borides.Coarse precipitations in the joint brazed at1240℃consisted of borides,Laves phase andδphase.The shear strength of joints was principally dominated by the brittle precipitations in diffusion zone,and the homogenization of microstructure improved the room-temperature shear strength to 820 MPa with the high-temperature shear strength of 627 MPa for the joint brazed at 1240℃/20 min.The joint fractured in diffusion zone and brazed seam,and the existence of borides and Laves phase in diffusion zone provide the potential origin for crack growth.

Dynamic recrystallization behavior of GH4169G alloy during hot compressive deformation

The microstructure evolutions and nucleation mechanisms of GH4169G alloy were studied by optical microscope, electron backscatter diffraction (EBSD) and transmission electron microscope (TEM). The hot compression tests were performed different imposed reductions in the range of true strain from 0.12 to 1.2 at the temperatures of 930 °-1050 ° with strain rates of 0.01 s^-1-l s^-1. It is found that cumulative and local misorientation increase firstly and then decrease when the strain is increased due to the progress of dynamic recrystallization (DRX). The low angle boundaries (LAGBs) rapidly develop to high angle boundaries (HAGBs) at relatively high deformation temperature or the low strain rate. There are three DRX mechanisms observed for GH4169 G alloy during hot deformation. Discontinuous dynamic recrystallization (DDRX) as the dominant mechanism for GH4169 G alloy is characterized by typical necklace structures and bulged-original boundaries. Besides, different deformation bands with dislocation cells formed in deformed matrix at low temperature and large strain, which indicates that continuous dynamic recrystallization (CDRX) contributed to the DRX process. The twin boundaries lost their coherent characteristics and provide sites for nucleation, which also accelerates the nucleation of DRX.

Simulation and experimental investigation of inner-jet electrochemical grinding of GH4169 alloy

GH4169 alloy is one of the most commonly used materials in aero engine turbine blades,but its machinability is poor because of its excellent strength at high temperatures. Electrochemical machining（ECM） has become a common method for machining this alloy and other difficult-tomachine materials. Electrochemical grinding（ECG） is a hybrid process combining ECM and conventional grinding. In this paper, investigations conducted on inner-jet ECG of GH4169 alloy are described. Two types of inner-jet ECG grinding wheels were used to machine a flat bottom surface.The machining process was simulated using COMSOL software, and machining gaps under different machining parameters were obtained. In addition, maximum feed rates and maximum material removal rates under different machining parameters were studied experimentally. The maximum sizes and the uniformity of the distributions of the gaps machined by the two grinding wheels were compared. The effects of different applied voltages on the machining results were also investigated.

Effect of δ Phase on Mechanical Properties of GH4169 Alloy at Room Temperature

Tensile tests of GH4169 alloy were performed at room temperature. Different fractions, distributions and shapes of δ phase was prepared by aging treated at 880 ℃, 930 ℃ and 980 ℃ for 5 h or 10 h. The effect of δ phase on the mechanical pro- perties of GH4169 alloy was investigated. The results show that 0.2% yield strength and ultimate tensile strength of GH4169 alloy increase by 61 MPa and 78 MPa respectively when the fraction of δ phase increases from 2.20% to 5.21%. Then, the ultimate tensile strength remains at 1 012 MPa even when the fraction of δ phase reaches 7.56%. The fraction effect of δ phase on the strength improvement of GH4169 alloy is more significant than morphology, and the critical fraction value is 5.21%. In addition, the elongation decreases by 14.1% when the fraction of δ phase increases from 2.20% to 7.56%. Excessive needle or short rod shaped 8 ohase is resoonsible for the reduction of eloneation.

A New Strategy for Restraining Dynamic Strain Aging in GH4169 Alloy During Tensile Deformation at High Temperature

The dynamic strain aging(DSA) behavior was investigated in GH4169 alloy during tensile deforming with electric-pulse current(EPC) at 750 ℃.The results show that DSA is restrained in the alloy when deformed with 40 Hz-EPC.The size ofγ " phase inner grains increases obviously and δ phase is facilitated to precipitate on grain boundary in the alloy applied with EPC,due to the promotion effect of EPC on the diffusion and segregation of atoms.Transmission electron microscopy(TEM)results indicate that dislocations can cut through small γ" precipitate with the size of less than 10 nm,while dislocations can only bypass dislocations when γ " precipitate grow up over 20 nm.The growth of precipitates consumes large amounts of atoms as well as the velocity of dislocation increase,which makes dislocations difficult to be pinned.Therefore,when γ" precipitates grow up to a large size more than the critical size of dislocation pinning,DSA is significantly restrained in the alloy after necking deformed with EPC.

Effect of Cold Rolling Parameters on the Longitudinal Residual Stress Distribution of GH4169 Alloy Sheet

For plastic deformed parts, the dimensional accuracy is significantly affected by residual stresses and so does the performance in service. Therefore, the rolling process of GH4169 alloy sheet at room temperature was investigated by finite element method. The effects of rolling reduction, friction coefficient, rolling velocity and initial stress on the longitudinal residual stress distribution over the thickness of GH4169 alloy sheet were analyzed. The results show that the values of longitudinal residual stress can be slightly reduced by increasing the rolling reduction and velocity. The longitudinal residual stress over the thickness distributes as ‘‘V＇＇ type or weak ‘‘W＇＇ type. The initial stress mainly has an effect on the longitudinal stress in the backward slip area. But the friction coefficient has remarkable influence on longitudinal residual stress. With the friction coefficient increasing from 0.1 to 0.5, the value of longitudinal residual stress on the sheet surface is reduced by 282 MPa. Simultaneously, the tensile stress turns into compressive stress with a strong‘‘W＇＇ type distribution.