The fracture toughness of a carbon/carbon composites oxidized at different temperature for 1 h was measured. The fracture surfaces were examined by scanning electron microscopy (SEM). The results indicate that oxida...The fracture toughness of a carbon/carbon composites oxidized at different temperature for 1 h was measured. The fracture surfaces were examined by scanning electron microscopy (SEM). The results indicate that oxidation temperature has significant effects on the fracture toughness. Fracture toughness decreases with the increase of the weight loss. The SEM images reveal that the decrease of fracture toughness was mainly attributed to the oxidation of the interface in the composite.展开更多
Three different castables based on the Al_2O_3–MgO –CaO system were prepared as steel-ladle purging plug refractories: corundum-based low-cement castable(C-LCC), corundum-spinel-based low-cement castable(C-S-LCC...Three different castables based on the Al_2O_3–MgO –CaO system were prepared as steel-ladle purging plug refractories: corundum-based low-cement castable(C-LCC), corundum-spinel-based low-cement castable(C-S-LCC), and corundum-spinel no-cement castable(C-S-NCC)(hydratable alumina(ρ-Al_2O_3) bonded). The fracture behavior at room temperature was tested by the method of "wedge-splitting" on samples pre-fired at different temperatures; the specific fracture energy G′f and notched tensile strength σNT were obtained from these tests. In addition, the Young's modulus E was measured by the method of resonance frequency of damping analysis(RFDA). The thermal stress resistance parameter R′′′′ calculated using the values of G′f, σNT, and E was used to evaluate the thermal shock resistance of the materials. According to the microstructure analysis results, the sintering effect and the bonding type of the matrix material were different among these three castables, which explains their different fracture behaviors.展开更多
基金Funded by National Natural Science Foundation of China(No.50702045)the Program for New Century Excellent Talents in University(No.NCET-08-0460)Basic Research Foundation of NWPU(No.JC20100227)
文摘The fracture toughness of a carbon/carbon composites oxidized at different temperature for 1 h was measured. The fracture surfaces were examined by scanning electron microscopy (SEM). The results indicate that oxidation temperature has significant effects on the fracture toughness. Fracture toughness decreases with the increase of the weight loss. The SEM images reveal that the decrease of fracture toughness was mainly attributed to the oxidation of the interface in the composite.
文摘Three different castables based on the Al_2O_3–MgO –CaO system were prepared as steel-ladle purging plug refractories: corundum-based low-cement castable(C-LCC), corundum-spinel-based low-cement castable(C-S-LCC), and corundum-spinel no-cement castable(C-S-NCC)(hydratable alumina(ρ-Al_2O_3) bonded). The fracture behavior at room temperature was tested by the method of "wedge-splitting" on samples pre-fired at different temperatures; the specific fracture energy G′f and notched tensile strength σNT were obtained from these tests. In addition, the Young's modulus E was measured by the method of resonance frequency of damping analysis(RFDA). The thermal stress resistance parameter R′′′′ calculated using the values of G′f, σNT, and E was used to evaluate the thermal shock resistance of the materials. According to the microstructure analysis results, the sintering effect and the bonding type of the matrix material were different among these three castables, which explains their different fracture behaviors.