Food safety problems caused by excessive nitrite addition have been frequently reported and the detection of nitrite in food is particularly important. The standing time during the pretreatment of primary sample has a...Food safety problems caused by excessive nitrite addition have been frequently reported and the detection of nitrite in food is particularly important. The standing time during the pretreatment of primary sample has a great influence on the concentration of nitrite tested by spectrophotometric method. In this context, three kinds of food samples are prepared, including canned mustard, canned fish and home-made pickled water. A series of standing times are placed during the sample pretreatments and the corresponding nitrite contents in these samples are detected by spectrophotometric method based on N-ethylenediamine dihydrochloride. This study aims to find out a reasonable standing time during the pretreatment of food sample, providing influence factor for precise detection of nitrite.展开更多
A high sensitive long period fiber grating（LPFG） sensor for the detection of nitrite is proposed, which is realized by coating multiple poly（sodium 4-styrensulfonate）（PSS） and poly（diallyldimethylammonium） chl...A high sensitive long period fiber grating（LPFG） sensor for the detection of nitrite is proposed, which is realized by coating multiple poly（sodium 4-styrensulfonate）（PSS） and poly（diallyldimethylammonium） chloride （PDDA） layers on the fiber grating surface. The sensitivity of this LPFG sensor is maximum when the number of assembled layers is 70. Under this condition, a nitrite concentration of 3×10^-3 mol/L, which is lower than the National Food Additive Standard, 4.2×10^-3 mol/L, can be distinguished. The sensitivity is further increased by 30% when nitrite was determined in the sucrose solution with a concentration of 65%, which provides a new solution for the best refraction index approaching matched index of the fiber cladding. Compared with chemical methods, this nitrite detection technology offers some advantages, such as high accuracy, non toxicity, high speed, low cost, without chemical reagent, and is suitable for foodstuff security detection.展开更多
文摘Food safety problems caused by excessive nitrite addition have been frequently reported and the detection of nitrite in food is particularly important. The standing time during the pretreatment of primary sample has a great influence on the concentration of nitrite tested by spectrophotometric method. In this context, three kinds of food samples are prepared, including canned mustard, canned fish and home-made pickled water. A series of standing times are placed during the sample pretreatments and the corresponding nitrite contents in these samples are detected by spectrophotometric method based on N-ethylenediamine dihydrochloride. This study aims to find out a reasonable standing time during the pretreatment of food sample, providing influence factor for precise detection of nitrite.
基金Supported by the National Natural Science Foundation of China(Nos.60707016 and 60807030)
文摘A high sensitive long period fiber grating（LPFG） sensor for the detection of nitrite is proposed, which is realized by coating multiple poly（sodium 4-styrensulfonate）（PSS） and poly（diallyldimethylammonium） chloride （PDDA） layers on the fiber grating surface. The sensitivity of this LPFG sensor is maximum when the number of assembled layers is 70. Under this condition, a nitrite concentration of 3×10^-3 mol/L, which is lower than the National Food Additive Standard, 4.2×10^-3 mol/L, can be distinguished. The sensitivity is further increased by 30% when nitrite was determined in the sucrose solution with a concentration of 65%, which provides a new solution for the best refraction index approaching matched index of the fiber cladding. Compared with chemical methods, this nitrite detection technology offers some advantages, such as high accuracy, non toxicity, high speed, low cost, without chemical reagent, and is suitable for foodstuff security detection.
