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Evolution of Bond-Order-Wave Phase in One-Dimensional Mott Insulators 被引量:3
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作者 HUANG Xiao-Xuan PAN Zheng-Quan +2 位作者 XU Zhao-Xin DAI Jian-Hui YING He-Ping 《Communications in Theoretical Physics》 SCIE CAS CSCD 2006年第5X期923-928,共6页
In this paper, by using the level spectroscopy method and bosonization theory, we discuss the evolution of the bond-order-wave (BOW) phase in a one-dimensional half-filled extended Hubbard model wlth the on-site Cou... In this paper, by using the level spectroscopy method and bosonization theory, we discuss the evolution of the bond-order-wave (BOW) phase in a one-dimensional half-filled extended Hubbard model wlth the on-site Coulomb repulsion U as well as the inter-site Coulomb repulsion V and antiferromagnetic exchange J. After clarifying the generic phase diagrams in three limiting cases with one of the parameters being fixed at zero individually, we find that the BOW phase in the U-V phase diagram is initially enlarged as J increases from zero but is eventually suppressed as J increases further in the strong-coupling regime. A three-dimensional phase diagram is suggested where the BOW phase exists in an extended region separated from the spin-density-wave and charge-density-wave phases. 展开更多
关键词 bond-order-wave phase Mott insulators one-dimensional extended Hubbard model
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A novel phase-sensitive scanning near-field optical microscope 被引量:2
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作者 武晓宇 孙琳 +1 位作者 谭峭峰 王佳 《Chinese Physics B》 SCIE EI CAS CSCD 2015年第5期346-351,共6页
Phase is one of the most important parameters of electromagnetic waves. It is the phase distribution that determines the propagation, reflection, refraction, focusing, divergence, and coupling features of light, and f... Phase is one of the most important parameters of electromagnetic waves. It is the phase distribution that determines the propagation, reflection, refraction, focusing, divergence, and coupling features of light, and further affects the intensity distribution. In recent years, the designs of surface plasmon polariton (SPP) devices have mostly been based on the phase modulation and manipulation. Here we demonstrate a phase sensitive multi-parameter heterodyne scanning near-field opti- cal microscope (SNOM) with an aperture probe in the visible range, with which the near field optical phase and amplitude distributions can be simultaneously obtained. A novel architecture combining a spatial optical path and a fiber optical path is employed for stability and flexibility. Two kinds of typical nano-photonic devices are tested with the system. With the phase-sensitive SNOM, the phase and amplitude distributions of any nano-optical field and localized field generated with any SPP nano-structures and irregular phase modulation surfaces can be investigated. The phase distribution and the interference pattern will help us to gain a better understanding of how light interacts with SPP structures and how SPP waves generate, localize, convert, and propagate on an SPP surface. This will be a significant guidance on SPP nano-structure design and optimization. 展开更多
关键词 phase detection scanning near-field optical microscope (SNOM) heterodyne interferometry surface plasmon polariton (SPP) devices
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Comparison of One-Dimensional Analysis with Experiment for CO<sub>2</sub>Two-Phase Nozzle Flow 被引量:1
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作者 Wakana Tsuru Satoshi Ueno +1 位作者 Yoichi Kinoue Norimasa Shiomi 《Open Journal of Fluid Dynamics》 2014年第5期415-424,共10页
The aim of this study is to investigate CO2 two-phase nozzle flow in terms of both experimental and analytical aspects for the optimum design of two-phase flow nozzle of CO2 two-phase flow ejector. In the experiment, ... The aim of this study is to investigate CO2 two-phase nozzle flow in terms of both experimental and analytical aspects for the optimum design of two-phase flow nozzle of CO2 two-phase flow ejector. In the experiment, it is measured that the temperature profile in the stream-wise direction of a divergent-convergent nozzle through which CO2 in the supercritical pressure condition is blown down into the atmosphere. In the analysis, a one-dimensional model which assumes steady, adiabatic, frictionless, and equilibrium is proposed. In the convergent part of the nozzle the flow is treated as single-phase flow of liquid, whereas in the divergent part the flow is treated as separated two-phase flow with saturated condition. The analytical results indicate that the temperature and the pressure decrease rapidly in the divergent part, and the void fraction increases immediately near the throat. Although this analysis is quite simple, the analytical results can follow the experimental results well within this study. 展开更多
关键词 Carbon Dioxide High-Speed Nozzle FLOW Gas-Liquid TWO-phase FLOW with phase Change Blow down Test one-dimensional ANALYSIS
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Phase matched scanning optical parametric chirped pulse amplification based on pump beam deflection
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作者 Rong Ye Huining Dong +1 位作者 Xianyun Wu Xiang Gao 《Chinese Physics B》 SCIE EI CAS CSCD 2021年第10期351-355,共5页
Combined with the optical beam deflection,a novel approach of phase matched broadband scanning optical parametric chirped pulse amplification(OPCPA)was proposed.For this scheme,there was no superfluous operations to t... Combined with the optical beam deflection,a novel approach of phase matched broadband scanning optical parametric chirped pulse amplification(OPCPA)was proposed.For this scheme,there was no superfluous operations to the chirped signal pulse which propagated in a changeless direction straightforward,but the pump beam were deflected in space with time by passing through a KTN crystal,which was applied with varied driving voltage.The theories of phase matching of each chirped signal frequency based on pump beam deflection was analyzed detailedly.And the type-I amplification of chirped signal with 800 nm central wavelength and 20 nm bandwidth pumped by 532 nm in BBO crystal was simulated as a case in point.The simulation results showed that the spectral distribution of chirped signal pulse was almost the same as the initial form,i.e.,there was nearly no narrowing on the amplified spectrum by using of the scanning OPCPA based on pump beam deflection.In addition,the simulations demonstrated that it was worth minimizing the voltage deviation applied to KTN crystal as much as possible for the sake of better waveform,larger bandwidth and higher conversion efficiency of amplified signal pulse in the proposed scanning OPCPA. 展开更多
关键词 optical parametric chirped pulse amplification optical beam deflection phase matching scanning KTN crystal
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Topological phase in one-dimensional Rashba wire
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作者 汪萨克 汪军 刘军丰 《Chinese Physics B》 SCIE EI CAS CSCD 2016年第7期393-400,共8页
We study the possible topological phase in a one-dimensional(1D) quantum wire with an oscillating Rashba spin–orbital coupling in real space. It is shown that there are a pair of particle–hole symmetric gaps formi... We study the possible topological phase in a one-dimensional(1D) quantum wire with an oscillating Rashba spin–orbital coupling in real space. It is shown that there are a pair of particle–hole symmetric gaps forming in the bulk energy band and fractional boundary states residing in the gap when the system has an inversion symmetry. These states are topologically nontrivial and can be characterized by a quantized Berry phase ±π or nonzero Chern number through dimensional extension. When the Rashba spin–orbital coupling varies slowly with time, the system can pump out 2 charges in a pumping cycle because of the spin flip effect. This quantized pumping is protected by topology and is robust against moderate disorders as long as the disorder strength does not exceed the opened energy gap. 展开更多
关键词 one-dimensional topological phase Rashba spin–orbit interaction spatial modulation quantized pump
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Wide-Angle Scanning Antennas for Millimeter-Wave 5G Applications 被引量:4
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作者 Raj Mittra Abdelkhalek Nasri Ravi Kumar Arya 《Engineering》 SCIE EI 2022年第4期60-71,共12页
The fifth generation(5G)network communication systems operate in the millimeter waves and are expected to provide a much higher data rate in the multi-gigabit range,which is impossible to achieve using current wireles... The fifth generation(5G)network communication systems operate in the millimeter waves and are expected to provide a much higher data rate in the multi-gigabit range,which is impossible to achieve using current wireless services,including the sub-6 GHz band.In this work,we briefly review several existing designs of millimeter-wave phased arrays for 5G applications,beginning with the low-profile antenna array designs that either are fixed beam or scan the beam only in one plane.We then move on to array systems that offer two-dimensional(2D)scan capability,which is highly desirable for a majority of 5G applications.Next,in the main body of the paper,we discuss two different strategies for designing scanning arrays,both of which circumvent the use of conventional phase shifters to achieve beam scanning.We note that it is highly desirable to search for alternatives to conventional phase shifters in the millimeter-wave range because legacy phase shifters are both lossy and costly;furthermore,alternatives such as active phase shifters,which include radio frequency amplifiers,are both expensive and power-hungry.Given this backdrop,we propose two different antenna systems with potential for the desired 2D scan performance in the millimeter-wave range.The first of these is a Luneburg lens,which is excited either by a 2D waveguide array or by a microstrip patch antenna array to realize 2D scan capability.Next,for second design,we turn to phased-array designs in which the conventional phase shifter is replaced by switchable PIN diodes or varactor diodes,inserted between radiating slots in a waveguide to provide the desired phase shifts for scanning.Finally,we discuss several approaches to enhance the gain of the array by modifying the conventional array configurations.We describe novel techniques for realizing both one-dimensional(1D)and 2D scans by using a reconfigurable metasurface type of panels. 展开更多
关键词 Luneburg lens scanning arrays Millimeter-wave antennas Switchable phase shifters Reconfigurable metasurfaces
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A First Principles Simulation Framework for the Interactions between a Si(001) Surface and a Scanning Probe
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作者 Dung Q. Ly Charalampos Makatsoris 《Journal of Surface Engineered Materials and Advanced Technology》 2012年第3期194-202,共9页
By means of total energy calculations within the framework of the local density approximation (LDA), the interactions between a silicon Si(001) surface and a scanning probe are investigated. The tip of the probe, comp... By means of total energy calculations within the framework of the local density approximation (LDA), the interactions between a silicon Si(001) surface and a scanning probe are investigated. The tip of the probe, comprising 4 Si atoms scans along the dimer lines above an asymmetric p(2 × 1) surface, at a distance where the chemical interaction between tip-surface is dominant and responsible for image resolution. At that distance, the tip causes the dimer to toggle when it scans above the lower atom of a dimer. The toggled dimers create an alternating pattern, where the immediately adjacent neighbours of a toggled dimer remain unchanged. After the tip has fully scanned across the p(2 × 1) surface, causes the dimers to arrange in a p(2 × 2) reconstruction, reproducing the images obtained in scanning probe experiments. Our modelling methodology includes simulations that reveal the energy input required to overcome the barrier to the onset of dimer toggling. The results show that the energy input to overcome this barrier is lower for the p(2 × 1) surface than that for the p(2 × 2) or c(4 × 2) surfaces. 展开更多
关键词 DFT Si(001)-p(2 × 1) p(2 × 2) c(4 × 2) scanning Probe Microscopy phase TRANSITIONS DIMER Toggling
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6-9 Python-based Phase Scan Application for ADS Linac
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作者 Hu Jianjun Wang Wangsheng Wang Zhijun 《IMP & HIRFL Annual Report》 2015年第1期270-270,共1页
Phase scan application is very important software for ADS Linac beam tuning. The scan/measure tools in OpenXAL was used previously. In order to improve the scanning efficiency, a new phase scan application was develop... Phase scan application is very important software for ADS Linac beam tuning. The scan/measure tools in OpenXAL was used previously. In order to improve the scanning efficiency, a new phase scan application was developed. The Python was selected as the programming language to make the development easier. 展开更多
关键词 phase scan APPLICATION
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Theory of Z-scan technique using Gaussian-Bessel beams with a phase object
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作者 金肖 税敏 +5 位作者 王玉晓 李常伟 杨俊义 张学如 杨昆 宋瑛林 《Chinese Physics B》 SCIE EI CAS CSCD 2010年第7期251-255,共5页
This paper reports the theoretical study of combining Z-scan technique with Gauss-Bessel (GB) beams beside a phase object (PO) to measure the third-order nonlinear susceptibility components. By using this method, ... This paper reports the theoretical study of combining Z-scan technique with Gauss-Bessel (GB) beams beside a phase object (PO) to measure the third-order nonlinear susceptibility components. By using this method, the sign of refractive index which depends on the shape of the close aperture Z-scan curve can be easily determined. Meanwhile, the magnitude of nonlinear coefficients can also be deduced by theoretical fit. The proposed method is advantageous for high sensitivity and imposes a lower stress in the cases of fragile materials, since small pulse energy is enough for the measurement of nonlinear coefficients. Predictions of the models are compared with Gaussian Z-scan measurement and GB Z-scan measurement. By using GB beams with a PO, the sensitivity of Z-scan measurements is found to be a factor of over 60 times greater than for Gaussian beams and 2 times greater than for Gaussian-Bessel beams. 展开更多
关键词 Gaussian-Bessel beams phase object Z-scan
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非线性相移对Z-scan曲线对称性的影响
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作者 王超 唐天同 康轶凡 《强激光与粒子束》 EI CAS CSCD 北大核心 2007年第10期1619-1622,共4页
基于由光束传输的ABCD矩阵得出的Z-scan透过率的解析结果,分析了Z-scan实验曲线随非线性相移的变化规律。发现随着相移的增加,折射非线性相移比吸收非线性相移对Z-scan曲线对称性的影响更大。对于具有强饱和吸收和弱自聚焦特性的非线性... 基于由光束传输的ABCD矩阵得出的Z-scan透过率的解析结果,分析了Z-scan实验曲线随非线性相移的变化规律。发现随着相移的增加,折射非线性相移比吸收非线性相移对Z-scan曲线对称性的影响更大。对于具有强饱和吸收和弱自聚焦特性的非线性介质,其Z-scan曲线随非线性折射相移的变小将失去典型的类色散特点。对于1μm厚的ZnCdSe-ZnSe多量子阱,扫描光源采用532 nm的基模高斯光束,采用透过率表达式来拟合所得的实验数据,在吸收非线性相移为0.9与耦合因子为-10条件下,推算出三阶非线性吸收系数为2×10-3cm/W,三阶非线性折射系数为8.0×10-8cm2/W,这与J.Ma等人的结果吻合。最后对曲线特征参数随非线性相移变化进行了数值计算,得到的曲线所对应的非线性相移与曲线谷位置的乘积近似为一常量,值为0.166。 展开更多
关键词 非线性相移 Z-scan方法 定量分析 类色散 不对称性
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Growth and characteristics of InAsSb epilayers with a cutoff wavelength of 4.8 μm prepared by one-step liquid phase epitaxy 被引量:3
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作者 GAO Yuzhu GONG Xiuying +1 位作者 FANG Weizheng Akihiro Ishida 《Rare Metals》 SCIE EI CAS CSCD 2009年第4期313-316,共4页
InAsSb epilayers with a cutoff wavelength of 4.8 μm have been successfully grown on InAs substrates by one-step liquid phase epitaxy (LPE) technology. The epilayers were characterized by X-ray diffraction (XRD), ... InAsSb epilayers with a cutoff wavelength of 4.8 μm have been successfully grown on InAs substrates by one-step liquid phase epitaxy (LPE) technology. The epilayers were characterized by X-ray diffraction (XRD), Fourier transform infrared (PTIR) transmittance measurements and scanning electron microscopy (SEM). The influence of different growth conditions on the optical and structural properties of the materials was studied. The results revealed that the good crystalline quality, mirror smooth surface and flat interface of InAsSb epilayers were achieved. They benefited from optimized growth conditions, i.e., sufficient homogeneity of the growth melt and a very slow cooling rate. 展开更多
关键词 INASSB liquid phase epitaxy crystalline quality cutoff wavelength scanning electron microscopy
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A two-step transient liquid phase diffusion bonding process of T91 steels 被引量:4
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作者 Chen Sijie Tang Hengjuan Zhao Pifeng 《China Welding》 EI CAS 2017年第2期52-57,共6页
In this study, a two-step heating process is introduced for transient liquid phase ( TLP) diffusion bonding fo r sound joints with T91 heat resistant steels. At first, a short-time higher temperature heatin... In this study, a two-step heating process is introduced for transient liquid phase ( TLP) diffusion bonding fo r sound joints with T91 heat resistant steels. At first, a short-time higher temperature heating step is addressed to melt the interlayer, followed by the second step to complete isothermal solidification at a low temperature. The most critical feature of our new method is producing a non-planar interface at the T9/ heat resistant steels joint. We propose a transitional liquid phase bonding of T91 heat resistant steels by this approach. Since joint microstructures have been studied, we tested the tensile strength to assess joint mechanical property. The result indicates that the solidified bond may contain a primary solid-solution, similar composition to the parent metal and free from precipitates. Joint tensile strength of the joint is not lower than parent materials. Joint bend's strengths are enhanced due to the higher metal-to-metal junction producing a non-planar bond lines. Nevertheless, the traditional transient liquid phase diffusion bonding produces planar ones. Bonding parameters of new process are 1 260 °C for 0. 5 min and 1 230 °C fo r 4 min. 展开更多
关键词 T91 transient liquid phase diffusion bonding two-step heating process scanning electron microscopy
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Effects of beryllium and iron additions on iron-bearing phase in A357 aluminum alloys 被引量:2
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作者 Chen Zhongwei Zhang Haifang Zhang Ruijie 《China Foundry》 SCIE CAS 2010年第3期275-277,共3页
Iron is the most deleterious impurity in the Al-Si-Mg casting alloys and can easily form inter-metallic compounds that can significantly affect the subsequent behavior of material properties.Using differential scannin... Iron is the most deleterious impurity in the Al-Si-Mg casting alloys and can easily form inter-metallic compounds that can significantly affect the subsequent behavior of material properties.Using differential scanning calorimetry (DSC) and microstructural analysis, how the Be and Fe additions affect the iron-bearing phase in A357 alloys was investigated.The results show that the iron-bearing phase in A357 alloy comprises mainly the plate-like β-Al5FeSi and a small quantity of the script-type π-Al8FeMg3Si6; and that the plate-like β-Al5FeSi proportion increases with increasing iron content in the alloy.The iron-bearing phase is mostly transformed from the plate-like β-Al5FeSi to the script-type π-Al8FeMg3Si6 with the addition of Be in the alloy.The hardness of alloy samples was also tested.The results show that both the increasing iron content and Be content can increase the hardness of the alloy.This may be contributed to the change of morphology and distribution of the iron-bearing phase in A357 alloy with the addition of iron or Be to the alloy. 展开更多
关键词 SOLIDIFICATION differential scanning calorimetry (DSC) A357 aluminum alloy microstructure iron-bearing phase
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Low-temperature phase transitions of sodium aluminate solutions 被引量:5
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作者 Wei LIU Zhou-lan YIN Zhi-ying DING 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第1期194-199,共6页
A series of low-temperature phase transitions of sodium aluminate solutions were studied by differential scanning calorimetry (DSC) and Raman spectroscopy. The results indicate that NaOH concentration is a primary imp... A series of low-temperature phase transitions of sodium aluminate solutions were studied by differential scanning calorimetry (DSC) and Raman spectroscopy. The results indicate that NaOH concentration is a primary impact factor for the binary eutectic point and ice melting temperature of sodium aluminate solutions with low NaOH concentration. In addition, the phase transition process of sodium aluminate solutions with low NaOH concentration from 123.15 to 283.15 K is divided into four steps: non-crystal to crystal, ternary eutectic reaction, binary eutectic reaction and ice melt. The projection phase diagram of NaOH-Al(OH)3-H2O system at low temperature was plotted, in which the ternary eutectic temperature for sodium aluminate solutions is 183.15 K. 展开更多
关键词 sodium aluminate solution low-temperature phase transition differential scanning calorimetry Raman spectroscopy eutectic reaction
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Preparation of Phase Change Microcapsule and Its Plication in Textiles 被引量:1
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作者 闵洁 寿晨燕 《Journal of Donghua University(English Edition)》 EI CAS 2010年第3期419-424,共6页
Phase change microcapsules(PCMs)are prepared with n-hexadecane and n-octadecane as core material,and melamine-formaldehyde resin is used as shell material by in-situ polymerization.Differential scanning calorimetry(DS... Phase change microcapsules(PCMs)are prepared with n-hexadecane and n-octadecane as core material,and melamine-formaldehyde resin is used as shell material by in-situ polymerization.Differential scanning calorimetry(DSC)was used to analyze the phase change properties.Thermal conductivity and maximum heat flux of cotton fabric finished with PCMs before and after being washed were also measured.It has been found that melting and crystal enthalpy of the PCMs decrease with decreasing the core/shell ratio,while qmax of fabric treated with PCMs decreases and the thermal conductivity increases.Study shows that fabric finished by the PCMs has good temperature conditioning function. 展开更多
关键词 phase change microcapsules qmax thermal conductivity COTTON differential scanning calorimetry(DSC)
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Phase Transition Behavior of Nanocrystalline Al<sub>2</sub>O<sub>3</sub>Powders 被引量:2
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作者 Balaraman Sathyaseelan Iruson Baskaran Kandasamy Sivakumar 《Soft Nanoscience Letters》 2013年第4期69-74,共6页
Alumina (Al2O3) has been synthesized through combustion synthesis (CS) technique. The calcined products were characterized using X-ray diffractional analysis (XRD), scanning electron microscopy (SEM), transmission ele... Alumina (Al2O3) has been synthesized through combustion synthesis (CS) technique. The calcined products were characterized using X-ray diffractional analysis (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and thermo-gravimetric analysis (TGA). TG-DTA results reveal the various stages involved in transition from γ-phase to α-Al2O3 phase. The first phase γ-Al2O3 was presented in the temperature range from 600°C-875°C as deduced from the XRD patterns with cubic crystal structure. The second stage occurs in the temperature range from 900°C-1000°C. In the final step, above 1000°C, the aluminium oxide appears completely as α-Al2O3, showing high crystallinity. The particle sizes are closely related to γ- to α-Al2O3 phase transition. 展开更多
关键词 NANOCRYSTALLINE Al2O3 phase Transitions Γ-AL2O3 Α-AL2O3 Differential scanning CALORIMETRY (DSC) Electron Microscopy (TEM and SEM)
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Dilute long period stacking/order(LPSO)-variant phases along the composition gradient in a Mg-Ho-Cu alloy 被引量:2
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作者 Kai Guan Daisuke Egusa Eiji Abe 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2022年第6期1573-1580,共8页
We have systematically investigated the microstructures of as-cast Mg_(97.49)Ho_(1.99)Cu_(0.43)Zr_(0.09)alloy by atomic resolution high-angle annular dark field scanning transmission electron microscopy(HAADF-STEM), r... We have systematically investigated the microstructures of as-cast Mg_(97.49)Ho_(1.99)Cu_(0.43)Zr_(0.09)alloy by atomic resolution high-angle annular dark field scanning transmission electron microscopy(HAADF-STEM), revealing the coexistence of 18R, 14H and 24R long period stacking/order(LPSO) phases with fully coherent interfaces along step-like composition gradient in a blocky intermetallic compound distributed at grain boundary. The short-range order(SRO) L1_(2)-type Cu_(6)Ho_(8)clusters embedded across AB’C’A-stacking fault layers are directly revealed at atomic scale. Importantly, the order degree of SRO clusters in the present dilute alloy is significant lower than previous 6M and 7M in-plane order reported in ternary Mg-TM(transition metal)-RE(rare earth) alloys, which can be well matched by 9M in-plane order. This directly demonstrates that SRO in-plane L1_(2)-type clusters can be expanded into more dilute composition regions bounded along the definite TM/RE ratio of 3/4. In addition, the estimated chemical compositions of solute enriched stacking fault(SESF) in all LPSO variants are almost identical with the ideal SESF composition of 9M in-plane order, regardless of the type of LPSO phases. The results further support the viewpoint that robust L1_(2)-type TM_(6)RE_(8)clusters play an important role in governing LPSO phase formation. 展开更多
关键词 Magnesium alloys Long period stacking/order(LPSO)phases Short-range order(SRO)clusters High-angle annular dark field scanning transmission electron microscopy(HAADF-STEM)
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A Review of Wideband Wide-Angle Scanning 2-D Phased Array and Its Applications in Satellite Communication 被引量:2
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作者 Yan Li Shaoqiu Xiao Jiajia Guo 《Journal of Communications and Information Networks》 2018年第1期21-30,共10页
In this review,research progress on the wideband wide-angle scanning two-dimensional phased arrays is summarized.The importance of the wideband and the wide-angle scanning characteristics for satellite communication i... In this review,research progress on the wideband wide-angle scanning two-dimensional phased arrays is summarized.The importance of the wideband and the wide-angle scanning characteristics for satellite communication is discussed.Issues like grating lobe avoidance,active reflection coefficient suppression and gain fluctuation reduction are emphasized in this review.Besides,techniques to address these issues and methods to realize the wideband wide-angle scanning phased array are reviewed. 展开更多
关键词 WIDEBAND wide-angle scanning twodimensional phased array satellite communication
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Thermodynamic Properties of CaCl<sub>2</sub>-CaF<sub>2</sub>-CaO System: Phase Diagram Investigation 被引量:1
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作者 Julien Claquesin Mathieu Gibilaro +3 位作者 Laurent Massot Olivier Lemoine Gilles Bourges Pierre Chamelot 《Materials Sciences and Applications》 2021年第4期139-151,共13页
The CaCl<sub>2</sub>-CaF<sub>2</sub>-CaO phase diagram was investigated in the CaO low region (<40 mol.%). CaCl<sub>2</sub>-CaF<sub>2</sub> and CaCl<sub>2</s... The CaCl<sub>2</sub>-CaF<sub>2</sub>-CaO phase diagram was investigated in the CaO low region (<40 mol.%). CaCl<sub>2</sub>-CaF<sub>2</sub> and CaCl<sub>2</sub>-CaO binary diagrams, constituting the ternary system, were first studied by Differential Scanning Calorimetry (DSC) measurements and X-Ray Diffraction (XRD) characterization;a good agreement was obtained between the phase diagram models calculated with FactSage&reg;software (FTsalt database) and present experimental data. As the CaF<sub>2</sub>-CaO liquidus could not be measured by DSC due to the high melting temperature, this diagram was calculated using FTsalt database combined with FToxid database of FactSage<sup>&reg;</sup> software. The ternary phase diagram was obtained by calculations and exhibits an eutectic at the composition CaCl<sub>2</sub>-CaF<sub>2</sub>-CaO (78.2-15.7-6.1 mol.%) melting at 637&deg;C, and five peritectic points. Measurements of relevant vertical cross-sections for three CaCl<sub>2</sub>-CaF<sub>2</sub> compositions (50-50, 40-60 and 30-70 mol.%) up to 18 mol.% CaO are in agreement with the ternary phase diagram model. For each section, the liquidus temperature is constant up to around 11 mol.% CaO and then sharply increases. Moreover, an increase of CaF<sub>2</sub> content in CaCl<sub>2</sub>-CaF<sub>2</sub> melt leads to a decrease of the CaO solubility in isothermal condition. 展开更多
关键词 Differential scanning Calorimetry (DSC) phase Diagram Calcium Chloride Calcium Fluoride Calcium Oxide Ternary System
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Austenite formation during intercritical annealing in C-Mn cold-rolled dual phase steel 被引量:1
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作者 李声慈 康永林 +1 位作者 朱国明 邝霜 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第4期1203-1211,共9页
Two different kinds of experimental techniques were used to in-situ study the austenite formation during intercritical annealing in C-Mn dual phase steel. The microstructure evolution was observed by confocal laser sc... Two different kinds of experimental techniques were used to in-situ study the austenite formation during intercritical annealing in C-Mn dual phase steel. The microstructure evolution was observed by confocal laser scanning microscope, and the austenite isothermal and non-isothermal transformation kinetics were studied by dilatometry. The results indicate that banded structure is produced for the reason of composition segregation and the competition between recrystallization and phase transformation. Austenite prefers to nucleate not only at ferrite/ferrite grain boundaries, but also inside the grains of ferrite.Furthermore, the austenitizing process is accomplished mainly via migration of the existing austenite/ferrite interface rather than nucleation of new grains. The incubation process can be divided into two stages which are controlled by carbon and manganese diffusion, respectively. During the incubation process, the nucleation rate of austenite decreases, and austenite growth changes from two-dimensional to one-dimensional. The partitioning coefficient, defined as the ratio of manganese content in the austenite to that in the adjacent ferrite, increases with increasing soaking time. 展开更多
关键词 dual phase steel confocal laser scanning microscope dilatometry austenitizing in situ observation
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