A wavelet-based spectral correlation algorithm to detect and estimate BPSK signal chip rate is proposed. Simulation results show that the proposed method can correctly estimate the BPSK signal chip rate, which may be ...A wavelet-based spectral correlation algorithm to detect and estimate BPSK signal chip rate is proposed. Simulation results show that the proposed method can correctly estimate the BPSK signal chip rate, which may be corrupted by the quadratic characteristics of the spectral correlation function, in a low SNR environment.展开更多
[ Objective] The research aimed to study assessment index system of the rainstorm disaster in Fujian Province based on spectral cluste- ring model with grey correlation analysis. [Method] According to meteorological d...[ Objective] The research aimed to study assessment index system of the rainstorm disaster in Fujian Province based on spectral cluste- ring model with grey correlation analysis. [Method] According to meteorological disaster yearbook in Fujian Province, by comprehensively consider- ing disaster-inducing factor, disaster-inducing environment, disaster-sustaining body and regional disaster-prevention level, evaluation index system of the regional rainstorm disaster in Fujian was established. By spectral clustering model based on grey correlation analysis, dsk zoning of the rain- storm disaster was conducted in each area of Fujian. Finally, effect and application of the clustering model were analyzed by case research. [ Re- sult] In order to dig immanent connection among regional characteristics and improve disaster-preventing linkage performance of the evaluation unit, a spectral clustering model based on grey correlation analysis was used to conduct risk zoning of the rainstorm disaster in Fujian Province. Moreo- ver, combined weight was introduced to judge each evaluation index, so as to adjust clustering model. By case study, rainstorm disaster levels in 67 counties were obtained. Internal characteristics of each type were analyzed, and main correlation factors of each type were extracted. It was compared with statistical result of the rainstorm disaster, verifying validity and feasibility of the model. [ Conclusion] The method was feasible, and its evaluated result had better differentiation and decision accuracv.展开更多
Systematic error suppression and test data processing are very important in improving the accuracy and sensitivity of the atom interferometer(AI)-based weak-equivalence-principle(WEP) test in space. Here we present a ...Systematic error suppression and test data processing are very important in improving the accuracy and sensitivity of the atom interferometer(AI)-based weak-equivalence-principle(WEP) test in space. Here we present a spectrum correlation method to investigate the test data of the AI-based WEP test in space by analyzing the characteristics of systematic errors and noises. The power spectrum of the Eotvos coefficient η, systematic errors, and noises in AI-based WEP test in space are analyzed and calculated in detail. By using the method, the WEP violation signal is modulated from direct current(DC) frequency band to alternating current(AC) frequency band. We find that the signal can be effectively extracted and the influence of systematic errors can be greatly suppressed by analyzing the power spectrum of the test data when the spacecraft is in an inertial pointing mode. Furthermore, the relation between the Eotvos coefficient η and the number of measurements is obtained under certain simulated parameters. This method will be useful for both isotopic and nonisotopic AI-based WEP tests in space.展开更多
Orthomorphic permutations have good characteristics in cryptosystems. In this paper, by using of knowledge about relation between orthomorphic permutations and multi-output functions, and conceptions of the generalize...Orthomorphic permutations have good characteristics in cryptosystems. In this paper, by using of knowledge about relation between orthomorphic permutations and multi-output functions, and conceptions of the generalized Walsh spectrum of multi-output functions and the auto-correlation function of multi-output functions to investigate the Walsh spectral characteristics and the auto-correlation function characteristics of orthormophic permutations, several results are obtained.展开更多
Cyclic spectral correlation above the bifrequency plane for the received signal was calculated by the strip spectral correlation algorithm (SSCA)and then was normalized. The result was expressed by matrix. The sum o...Cyclic spectral correlation above the bifrequency plane for the received signal was calculated by the strip spectral correlation algorithm (SSCA)and then was normalized. The result was expressed by matrix. The sum of error-square was computed between corresponding elements for the theoretical sampling matrix of all kinds of modulated signals and calculated matrix. The modulation type was recognized by exploiting the minimum value of the sum of error-square. No extracted characteristic parameter and prior information are needed for identifying the modulation type compared to the conventional methods. In addition, the new method extends the recognition scope and has high recognition probability at low SNR. The simulation results obtained by means of Monter-Carlo method proved the presented algorithm.展开更多
Many modulated communication signals exhibit a cyclostationarity (or periodic correlation) property. To exploit the underlying periodicity of the modulated signal in the real-time recognition schcme of radio eilviro...Many modulated communication signals exhibit a cyclostationarity (or periodic correlation) property. To exploit the underlying periodicity of the modulated signal in the real-time recognition schcme of radio eilvironments, this letter introduces a spectral correlation method to identify the number and the direction of multi-path in the environment of frequency-selective fading channel. By simulation, the graphs of spatial spectra corresponding to a certain cycle frequency is presented to show the accuracy of spectral correlation method in multi-path environment recognition.展开更多
We report the observed photon bunching statistics of biexciton cascade emission at zero time delay in single quantum dots by second-order correlation function g(2) (T) measurements under continuous wave excitation...We report the observed photon bunching statistics of biexciton cascade emission at zero time delay in single quantum dots by second-order correlation function g(2) (T) measurements under continuous wave excitation. It is found that the bunching phenomenon is independent of the biexciton binding energy when it varies from 0.59 meV to nearly zero. The photon bunching takes place when the exeiton photon is not spectrally distinguishable from the biexciton photon, and either of them can trigger the %tart' in a Hanbury-Brown and Twiss setup. However, if the exciton energy is spectrally distinguishable from the biexciton, the photon statistics will become asymmetric and a cross-bunching lineshape can be obtained. The theoretical calculations based on a model of three-level rate-equation analysis are consistent with the result of g(2)(τ) correlation function measurements.展开更多
In this study,seven isotopic databases are presented and analyzed to identify mantle and crustal episodes on a global scale by focusing on periodicity ranging from 70 to 200 million years(Myr).The databases are the la...In this study,seven isotopic databases are presented and analyzed to identify mantle and crustal episodes on a global scale by focusing on periodicity ranging from 70 to 200 million years(Myr).The databases are the largest,or among the largest,compiled for each type of data-with an objective of finding some samples from every region of every continent,to make each database as global as conceivably possible.The databases contain zircon Lu/Hf isotopic data,whole-rock Sm/Nd isotopic data,U/Pb detrital zircon ages,U/Pb igneous zircon ages,U/Pb non-zircon ages,whole-rock Re/Os isotopic data,and large igneous province ages.Part I of this study focuses on the periodicities of age histograms and geochemical averages developed from the seven databases,via spectral and cross-correlation analyses.Natural physical cycles often propagate in exact integer multiples of a fundamental cycle,referred to as harmonics.The tests show that harmonic geological cycles of^93.5 and^187 Myr have persisted throughout terrestrial history,and the cyclicities are statistically significant for U/Pb igneous zircon ages,U/Pb detrital zircon ages,U/Pb zircon-rim ages,large igneous province ages,meanεHf(t)for all samples,meanεHf(t)values for igneous-only samples,and relative abundance of mafic rocks.Equally important,cross-correlation analyses show these seven time-series are nearly synchronous(±7 Myr)with a model consisting of periodicities of 93.5 and 187 Myr.Additionally,the similarities between peaks in the 93.5 and 187 Myr mantle cycles and terminal ages of established and suspected superchrons provide a framework for predicting and testing superchron periodicity.展开更多
Time evolution dynamics of three non-coupled two-level atoms independently interacting with their reservoirs is solved exactly by considering a damping Lorentzian spectral density.For three atoms initially prepared in...Time evolution dynamics of three non-coupled two-level atoms independently interacting with their reservoirs is solved exactly by considering a damping Lorentzian spectral density.For three atoms initially prepared in Greenberger-Horne-Zeilinger-type state,quantum correlation dynamics in a Markovian reservoir is compared with that in a nonMarkovian reservoir.By increasing detuning quantity in the non-Markovian reservoir,three-atom correlation dynamics measured by negative eigenvalue presents a trapping phenomenon which provides long-time quantum entanglement.Then we compare the correlation dynamics of three atoms with that of two atoms,measured by quantum entanglement and quantum discord for an initial robuster-entangled type state.The result further confirms that quantum discord is indeed different from quantum entanglement in identifying quantum correlation of many bodies.展开更多
Chaotic dynamics of highly excited vibration of deuterium cyanide is explored by two independent approaches: (1) the Lyapunov analysis, based on the classical phase space for the levels, and (2) the Dixon dip ana...Chaotic dynamics of highly excited vibration of deuterium cyanide is explored by two independent approaches: (1) the Lyapunov analysis, based on the classical phase space for the levels, and (2) the Dixon dip analysis based on the concepts of pendulum dynamics and quantized levels. The results show that there is evident correlation between these two algorithms. We also propose that the reciprocal of energy difference between two nearby Dixon dips can be taken as a qualitative measure for the degree of dynamical chaos.展开更多
To solve the problem of the spatial correlation for adjacent areas in traditional spectral unmixing methods, we propose an area-correlated spectral unmixing method based on Bayesian nonnegative matrix factorization. I...To solve the problem of the spatial correlation for adjacent areas in traditional spectral unmixing methods, we propose an area-correlated spectral unmixing method based on Bayesian nonnegative matrix factorization. In the proposed me-thod, the spatial correlation property between two adjacent areas is expressed by a priori probability density function, and the endmembers extracted from one of the adjacent areas are used to estimate the priori probability density func-tions of the endmembers in the current area, which works as a type of constraint in the iterative spectral unmixing process. Experimental results demonstrate the effectivity and efficiency of the proposed method both for synthetic and real hyperspectral images, and it can provide a useful tool for spatial correlation and comparation analysis between ad-jacent or similar areas.展开更多
Most noise suppression algorithms of single channel use the mean of noisy segments to estimate the characteristics of noise spectrum, ignoring the estimation of noise in speech segments. Therefore, when the energy lev...Most noise suppression algorithms of single channel use the mean of noisy segments to estimate the characteristics of noise spectrum, ignoring the estimation of noise in speech segments. Therefore, when the energy level of noise varies with the time, the performance of removing noise will be degraded. To solve this problem, a speech enhancement approach based on dynamic noise estimation within correlation domain was proposed. This method exploits the characteristics that noise energy mainly concentrates on 0 th order correlation coefficients, signal is auto correlated but signal and noise, noise and noise are uncorrelated, then estimates and decomposes the noise, thus helps to solve the above mentioned problem. The results of recognition experiments on speech signals of 15 Chinese cities’ names corrupted by noise of exhibition hall shows, this approach is better than SS (Spectral Subtraction) method, adapts better to the variances of energy levels of speech signal corrupted by noise, has some practicability to improve the robustness of recognition systems under noisy environment.展开更多
The fluorescence emission wavelength [lambda(max(em))] values of three types of benzaldehyde derivatives, namely, ethylene acetals (1-Ys), 4-nitrophenylhydrazones (2-Ys) and phenylhydrazones (3-Ys), have been measured...The fluorescence emission wavelength [lambda(max(em))] values of three types of benzaldehyde derivatives, namely, ethylene acetals (1-Ys), 4-nitrophenylhydrazones (2-Ys) and phenylhydrazones (3-Ys), have been measured. Correlation analyses by the dual-parameter equation show that the lambda(max(em)) values of 1-Ys are mainly affected by the spin-delocalization effects of the substituents, while those of 2-Ys are mainly affected by the polar effects. However, those of 3-Ys are independent of the substituents.展开更多
基于浙江测震台网记录到的2017年2—9月磐安地区发生的地震序列资料,采用Brune震源模型理论和波谱分析方法,得到磐安震群序列的应力降、视应力等震源参数。利用台站的零频幅值,计算谱振幅相关系数。采用聚类分组,并结合Cut and Paste(C...基于浙江测震台网记录到的2017年2—9月磐安地区发生的地震序列资料,采用Brune震源模型理论和波谱分析方法,得到磐安震群序列的应力降、视应力等震源参数。利用台站的零频幅值,计算谱振幅相关系数。采用聚类分组,并结合Cut and Paste(CAP)反演方法得到ML4.0主地震事件的震源机制解,系统分析小地震的震源机制的一致性程度。结果显示:震源区应力降值在0.00~0.80 MPa之间,整体构造应力较低;谱振幅相关系数较低,在0.86~0.95之间,震源机制整体相似程度不高;应力积累没有形成一个优势方向,可能指示磐安序列为低摩擦应力的断层作用。研究结果表明:磐安地震序列为普通的小震序列,其震源机制类型与构造应力场基本一致;谱振幅相关分析法可为小震序列的震后快速判定提供重要依据。展开更多
为优化黄芪瞬时高温灭菌(high temperature short time,HTST)工艺参数并多维度考察其对黄芪质量的影响,基于指标相关性的权重系数(criteria importance though intercrieria correlation,CRITIC)法采用正交设计优化黄芪灭菌工艺参数,以...为优化黄芪瞬时高温灭菌(high temperature short time,HTST)工艺参数并多维度考察其对黄芪质量的影响,基于指标相关性的权重系数(criteria importance though intercrieria correlation,CRITIC)法采用正交设计优化黄芪灭菌工艺参数,以灭菌温度、灭菌时间、药材粉碎粒度为考察因素,以灭菌率、5种化合物含量及1,1-二苯基-2-苦基肼自由基(1,1-diphenyl-2-picrylhydrazyl,DPPH·)清除率为考察指标,通过直观及方差分析评价灭菌对3个考察指标的影响;并运用液质联用技术(liquid chromatography-mass spectrometry,LC-MS)确认指纹图谱共有峰的结构,以偏最小二乘回归分析法分析共有峰与抗氧化活性的谱效关系。结果显示,灭菌温度是具有显著影响的因素(P<0.05),最佳灭菌工艺参数为灭菌温度(170±2)℃,灭菌时间5 s,粉碎粒度50目;按优化工艺灭菌后的3批样品微生物水平均符合药典规定,5种化合物含量及DPPH·清除率与灭菌前比较无明显变化;灭菌前后指纹图谱相似度均大于0.900;谱效学分析相关性结果与化合物单体抗氧化的试验结果及其结构特点基本一致。综上所述,瞬时高温灭菌对黄芪中微生物具有明显杀灭作用且对其质量无明显影响,表明该方法适用于黄芪药材灭菌。展开更多
文摘A wavelet-based spectral correlation algorithm to detect and estimate BPSK signal chip rate is proposed. Simulation results show that the proposed method can correctly estimate the BPSK signal chip rate, which may be corrupted by the quadratic characteristics of the spectral correlation function, in a low SNR environment.
基金Supported by Special Item of the Public Sector(Meteorological) Science Research(GYHY201106040)
文摘[ Objective] The research aimed to study assessment index system of the rainstorm disaster in Fujian Province based on spectral cluste- ring model with grey correlation analysis. [Method] According to meteorological disaster yearbook in Fujian Province, by comprehensively consider- ing disaster-inducing factor, disaster-inducing environment, disaster-sustaining body and regional disaster-prevention level, evaluation index system of the regional rainstorm disaster in Fujian was established. By spectral clustering model based on grey correlation analysis, dsk zoning of the rain- storm disaster was conducted in each area of Fujian. Finally, effect and application of the clustering model were analyzed by case research. [ Re- sult] In order to dig immanent connection among regional characteristics and improve disaster-preventing linkage performance of the evaluation unit, a spectral clustering model based on grey correlation analysis was used to conduct risk zoning of the rainstorm disaster in Fujian Province. Moreo- ver, combined weight was introduced to judge each evaluation index, so as to adjust clustering model. By case study, rainstorm disaster levels in 67 counties were obtained. Internal characteristics of each type were analyzed, and main correlation factors of each type were extracted. It was compared with statistical result of the rainstorm disaster, verifying validity and feasibility of the model. [ Conclusion] The method was feasible, and its evaluated result had better differentiation and decision accuracv.
基金Project supported by the National Natural Science Foundation of China(Grants No.11947057)the Foundation for Distinguished Young Scientist of Jiangxi Province,China(Grant No.2016BCB23009)the Postdoctoral Applied Research Program of Qingdao City,Shandong Province,China(Grant No.62350079311135).
文摘Systematic error suppression and test data processing are very important in improving the accuracy and sensitivity of the atom interferometer(AI)-based weak-equivalence-principle(WEP) test in space. Here we present a spectrum correlation method to investigate the test data of the AI-based WEP test in space by analyzing the characteristics of systematic errors and noises. The power spectrum of the Eotvos coefficient η, systematic errors, and noises in AI-based WEP test in space are analyzed and calculated in detail. By using the method, the WEP violation signal is modulated from direct current(DC) frequency band to alternating current(AC) frequency band. We find that the signal can be effectively extracted and the influence of systematic errors can be greatly suppressed by analyzing the power spectrum of the test data when the spacecraft is in an inertial pointing mode. Furthermore, the relation between the Eotvos coefficient η and the number of measurements is obtained under certain simulated parameters. This method will be useful for both isotopic and nonisotopic AI-based WEP tests in space.
基金Supported by State Key Laboratory of InformationSecurity Opening Foundation(01-02) .
文摘Orthomorphic permutations have good characteristics in cryptosystems. In this paper, by using of knowledge about relation between orthomorphic permutations and multi-output functions, and conceptions of the generalized Walsh spectrum of multi-output functions and the auto-correlation function of multi-output functions to investigate the Walsh spectral characteristics and the auto-correlation function characteristics of orthormophic permutations, several results are obtained.
文摘Cyclic spectral correlation above the bifrequency plane for the received signal was calculated by the strip spectral correlation algorithm (SSCA)and then was normalized. The result was expressed by matrix. The sum of error-square was computed between corresponding elements for the theoretical sampling matrix of all kinds of modulated signals and calculated matrix. The modulation type was recognized by exploiting the minimum value of the sum of error-square. No extracted characteristic parameter and prior information are needed for identifying the modulation type compared to the conventional methods. In addition, the new method extends the recognition scope and has high recognition probability at low SNR. The simulation results obtained by means of Monter-Carlo method proved the presented algorithm.
文摘Many modulated communication signals exhibit a cyclostationarity (or periodic correlation) property. To exploit the underlying periodicity of the modulated signal in the real-time recognition schcme of radio eilvironments, this letter introduces a spectral correlation method to identify the number and the direction of multi-path in the environment of frequency-selective fading channel. By simulation, the graphs of spatial spectra corresponding to a certain cycle frequency is presented to show the accuracy of spectral correlation method in multi-path environment recognition.
基金Supported by the National Key Basic Research Program of China under Grant No 2013CB922304the National Natural Science Foundation of China under Grant Nos 11474275 and 11464034
文摘We report the observed photon bunching statistics of biexciton cascade emission at zero time delay in single quantum dots by second-order correlation function g(2) (T) measurements under continuous wave excitation. It is found that the bunching phenomenon is independent of the biexciton binding energy when it varies from 0.59 meV to nearly zero. The photon bunching takes place when the exeiton photon is not spectrally distinguishable from the biexciton photon, and either of them can trigger the %tart' in a Hanbury-Brown and Twiss setup. However, if the exciton energy is spectrally distinguishable from the biexciton, the photon statistics will become asymmetric and a cross-bunching lineshape can be obtained. The theoretical calculations based on a model of three-level rate-equation analysis are consistent with the result of g(2)(τ) correlation function measurements.
文摘In this study,seven isotopic databases are presented and analyzed to identify mantle and crustal episodes on a global scale by focusing on periodicity ranging from 70 to 200 million years(Myr).The databases are the largest,or among the largest,compiled for each type of data-with an objective of finding some samples from every region of every continent,to make each database as global as conceivably possible.The databases contain zircon Lu/Hf isotopic data,whole-rock Sm/Nd isotopic data,U/Pb detrital zircon ages,U/Pb igneous zircon ages,U/Pb non-zircon ages,whole-rock Re/Os isotopic data,and large igneous province ages.Part I of this study focuses on the periodicities of age histograms and geochemical averages developed from the seven databases,via spectral and cross-correlation analyses.Natural physical cycles often propagate in exact integer multiples of a fundamental cycle,referred to as harmonics.The tests show that harmonic geological cycles of^93.5 and^187 Myr have persisted throughout terrestrial history,and the cyclicities are statistically significant for U/Pb igneous zircon ages,U/Pb detrital zircon ages,U/Pb zircon-rim ages,large igneous province ages,meanεHf(t)for all samples,meanεHf(t)values for igneous-only samples,and relative abundance of mafic rocks.Equally important,cross-correlation analyses show these seven time-series are nearly synchronous(±7 Myr)with a model consisting of periodicities of 93.5 and 187 Myr.Additionally,the similarities between peaks in the 93.5 and 187 Myr mantle cycles and terminal ages of established and suspected superchrons provide a framework for predicting and testing superchron periodicity.
基金Project supported by the National Natural Science Foundation of China (Grant Nos. 11104113 and 11264011)the Natural Science Foundation of Hunan Province,China (Grant Nos. 09JJ6011 and 11JJ6007)
文摘Time evolution dynamics of three non-coupled two-level atoms independently interacting with their reservoirs is solved exactly by considering a damping Lorentzian spectral density.For three atoms initially prepared in Greenberger-Horne-Zeilinger-type state,quantum correlation dynamics in a Markovian reservoir is compared with that in a nonMarkovian reservoir.By increasing detuning quantity in the non-Markovian reservoir,three-atom correlation dynamics measured by negative eigenvalue presents a trapping phenomenon which provides long-time quantum entanglement.Then we compare the correlation dynamics of three atoms with that of two atoms,measured by quantum entanglement and quantum discord for an initial robuster-entangled type state.The result further confirms that quantum discord is indeed different from quantum entanglement in identifying quantum correlation of many bodies.
基金Supported by the National Natural Science Foundation of China under Grant No 20373030, the Key Project of the Ministry of Education of China under Grant No 306020.
文摘Chaotic dynamics of highly excited vibration of deuterium cyanide is explored by two independent approaches: (1) the Lyapunov analysis, based on the classical phase space for the levels, and (2) the Dixon dip analysis based on the concepts of pendulum dynamics and quantized levels. The results show that there is evident correlation between these two algorithms. We also propose that the reciprocal of energy difference between two nearby Dixon dips can be taken as a qualitative measure for the degree of dynamical chaos.
文摘To solve the problem of the spatial correlation for adjacent areas in traditional spectral unmixing methods, we propose an area-correlated spectral unmixing method based on Bayesian nonnegative matrix factorization. In the proposed me-thod, the spatial correlation property between two adjacent areas is expressed by a priori probability density function, and the endmembers extracted from one of the adjacent areas are used to estimate the priori probability density func-tions of the endmembers in the current area, which works as a type of constraint in the iterative spectral unmixing process. Experimental results demonstrate the effectivity and efficiency of the proposed method both for synthetic and real hyperspectral images, and it can provide a useful tool for spatial correlation and comparation analysis between ad-jacent or similar areas.
文摘Most noise suppression algorithms of single channel use the mean of noisy segments to estimate the characteristics of noise spectrum, ignoring the estimation of noise in speech segments. Therefore, when the energy level of noise varies with the time, the performance of removing noise will be degraded. To solve this problem, a speech enhancement approach based on dynamic noise estimation within correlation domain was proposed. This method exploits the characteristics that noise energy mainly concentrates on 0 th order correlation coefficients, signal is auto correlated but signal and noise, noise and noise are uncorrelated, then estimates and decomposes the noise, thus helps to solve the above mentioned problem. The results of recognition experiments on speech signals of 15 Chinese cities’ names corrupted by noise of exhibition hall shows, this approach is better than SS (Spectral Subtraction) method, adapts better to the variances of energy levels of speech signal corrupted by noise, has some practicability to improve the robustness of recognition systems under noisy environment.
文摘The fluorescence emission wavelength [lambda(max(em))] values of three types of benzaldehyde derivatives, namely, ethylene acetals (1-Ys), 4-nitrophenylhydrazones (2-Ys) and phenylhydrazones (3-Ys), have been measured. Correlation analyses by the dual-parameter equation show that the lambda(max(em)) values of 1-Ys are mainly affected by the spin-delocalization effects of the substituents, while those of 2-Ys are mainly affected by the polar effects. However, those of 3-Ys are independent of the substituents.
文摘基于浙江测震台网记录到的2017年2—9月磐安地区发生的地震序列资料,采用Brune震源模型理论和波谱分析方法,得到磐安震群序列的应力降、视应力等震源参数。利用台站的零频幅值,计算谱振幅相关系数。采用聚类分组,并结合Cut and Paste(CAP)反演方法得到ML4.0主地震事件的震源机制解,系统分析小地震的震源机制的一致性程度。结果显示:震源区应力降值在0.00~0.80 MPa之间,整体构造应力较低;谱振幅相关系数较低,在0.86~0.95之间,震源机制整体相似程度不高;应力积累没有形成一个优势方向,可能指示磐安序列为低摩擦应力的断层作用。研究结果表明:磐安地震序列为普通的小震序列,其震源机制类型与构造应力场基本一致;谱振幅相关分析法可为小震序列的震后快速判定提供重要依据。
文摘为优化黄芪瞬时高温灭菌(high temperature short time,HTST)工艺参数并多维度考察其对黄芪质量的影响,基于指标相关性的权重系数(criteria importance though intercrieria correlation,CRITIC)法采用正交设计优化黄芪灭菌工艺参数,以灭菌温度、灭菌时间、药材粉碎粒度为考察因素,以灭菌率、5种化合物含量及1,1-二苯基-2-苦基肼自由基(1,1-diphenyl-2-picrylhydrazyl,DPPH·)清除率为考察指标,通过直观及方差分析评价灭菌对3个考察指标的影响;并运用液质联用技术(liquid chromatography-mass spectrometry,LC-MS)确认指纹图谱共有峰的结构,以偏最小二乘回归分析法分析共有峰与抗氧化活性的谱效关系。结果显示,灭菌温度是具有显著影响的因素(P<0.05),最佳灭菌工艺参数为灭菌温度(170±2)℃,灭菌时间5 s,粉碎粒度50目;按优化工艺灭菌后的3批样品微生物水平均符合药典规定,5种化合物含量及DPPH·清除率与灭菌前比较无明显变化;灭菌前后指纹图谱相似度均大于0.900;谱效学分析相关性结果与化合物单体抗氧化的试验结果及其结构特点基本一致。综上所述,瞬时高温灭菌对黄芪中微生物具有明显杀灭作用且对其质量无明显影响,表明该方法适用于黄芪药材灭菌。