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Microwave-assisted synthesis of new N^4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions 被引量:4
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作者 Qing Han Li Zhi Gang Zhao 《Chinese Chemical Letters》 SCIE CAS CSCD 2008年第9期1035-1038,共4页
Six new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from [bi-(4-fluorophenyl)-methyl]-piperazine in solvent-free condition under microwave irradiation with excell... Six new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from [bi-(4-fluorophenyl)-methyl]-piperazine in solvent-free condition under microwave irradiation with excellent yields. Their structures have been determined by elemental analysis, IR, MS and 1H NMR data. 展开更多
关键词 bi-(4-Fluorophenyl)-methyl]-piperazine THIOSEMICARBAZONES Microwave irradiation SOLVENT-FREE organic synthese
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