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EXPERIMENTAL STUDY OF OPTICALLY CONTROLLED DIELECTRIC RESONATOR OSCILLATOR
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作者 郭开周 L.A.Trinogga 杨荣生 《Journal of Electronics(China)》 1994年第2期180-186,共7页
Some new experimental results of optically controlled dielectric resonator oscillators (DROs) are presented. A very stable X-band DRO was found to be optically tunable up to 17.5 MHz with modulation rate of 1.17 MHz/m... Some new experimental results of optically controlled dielectric resonator oscillators (DROs) are presented. A very stable X-band DRO was found to be optically tunable up to 17.5 MHz with modulation rate of 1.17 MHz/mW with red light illumination. And an even higher modulation rate of 2.24 MHz/mW with illumination of violet light was obtained. Instead of a drop in optically controlled DRO output power, a little rise of output power was achieved. 展开更多
关键词 optically controlled MICROWAVE DIELECTRIC RESONATOR OSCILLATOR optically controlled frequency tuning
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Controllable Synthesis of Au NRs and Its Flexible SERS Optical Fiber Probe with High Sensitivity
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作者 熊文豪 WANG Wenbo +1 位作者 LONG Yuting 李宏 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第1期7-16,共10页
The surface-enhanced Raman scattering(SERS) optical fiber probes were successfully prepared by self-assembling on polyelectrolyte multilayers. Gold nanorods(Au NRs) were used as SERS enhancement material to give excel... The surface-enhanced Raman scattering(SERS) optical fiber probes were successfully prepared by self-assembling on polyelectrolyte multilayers. Gold nanorods(Au NRs) were used as SERS enhancement material to give excellent biological affinity and stability to the SERS optical fiber probes. Au NRs were synthesized by seed growth method. The synergistic effect between AgNO_(3) and surfactant was investigated, and the highest yield was found when AgNO_(3) was 500 uL. Meanwhile, different SERS optical fiber probes were obtained by selecting silane coupling agent, polyelectrolyte multilayer and graphene oxide(GO) to treat quartz fiber. It was found that the SERS optical fiber probes obtained by the self-assembled on polyelectrolyte multilayers method performed better than those by other methods. In addition, Mapping was combined with finite element simulation to analyze the electromagnetic field distribution at the fiber end face.The electromagnetic field distribution of Au NRs was investigated, the difference of electromagnetic field intensity around the Au NRs with different arrangements was compared, the strongest signal was obtained when the Au NRs were head-to-head. Finally, sensitivity of the optimized SERS optical fiber probes could reach 10^(-9)mol/L, with excellent stability and repeatability. 展开更多
关键词 surface-enhanced Raman scattering(SERS) optical fiber probe gold nanorods(Au NRs) polyelectrolyte multilayers controllable synthesis
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A New Type of Fiber-induced Optically Controllable Silicon-loaded Millimeter Waveguide Switch
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作者 李新碗 《High Technology Letters》 EI CAS 1996年第2期48-50,共3页
In this paper,a new type of optically controllable silicon slab loaded E-plane millimeterwave rectangular waveguide switch is presented.It uses SELFOC lens to couple optical puls-es to silicon slab with optical fiber.... In this paper,a new type of optically controllable silicon slab loaded E-plane millimeterwave rectangular waveguide switch is presented.It uses SELFOC lens to couple optical puls-es to silicon slab with optical fiber.The on/off ratio reaches 42dB,the front fringe of suchkind swith is less than 0.05μs,and the insertion loss is less than 1dB in the full band of 26.5GHz to 40GHz. 展开更多
关键词 optically controlLABLE WAVEGUIDE switch optical FIBER Silicon SLAB
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Control of light scattering by nanoparticles with optically-induced magnetic responses 被引量:2
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作者 刘伟 Andrey E. Miroshnichenko Yuri S. Kivshar 《Chinese Physics B》 SCIE EI CAS CSCD 2014年第4期41-51,共11页
Conventional approaches to control and shape the scattering pattems of light generated by different nanostructures are mostly based on engineering of their electric response due to the fact that most metallic nanostru... Conventional approaches to control and shape the scattering pattems of light generated by different nanostructures are mostly based on engineering of their electric response due to the fact that most metallic nanostructures support only electric resonances in the optical frequency range. Recently, fuelled by the fast development in the fields of metamaterials and plasmonics, artificial optically-induced magnetic responses have been demonstrated for various nanostructures. This kind of response can be employed to provide an extra degree of freedom for the efficient control and shaping of the scattering patterns of nanoparticles and nanoantennas. Here we review the recent progress in this research direction of nanoparticle scattering shaping and control through the interference of both electric and optically-induced magnetic responses. We discuss the magnetic resonances supported by various structures in different spectral regimes, and then summarize the original results on the scattering shaping involving both electric and magnetic responses, based on the interference of both spectrally separated (with different resonant wavelengths) and overlapped dipoles (with the same resonant wavelength), and also other higher-order modes. Finally, we discuss the scattering control utilizing Fano resonances associated with the magnetic responses. 展开更多
关键词 optically-induced magnetic response scattering control Mie resonance Fano resonance
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Optically Controllable Gray-Level Diffraction from a BCT Photonic Crystal Based on Azo Dye-Doped HPDLC
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作者 Shing-Trong Wu Chung-Hung Liu +2 位作者 Jui-Hsiang Liu Ming-Hsien Li Andy Ying-Guey Fuh 《Optics and Photonics Journal》 2014年第10期288-295,共8页
We investigated optically controllable gray-level diffraction from a body-centered tetragonal photonic crystal that was based on an azo-dye-doped holographic polymer dispersed liquid crystal. The sample is fabricated ... We investigated optically controllable gray-level diffraction from a body-centered tetragonal photonic crystal that was based on an azo-dye-doped holographic polymer dispersed liquid crystal. The sample is fabricated by use of two-beam interference with multi-exposure. Bichromatic pumping beams at various intensities were used to pump the sample to change the concentration of the cis isomer and, in turn, modulate the effective index of the photonic crystals as well as their diffraction intensity. Three pumping processes were utilized to produce gray-level switching of diffractive light. This study demonstrates the optimum gray-level to be 15-level of up-step and down-step. The simulation of the diffraction intensity under bichromatic pumping sources was also studied. 展开更多
关键词 All optically control Gray-Level Photonic CRYSTALS HPDLC
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All-optical switch and transistor based on coherent light-controlled single two-level atom coupling with two nanowires
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作者 Xin-Qin Zhang Xiu-Wen Xia +2 位作者 Jing-Ping Xu Mu-Tian Cheng Ya-Ping Yang 《Chinese Physics B》 SCIE EI CAS CSCD 2019年第11期179-185,共7页
Atom–nanowire coupling system is a promising platform for optical quantum information processing. Unlike the previous designing of optical switch and transistor requiring a dedicated multi-level emitter and high fine... Atom–nanowire coupling system is a promising platform for optical quantum information processing. Unlike the previous designing of optical switch and transistor requiring a dedicated multi-level emitter and high fineness microcavity,a new proposal is put forward which contains a single two-level atom asymmetrically coupled with two nanowires. Singleemitter manipulation of photonic signals for bilateral coherent incident is clear now, since we specify atomic saturation nonlinearity into three contributions which brings us a new approach to realizing light-controlled-light at weak light and single-atom levels. An efficient optically controllable switch based on self-matching-induced-block and a concise optical transistor are proposed. Our findings show potential applications in full-optical devices. 展开更多
关键词 opticAL transistor opticAL switch nano-waveguide light-controlled-light
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Obstacle Avoidance of Flapping⁃Wing Air Vehicles Based on Optical Flow and Fuzzy Control 被引量:12
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作者 FU Qiang WANG Jin +2 位作者 GONG Le WANG Jingyuan HE Wei 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI CSCD 2021年第2期206-215,共10页
The flapping-wing air vehicle(FWAV)is a kind of bio-inspired robot whose wings can flap up and down like bird and insect wings.A vision-based obstacle avoidance method for FWAVs is proposed in this paper.First,the Far... The flapping-wing air vehicle(FWAV)is a kind of bio-inspired robot whose wings can flap up and down like bird and insect wings.A vision-based obstacle avoidance method for FWAVs is proposed in this paper.First,the Farneback algorithm is used to calculate the optical flow field of the first-view video frames taken by the on-board image transmission camera.Based on the optical flow information,a fuzzy obstacle avoidance controller is then designed to generate the FWAV steering commands.Experimental results show that the proposed obstacle avoidance method can accurately identify obstacles and achieve obstacle avoidance for FWAVs. 展开更多
关键词 dense optical flow monocular vision obstacle avoidance flapping-wing air vehicle fuzzy control
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Comparison between iterative wavefront control algorithm and direct gradient wavefront control algorithm for adaptive optics system 被引量:1
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作者 程生毅 刘文劲 +3 位作者 陈善球 董理治 杨平 许冰 《Chinese Physics B》 SCIE EI CAS CSCD 2015年第8期391-397,共7页
Among all kinds of wavefront control algorithms in adaptive optics systems, the direct gradient wavefront control algorithm is the most widespread and common method. This control algorithm obtains the actuator voltage... Among all kinds of wavefront control algorithms in adaptive optics systems, the direct gradient wavefront control algorithm is the most widespread and common method. This control algorithm obtains the actuator voltages directly from wavefront slopes through pre-measuring the relational matrix between deformable mirror actuators and Hartmann wavefront sensor with perfect real-time characteristic and stability. However, with increasing the number of sub-apertures in wavefront sensor and deformable mirror actuators of adaptive optics systems, the matrix operation in direct gradient algorithm takes too much time, which becomes a major factor influencing control effect of adaptive optics systems. In this paper we apply an iterative wavefront control algorithm to high-resolution adaptive optics systems, in which the voltages of each actuator are obtained through iteration arithmetic, which gains great advantage in calculation and storage. For AO system with thousands of actuators, the computational complexity estimate is about O(n2) ~ O(n3) in direct gradient wavefront control algorithm, while the computational complexity estimate in iterative wavefront control algorithm is about O(n) ~(O(n)3/2), in which n is the number of actuators of AO system. And the more the numbers of sub-apertures and deformable mirror actuators, the more significant advantage the iterative wavefront control algorithm exhibits. 展开更多
关键词 adaptive optics iterative wavefront control algorithm direct gradient wavefront control algorithm
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Computer Controlled Polishing of the Off-axis Aspheric Mirrors 被引量:4
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作者 ZHANG Xue jun,WENG Zhi cheng,ZHANG Zhong yu, WANG Quan dou,ZHANG Feng (Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, Changchun 130022, China) 《光学精密工程》 EI CAS CSCD 2001年第5期467-473,共7页
In this paper, the manufacturing and testing procedures to make large off-axis aspherical mirrors are presented. The difficulties in polishing and testing for both circular aperture and rectangular aperture mirrors ar... In this paper, the manufacturing and testing procedures to make large off-axis aspherical mirrors are presented. The difficulties in polishing and testing for both circular aperture and rectangular aperture mirrors are previewed, and a possible solution is given. The two mirrors have been polished by means of CCOS, and the final accuracy is 25nm rms for 770mm×210mm rectangular mirror and 20nm rms for φ600mm circular mirror. These results just meet the optical tolerances specified by the designer, and the manufacturing and testing procedures presented here show good ability to make the large off-axis aspherical mirrors. 展开更多
关键词 asphere computer-controlled POLISHING opticAL TESTING
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Phase Control of Transient Optical Properties of Double Coupled Quantum-Dot Nanostructure via Gaussian Laser Beams 被引量:1
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作者 J.Shiri F.Shahi +1 位作者 M.R.Mehmannavaz L.Shahrassai 《Chinese Physics Letters》 SCIE CAS CSCD 2018年第2期29-33,共5页
We theoretically analyze the transient properties of a probe field absorption and dispersion in a coupled semiconductor double-quantum-dot nanostructure.We show that in the presence of the Gaussian laser beams,absorpt... We theoretically analyze the transient properties of a probe field absorption and dispersion in a coupled semiconductor double-quantum-dot nanostructure.We show that in the presence of the Gaussian laser beams,absorption and dispersion of the probe field can be dramatically influenced by the relative phase between applied fields and intensity of the Gaussian laser beams.Transient and steady-state behaviors of the probe field absorption and dispersion are discussed to estimate the required switching time.The estimated range is between 5-8 ps for subluminal to superluminal light propagation. 展开更多
关键词 Phase control of Transient optical Properties of Double Coupled Quantum-Dot Nanostructure via Gaussian Laser Beams QDs
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A Novel Stateful PCE-Cloud Based Control Architecture of Optical Networks for Cloud Services 被引量:1
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作者 QIN Panke CHEN Xue +1 位作者 WANG Lei WANG Liqian 《China Communications》 SCIE CSCD 2015年第10期117-127,共11页
The next-generation optical network is a service oriented network,which could be delivered by utilizing the generalized multiprotocol label switching(GMPLS) based control plane to realize lots of intelligent features ... The next-generation optical network is a service oriented network,which could be delivered by utilizing the generalized multiprotocol label switching(GMPLS) based control plane to realize lots of intelligent features such as rapid provisioning,automated protection and restoration(P&R),efficient resource allocation,and support for different quality of service(QoS) requirements.In this paper,we propose a novel stateful PCE-cloud(SPC)based architecture of GMPLS optical networks for cloud services.The cloud computing technologies(e.g.virtualization and parallel computing) are applied to the construction of SPC for improving the reliability and maximizing resource utilization.The functions of SPC and GMPLS based control plane are expanded according to the features of cloud services for different QoS requirements.The architecture and detailed description of the components of SPC are provided.Different potential cooperation relationships between public stateful PCE cloud(PSPC) and region stateful PCE cloud(RSPC) are investigated.Moreover,we present the policy-enabled and constraint-based routing scheme base on the cooperation of PSPC and RSPC.Simulation results for verifying the performance of routing and control plane reliability are analyzed. 展开更多
关键词 optical networks control plane GMPLS stateful PCE cloud computing Qo S
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Controlling and synchronizing spatiotemporal chaos of the coupled Bragg acousto-optical bistable map system using nonlinear feedback 被引量:12
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作者 岳立娟 沈柯 《Chinese Physics B》 SCIE EI CAS CSCD 2005年第9期1760-1765,共6页
In this paper we present the control and synchronization of a coupled Bragg acousto-optic bistable map system using nonlinear feedback technology. This nonlinear feedback technology is useful to control a temporally c... In this paper we present the control and synchronization of a coupled Bragg acousto-optic bistable map system using nonlinear feedback technology. This nonlinear feedback technology is useful to control a temporally chaotic system as well as a spatiotemporally chaotic system. It can be extended to synchronize the spatiotemporal chaos. It can work in a wide range of the controlled and synchronized signals, so it can decrease the sensitivity down to a noise level. The synchronization can be obtained by the analysis of the largest conditional Lyapunov exponent spectrum, and easily implemented in practical systems just by adjusting the coupled strength without any pre-knowledge of the dynamic system required. 展开更多
关键词 synchronization and control spatiotemporal chaos nonlinear feedback acousto-optic bistable map system
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Influences of control coherence and decay coherence on optical bistability in a semiconductor quantum well
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作者 艾剑锋 陈爱喜 邓黎 《Chinese Physics B》 SCIE EI CAS CSCD 2013年第2期283-286,共4页
We discuss the influences of two different types of mechanisms of quantum coherence on optical bistability in a semiconductor quantum well structure.In the first mechanism,only quantum coherence induced by the resonan... We discuss the influences of two different types of mechanisms of quantum coherence on optical bistability in a semiconductor quantum well structure.In the first mechanism,only quantum coherence induced by the resonant coupling of a strong control laser is considered.In the second mechanism,the decay coherence is taken into account under the condition where the control field is weak.In two different cases,optical bistability can be obtained through choosing appropriate physical parameters.Our studies show quantum coherence makes the optical nonlinear effect of the system become stronger,which takes an important role in the process of generating optical bistability.A semiconductor quantum well with flexibility and easy integration in design could potentially be exploited in real solid-state devices. 展开更多
关键词 optical bistability decay coherence control coherence
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Optical phase front control in a metallic grating with equally spaced alternately tapered slits
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作者 郑改革 吴义根 徐林华 《Chinese Physics B》 SCIE EI CAS CSCD 2013年第10期337-344,共8页
A technique capable of focusing and bending electromagnetic (EM) waves through plasmonic gratings with equally spaced alternately tapered slits has been introduced. Phase resonances are observed in the optical respo... A technique capable of focusing and bending electromagnetic (EM) waves through plasmonic gratings with equally spaced alternately tapered slits has been introduced. Phase resonances are observed in the optical response of transmission gratings, and the EM wave passes through the tuning slits in the form of surface plasmon polaritons (SPPs) and obtains the required phase retardation to focus at the focal plane. The bending effect is achieved by constructing an asymmetric phase front which results from the tapered slits and gradient refractive index (GRIN) distribution of the dielectric material. Rigorous electromagnetic analysis by using the two-dimensional (2D) finite difference time domain (FDTD) method is employed to verify our proposed designs. When the EM waves are incident at an angle on the optical axis, the beam splitting effect can also be achieved. These index-modulated slits are demonstrated to have unique advantages in beam manipulation compared with the width-modulated ones. In combination with previous studies, it is expected that our results could lead to the realization of ootimum designs for plasmonic nanolenses. 展开更多
关键词 surface plasmon polaritons optical phase front control metallic grating nanophotonic device
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Optical properties of CeO_2/Fe_3O_4 solar control glass coating
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作者 ZHAO Hongsheng LIU Bing HU Hongpo LI Ziqiang SHAO Youlin 《Rare Metals》 SCIE EI CAS CSCD 2006年第z1期351-354,共4页
A cerium-iron oxide solar control coating on glass was prepared by citric acid sol-gel method, dip-coating techniques and proper heat treatment process. Results show that the cerium-iron glass coating is composed of n... A cerium-iron oxide solar control coating on glass was prepared by citric acid sol-gel method, dip-coating techniques and proper heat treatment process. Results show that the cerium-iron glass coating is composed of nanocrystalline CeO2, Fe2O3, and nano holes. The cerium-iron glass coating has high transmittance in visible light, low UV and near IR transmittance. The wavelength of absorption edge for most glass coating has an obvious redshift to about 375 nm. There exist a wide absorption band at the range of 800-1600 nm and high transmittance at the wavelength from 400 nm to 800 nm, and the solar energy and visible transmittances are 50% and 65%, respectively. It ascribes to the high content of trivalence cerium and bivalence iron ions in the cerium/iron coating. It is indicated that this kind of glass coating has very good UV-sheering and heat-insulating property, can be used as an effective solar control glass in automobile and architecture. 展开更多
关键词 solar control glass coating sol-gel method optical properties
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QUANTITATIVE CONTROL OF OPTICAL CLEARING EFFECTS STUDIED WITH TISSUE-LIKE PHANTOM
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作者 JINGYING JIANG WEI CHEN +1 位作者 QILIANG GONG KEXIN XU 《Journal of Innovative Optical Health Sciences》 SCIE EI CAS 2010年第3期195-202,共8页
Tissue optical clearing by use of optical clearing agents(OCAs)has been proven to have potential to reduce the highly scattering effect of biological tissues in optical techniques.However,the difference in tissue samp... Tissue optical clearing by use of optical clearing agents(OCAs)has been proven to have potential to reduce the highly scattering effect of biological tissues in optical techniques.However,the difference in tissue samples could lead to unreliable results,making it difficult to quantitatively control the dose of OCAs during the course of tissue optical clearing.In this work,in order to study the effects of optical clearing,we customized tissue-like phantoms with optical properties of some biological tissue.Diffuse reflectance and total transmittance of tissue-like phantoms with different OCAs(DMSO or glycerol)and porcine skin tissues were measured.Then optical property parameters were calculated by inverse adding-doubling(IAD)algorithm.Results showed that OCAs could lead to a reduction in scattering of tissue-like phantoms as it did to porcine skin tissue in vitro.Furthermore,a series of relational expressions could be fit to quantitatively describe the relationship between the doses of OCAs and the reduction of scattering effects.Therefore,proper tissue-like phantom could facilitate optical clearing to be used in quantitative control of tissue optical properties,and further promote the application potential of optical clearing to light-based noninvasive diagnostic and therapeutic techniques. 展开更多
关键词 optical clearing effects tissue-like phantom quantitative control optical properties scattering effects optical clearing agents(OCAs)
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A Novel Optical Control Plane for Switching an Electro-Optical Hybrid Node in Translucent WDM Optical Networks
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作者 Sridhar Iyer Shree Prakash Singh 《Communications and Network》 2013年第1期57-68,共12页
In a translucent network scenario, development of an optical control plane (OCP) that is aware of the location and number of available regenerators and all-optical wavelength converters (AOWCs) is of paramount importa... In a translucent network scenario, development of an optical control plane (OCP) that is aware of the location and number of available regenerators and all-optical wavelength converters (AOWCs) is of paramount importance. However, current generalized multiprotocol label switching (GMPLS) protocol suite does not consider the distribution of regenerator and AOWC availability information to all the network nodes. In this paper, we propose a novel optical control plane (OCP) architecture that 1) disseminates information about network components (i.e. regenerators and AOWCs) to all the network nodes, and 2) evaluates candidate routes which use fewest amounts of network components. Performance of the proposed OCP is compared with a recently proposed hybrid OCP approach in terms of blocking performance, number of deployed components and lightpath establishment setup times. The obtained simulation results show that the proposed OCP approach demonstrates low connection blocking and establishes lightpaths by 1) minimizing the overall network cost owing to the deployment of minimum total number of network components, and 2) demonstrating acceptable lightpath establishment setup times at all traffic loads. Further, the proposed OCP methodology is compatible and suitable for controlling the operations of a novel electro-optical hybrid translucent node which is a latency efficient technology capable of delivering a cost effective implementation suitable for large scale deployment. 展开更多
关键词 opticAL control Plane TRANSLUCENT WDM opticAL Network Physical Layer IMPAIRMENTS Regenerators All-optical Wave-Length Converters GMPLS PLI-SQARWA
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The Effects of Power Control on Free-Space Optical Communications during Snowfall and Rainfall
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作者 Salem Salamah Muhammad A. Alsubaie +2 位作者 Mubarak Alhajri Mahmoud Alnaser Ahmed Mohamed Abdalla 《International Journal of Communications, Network and System Sciences》 2018年第10期216-227,共12页
Free-space optical (FSO) communication requires a line-of-sight connection between a transmitter and a receiver in which the information signal is modulated by an optical carrier that propagates in free space. The FSO... Free-space optical (FSO) communication requires a line-of-sight connection between a transmitter and a receiver in which the information signal is modulated by an optical carrier that propagates in free space. The FSO channel is greatly affected by weather conditions such as fog, rain, and snow. In the literature, several adaptive techniques, such as power control (PC), have been suggested to mitigate channel link degradations. In this paper, we investigate the effects of snow and rain attenuation on the bit error rate (BER) of the FSO system using two types of modulations, the on-off keying (OOK) modulation and the pulse-position modulation (16-PPM). The effect of PC on the performance of FSO communications is also examined in this study. We evaluated the system’s performance with two types of snow, wet snow and dry snow, as well as with different rain regions. Results show that PC improves the BER of the FSO system;a high rate of improvement is found for wet snow and rain. PC has almost no effect with dry snow because of the high attenuation and the limitations on transmitted power. The BER for 16-PPM is better than that for OOK modulation. 展开更多
关键词 Free Space optical Communications SNOW ATTENUATION RAIN ATTENUATION Power control
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An autobias control system for the electro optic modulator used in a quantum key distribution system 被引量:1
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作者 陈文芬 魏正军 +6 位作者 郭莉 侯丽燕 王赓 王金东 张智明 郭建平 刘颂豪 《Chinese Physics B》 SCIE EI CAS CSCD 2014年第8期261-268,共8页
In a quantum key distribution system, it is crucial to keep the extinction ratio of the coherent pulses stable. This means that the direct current bias point of the electro-optic modulator (EOM) used for generating ... In a quantum key distribution system, it is crucial to keep the extinction ratio of the coherent pulses stable. This means that the direct current bias point of the electro-optic modulator (EOM) used for generating coherent pulses must be locked. In this paper, an autobias control system based on a lock-in-amplifier for the EOM is introduced. Its drift information extracting theory and control method are analyzed comprehensively. The long term drift of the extinction ratio of the coherent pulses is measured by a single photon detector, which indicates that the autobias control system is effective for stabilizing the bias point of the EOM. 展开更多
关键词 quantum key distribution electro-optic modulator autobias control lock-in-amplifier
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Determination of Impurity Silicon in Anticancer Drug (Ge-132) by Electrothermally Atomised Atomic Absorption Spectrometry with Optical Temperature Control Accessory
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作者 Xie Shujuan, Wang Daning and Zou Mingqiang (Jilin I/E Commodity Inspection Bureau, Changchun)Cui Xiaoyuan,Ren Yulin and Zheng Yansheng (Department of Chemistry, Jilin University, Changchun)Wang Jincheng (Dalian Military Medical School, Dalian) 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1991年第4期205-211,共7页
The present paper describes the ashing and atomization processes in silicon analysis by electrothermally atomised atomic absorption spectrometry(EAAAS) with an uncoat-ed graphite tube, a pyrolytically coated graphite ... The present paper describes the ashing and atomization processes in silicon analysis by electrothermally atomised atomic absorption spectrometry(EAAAS) with an uncoat-ed graphite tube, a pyrolytically coated graphite tube and a tungsten-coated graphitetube. The sensitivity and linear range of three graphite tubes were compared. By using optical temperature control accessory, the signals are enhanced by a factor of 2 and the germanium interferences in the determination of silicon are eliminated. The effects of time constant and carrier gas flow-rate on the determination of silicon were also tested. The sample can be directly analyzed in its aqueous solution without any pretreatment. The measurements of samples containing 0. 2 μg/mL and 0. 4 μg/mL silicon were run ten times and the variation coefficient is 4. 9% and 2.6%, respectively. The recovery tests for carboxyethyl germanium sesquioxide(Ge-132) synthesized and imported were performed, and the recoveries are 97. 0% and 110%, respectively. Keywords Carboxyethyl germanium sesquioxide, Electrothermally atomised atomic absorption spectrometry, Silicon 展开更多
关键词 Determination of Impurity Silicon in Anticancer Drug by Electrothermally Atomised Atomic Absorption Spectrometry with optical Temperature control Accessory GE-132
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